Capability Manual

Middle East CAPABILITY MANUAL

Management Office & Dubai Laboratory Fujairah

:

P.O Box.5778, TP/010305, Techno Park, Dubai, U.A.E., Tel. +971-4-8867400, Fax. +971-4-8867401/8867402 Email : [email protected]; [email protected]; [email protected]

:

Fujairah Free Zone 1, P.O Box. 3026, Fujairah, U.A.E Lab : Tel : +9719 2228360, Fax: +9719 2228370, Email : geo_chem @eim.ae Operations : Tel:+9719 2282927, Fax: +9719 2282928, Email: [email protected]

Revision No. 09 ; Revision Date : 15/05/2010

We offer the following services INSPECTION

ANALYSIS

Marine survey Bunker survey De-ballasting monitoring On hire/off hire survey Inspection of vessel tanks Inter tank transfer operation Doping operation Deslopping operation Supervision of Loading Discharge supervision Loss minimisation Investigation of loss/shortage Draft survey ROB survey Sampling Stock verification Stock monitoring Inspection of Pipe lines

Condensate/Crude oil Potable/ Fresh /Waste water Biological & Microbiological testing Naphtha Aviation fuel Gasoline Bunker, Diesel & Long Residue Asphalt & Bitumen Lubricant, Transformer Oil Gas Petrochemical, Solvent & Aromatics Fertilizer Fire Fighting Foam Food Coolant Detergent Halon Tea Sugar Metals Agricultural products Chemicals Pharmaceuticals Dyes and dye intermediate Processed and packaged food products Stack Monitoring

CALIBRATION Temperature, Pressure, Weight (Mass) & Storage Tanks

MAN POWER SUPPLY TECHNICAL SPECIALISTS, CHEMISTS & LABORATORY TECHNICIANS PROVIDED TO CUSTOMER LOCATIONS TO UNDERTAKE QUALITY CONTROL ANALYSIS. SPECIAL PROJECTS AT OFFSHORE & ONSHORE FACILITIES. Revision No. 09 ; Revision Date : 15/05/2010

TABLE OF CONTENTS Sl.No.

PRODUCT

PAGES

1

CONDENSATE / CRUDE OIL ANALYSIS

2-4

2

POTABLE /FRESH WATER ANALYSIS

5-7

3

WASTE WATER & GROUND WATER ANALYSIS

8

4

MICROBIOLOGICAL ANALYSIS

9

5

NAPHTHA ANALYSIS

10-12

6

AVIATION FUEL / KEROSENE ANALYSIS

13-14

7

GASOLINE ANALYSIS

15-16

8

BUNKER FUEL, DIESEL OIL & LONG RESIDUE ANALYSIS

17-19

9

ASPHALT / BITUMEN ANALYSIS

10

LUBRICANT ANALYSIS

11

GREASE ANALYSIS

23

12

BASE OIL ANALYSIS

24

13

TRANSFORMER OIL ANALYSIS

25

14

PETROCHEMICALS, SOLVENTS & AROMATICS

15

GAS ANALYSIS

28

16

FERTILIZER ANALYSIS

29

17

FIRE FIGHTING FOAM ANALYSIS

30

18

FOOD ANALYSIS

31

19

COOLANT ANALYSIS

32

20

DETERGENT ANALYSIS

32

21

HALOGEN ANALYSIS

32

22

TEA ANALYSIS

33

23

SUGAR ANALYSIS

33

24

AMBIENT & INDOOR AIR QUALITY MONITORING / NOISE MONITORING

34

25

FLUE GAS / STACK MONITORING

35

26

MISCELLANEOUS ANALYSIS

36

27

CALIBRATION

37

Geo-Chem Middle East

Revision No.09;Revision Date :15-05-2010

20 21-22

26-27

Page 1 of 37

CONDENSATE/CRUDE OIL ANALYSIS TEST, UNIT Acidity, mg KOH/g Acidity, mg KOH/g Acidity, mg KOH/g API Gravity @ 60 °F API Gravity @ 60 °F API Gravity @ 60 °F API Gravity @ 60 °F Appearance Arsenic, ppb Arsenic, ppb Ash Content, % Wt Asphaltine Content, % Wt B S & Water, % Vol B S & Water, % Vol B S & Water, % Vol Benzene Content, % Vol Carbon Residue % Wt Carbon Residue % Wt Carbon Residue on 10 % Residue Carbon Residue on 10 % Residue Cetane Index Chloride Content,ppm Chloride, ppm Chloride, ppm Chloride, ppm Chloride, ppm Chloride, ppm Chloride, ppm Cloud Point, °C Cloud Point, °C Colour Saybolt Composition upto C 36+ Copper Corrosion (3hrs at 100°C),Rating Density, kg/L Density, kg/L Density, kg/L Distillation, °C Distillation, °C


METHOD ASTM D 664 ASTM D 974 IP 139 ASTM D 1298 ASTM D 4052 ASTM D 5002 IP 365 Visual UOP 296 UOP 387 ASTM D 482 IP 143 ASTM D 1796 ASTM D 2709 ASTM D 4007 ASTM D 3606 ASTM D 524 IP 14 ASTM D 189 IP 13 ASTM D 976 ASTM D 808 ASTM D 4929 ASTM D 5194 MCT UOP 395 UOP 588 UOP 779 ASTM D 2500 IP 219 ASTM D 156 GC ASTM D 130 ASTM D 1298 ASTM D 4052 IP 150 ASTM D 86 IP 123


Page 2 of 37

CONDENSATE/CRUDE OIL ANALYSIS TEST, UNIT Existing Gum, mg/100 ml Finger Print Analysis Flash Point, °C Flash Point, °C Hydrocarbon Types, % Vol, Hydrogen Sulphide Content, ppm Hydrogen Sulphide Content, ppm Hydrogen Sulphide Content, ppm Hydrogen Sulphide on Vapour Space, ppm Kinematic Viscosity, cSt Kinematic Viscosity, cSt Kvalue Lead Content, ppb Lead Content, ppb Mercaptan Sulphur Content, ppm Mercaptan Sulphur Content, ppm Mercaptan Sulphur Content, ppm Mercaptan Sulphur Content, ppm Mercury, ppb Mercury, ppb Metals (Trace), ppm Metals Content, ppm Metals Content, ppm Micro Carbon Residue % Wt. Micro Carbon Residue on 10% bottom, % Wt MTBE (Oxygenates), % Wt Nitrogen (Basic), ppm Nitrogen Content, % Wt Nitrogen Content, ppm Wt Nitrogen Content, ppm Wt Oxygenates (Trace), ppm Wt Paraffin wax, %wt PIONA PONA Analysis by GC Pour Point, °C Pour Point, °C R.V.P @ 100 °F, psi R.V.P @ 100 °F, psi Relative Density Geo-Chem Middle East

METHOD ASTM D 381 FT IR ASTM D93 IP 170 GC DHA IP 103 Method B Mobil MM 787 UOP 169 ASTM D 5705 ASTM D 445 IP 71 UOP 375 IP 224 UOP 350 ASTM D 3227 ASTM D 5623 IP 104 IP 342 AAS Cold Vapour UOP 938 UOP 391 AAS ICP ASTM D 4530 ASTM D 4530 ASTM D 4815 UOP 430 ASTM D 3228 ASTM D 4629 ASTM D 5762 LOWOX-GC UOP 46 G C DHA (ASTM D 6730) ASTM D 5443 ASTM D 97 IP 15 ASTM D 323 IP 69 ASTM D 1298


Page 3 of 37

CONDENSATE/CRUDE OIL ANALYSIS TEST, UNIT Relative Density Salt Content, ptb Sediment by Extraction, % Wt. Sediment by Extraction, % Wt. Sediment by Mem. Filtration, % Wt Sulphur Content, %wt Sulphur Content, ppm Wt True Boiling Point ( Assay), °C Water Content, % Vol Water Content, % Vol Water Content, ppm Water Content, ppm Water by distillation, % Vol


METHOD ASTM D ASTM D ASTM D IP 53 ASTM D ASTM D ASTM D ASTM D ASTM D IP 358 ASTM D ASTM D ASTM D


4052 3230 473 4807 4294 5453 2892 4006 4377 4928 95

Page 4 of 37

POTABLE /FRESH WATER ANALYSIS TEST, UNIT Appearance Acidity Aluminium Aluminium Alkalinity Ammonia Antimony Arsenic Selenium Bicarbonate Barium Barium Bismuth Bismuth Boron Boron Bromide Cadmium Cadmium Calcium Calcium Calcium Carbon Dioxide Carbonate Chromium ( Total) Chromium ( Total) Chromium ( Hexavalent) Chloride Chlorine Colour Copper Copper Cobalt Cobalt Cyanide Cyanide Detergent ( Anionic) Electrical Conductivity


METHOD APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA

2110 (Visual) 2310 B 3111 D 3120 B 2320 B 4500 NH3 B & C 3111 B 3114 B & C 3114 B & C 2320 B 3111 D 3120 D 3111 B 3120 B 3111 D 3120 B 4500 Br.B 3111 B 3120 B 3111 B 3500 Ca.B 3120B 4500 Co2 B, C, D 2320 B 3111 B 3120 B 3500 Cr.B 4500 Cl.B 4500 – Cl B, G 2120 B 3111 B 3120 B 3111B 3120 B 4500 CN-E, D

APHA 4500 CN- D APHA 5540 APHA 2510 B


Page 5 of 37

POTABLE /FRESH WATER ANALYSIS TEST, UNIT

METHOD

Fluoride Floatables ( Particulate)

APHA 4500 F-D APHA 2530 B

Fixed and volatile solids ignited @ 550°C Hydrogen Sulphide Hydroxyl Hydrazine Hardness Iron Iron Iodine Iodide Lead Lithium Magnesium Magnesium Magnesium Mercury Molybdenum Metals ( Al, Ba, Be, Ca, Mo, Si, V, Ti) Metals (Al, Ba, Be , Cd, Ca, Cr, Co, Cu, Fe, Pb, Mg, Mn, Ni, Ag, Na, Sr, Zn, Mo) Metals (Al, Ba, Be , Cd, Ca, Cr, Co, Cu, Fe, Pb, Mg, Mn, Ni, Ag, Na, Sr, Zn, Mo) Metals by ICP Nitrate Nitrite Nitrogen ( Ammonia ) Nitrogen ( Organic ) Nitrogen ( Nitrite ) Nitrogen ( Nitrate ) Odour Odour Oil & Grease Oxygen ( Dissolved) Particle Count Phenols pH Phosphate Phosphorous Potassium Potassium Redox Potential

APHA 2540 E APHA 4500 S2 APHA 2320 B UV Spectrometer APHA 2340 B & C APHA 3111 B APHA 3500 Fe-B APHA 4500 I APHA 4500 I- C APHA 3111 B APHA 3111 B APHA 3111 B EDTA Titrimetry APHA 3500 Mg.B APHA 3112 B APHA 3111 D APHA 3110 APHA 3111


APHA 3120 B APHA 3125 APHA 4500 NO3 B APHA 4500 NO2 B APHA 4500 NH3 B,C APHA 4500 N Org. B APHA 4500 NO2- B APHA 4500 NO3- B APHA 2150 B ASTM D – 12 92-86 APHA 5520 B, C APHA 4500 OC & G Coulter Counter APHA 5530 C & D APHA 4500 H+B APHA 4500 P-C APHA 4500 P APHA 3111 B APHA 3120 B APHA 2580 B


Page 6 of 37

POTABLE /FRESH WATER ANALYSIS Resistivity Residual Chlorine Settleable solids

TEST, UNIT

METHOD API 2.9 APHA 4500 Cl-G APHA 2540 F

Silica Silica Silica Silver Silver Sodium Sodium Sulfide Sulfide Sulphite Sulphate Strontium Strontium Surfactants ( Anionic ) Salinity Threshold Odour Tin Turbidity Total Hardness Total Solids Total Suspended Solid Total Dissolved Solid Titanium Titanium TPH TPH

APHA 3111 D APHA 4500 Si.C APHA 4500 Si.D APHA 3111 B APHA 3120 B APHA 3111 B APHA 3120 B APHA 4500 S2 D APHA 4500 S2 E APHA 4500 SO3 B APHA 4500 S042-B APHA 3111 B APHA 3120 B APHA 5540 C APHA 2520 B/C APHA 2150 B APHA 3111 B APHA 2130 B APHA 2340 C APHA 2540B APHA 2540 D APHA 2540 C APHA 3111 D APHA 3120 B ASTM 3921 APHA 5520F



Page 7 of 37

WASTE WATER ANALYSIS TEST, UNIT Biochemical Oxygen Demand Biochemical Oxygen Demand Chemical Oxygen Demand Chemical Oxygen Demand Chemical Oxygen Demand Conductivity Dissolved Oxygen Dissolved Oxygen Metals ( Cu,Cd, Pb, Ni, Zn, Cr, Cu, Fe, Mn & Ag) Metals ( Cu,Cd, Pb, Ni, Zn, Cr, Cu, Fe, Mn & Ag) Metals ( Cu,Cd, Pb, Ni, Zn, Cr, Cu, Fe, Mn & Ag) Oil & Grease Oil & Grease Oil & Grease pH Total Suspended Solids Total Dissolved Solid


METHOD APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA

5210 D 5210 B 5220 B 5220 C 5220D 2510 B 4500 O G 4500 O C 3030 3111 3120 B 5520B 5520 C 5520 D

APHA 4500 H APHA 2540 D APHA 2540 C


+

Page 8 of 37

MICROBIOLOGICAL EXAMINATION TEST, UNIT

METHOD

IN WATER Heterotrophic Plate Count Total Coliforms Faecal Coliforms Faecal Streptococci Pseudomonas aeruginosa Salmonella Legionella Legionella Sulphate Reducing Bacteria (SRB)

APHA 9215 APHA 9222 APHA 9222 APHA 9230 APHA 9213 APHA 9260 APHA 9260 FDA-BAM APHA 9240

D B D C E D J D

IN SEAFOOD SAMPLE Total Bacterial Count Bacillus cereus Staphylococcus aureus Salmonella E.coli Vibrio parahaemolyticus Yeast and Molds IN NON SEA FOOD SAMPLE Total Bacterial Count Bacillus cereus Staphylococcus aureus Salmonella E.coli Yeast and Molds IN ICE CUBE SAMPLE pH Heterotrophic Plate Count Total Bacterial Count Total Coliforms Total Coliforms Faecal Coliforms Faecal Coliforms FROM SWAB SAMPLES Total Plate Count Faecal Coliforms Staphylococcus aureus


FDA-BAM FDA-BAM FDA-BAM FDA-BAM FDA-BAM FDA-BAM FDA-BAM FDA-BAM FDA-BAM FDA-BAM FDA-BAM FDA-BAM FDA-BAM APHA 4500 APHA 9215 FDA-BAM APHA 9222 FDA-BAM APHA 9222 FDA-BAM

H+ D B D

FDA-BAM FDA-BAM FDA-BAM


Page 9 of 37

NAPHTHA ANALYSIS TEST, UNIT Acidity, mgKOH/g Acidity, mgKOH/g Acidity, mgKOH/g o

API Gravity @ 60 F o API Gravity @ 60 F o API Gravity @ 60 F o API Gravity @ 60 F Appearance Arsenic, ppb Arsenic, ppb Arsenic, ppb Ash Content, % Wt. Ash Content, % Wt. B S & Water, % Vol Benzene Content, % Vol Carbon Disulphide Carbon Residue on 10 % bottom, % Wt Carbon Residue on 10 % bottom, % Wt Carbon Residue, % Wt. Carbon Residue, % Wt. Chloride, ppm Chloride, ppm Chloride, ppm Chloride, ppm Chloride, ppm Cloud Point, oC Cloud Point, oC Colour Colour Colour Saybolt Copper Corrosion Test Copper Corrosion Test Density, kg/L Density, kg/L Density, kg/L Distillation Distillation Distillation


METHOD ASTM D 664 ASTM D 974 IP 139 ASTM D 1298 ASTM D 287 ASTM D 4052 IP 365 Visual Cold Vapour UOP 296 UOP 387 ASTM D 482 IP 4 ASTM D 1796 & 2709 ASTM D 3606 ASTM D5623 ASTM D 189 IP 13 ASTM D 524 IP 14 ASTM D 4929 ASTM D 5194 UOP 395 UOP 588 UOP 779 ASTM D 2500 IP 219 ASTM D 1500 IP 196 ASTM D 156 ASTM D 130 IP 154 ASTM D 1298 IP 160 ASTM D 4052 ASTM D 1078 ASTM D 86 IP 123


Page 10 of 37

NAPHTHA ANALYSIS TEST, UNIT Doctor Test Flash Point, °C Hydrocarbon Types, % Vol. Hydrocarbon Types, % Vol. Hydrogen Sulphide Content, ppm Hydrogen Sulphide Content, ppm Hydrogen Sulphide Content, ppm Hydrogen Sulphide Content, ppm Hydrogen Sulphide on Vapour Space, ppm Lead Content, ppb Mercaptan Sulphur Content, ppm Mercaptan Sulphur Content, ppm Mercaptan Sulphur Content, ppm Mercaptan Sulphur Content, ppm Mercury, ppb Mercury, ppb Metals (Trace), ppm Metals Content, ppm Metals Content, ppm Micro Carbon Residue on 10% bottom, % Wt Micro Carbon Residue, % Wt MON MTBE (Oxygenates), % Vol Nitrogen (Basic), ppm Nitrogen (Total),ppm Nitrogen (Total),ppm Nitrogen Content, % wt. Oxygenates (Trace), ppm Wt PONA PONA Pour Point ,oC Pour Point ,oC R V P. @100 oF, psi R V P. @100 oF, psi Residue on Evaporation, mg/100ml RON Salt Content, ptb Salt Content, ptb Salt Content, ptb Geo-Chem Middle East

METHOD IP 30 ASTM D 93 FIA GC DHA ASTM D 5623 IP 103Method B Mobil MM 787 UOP 163 Drager IP 224 IP 104 ASTM D 3227 ASTM D 5623 IP 342 Cold Vapour UOP 938 UOP 391 AAS ICP ASTM D 4530 ASTM D 4530 ASTM D2700 ASTM D 4815 UOP 430 T ASTM D 4629 ASTM D 5762 ASTM D 3228 LOWOX -GC ASTM D 5443 G C DHA ASTM D 97 IP 15 ASTM D 323 IP 69 ASTM D 1353 ASTM D 2699 ASTM D 3230 IP 265 IP 77


Page 11 of 37

NAPHTHA ANALYSIS TEST, UNIT Saturates, Aromatics & Olefins Saturates, Aromatics & Olefins Sediment by Mem. Filtration, % Wt Sulphur Content species, ppm Sulphur Content, % Wt Sulphur Content, % Wt Sulphur Content, % Wt Viscosity Kinematic, cSt Water Content, % Vol Water Content, ppm Water Content, ppm Wax Content, % Wt


METHOD ASTM D IP 156 ASTM D ASTM D ASTM D ASTM D IP 107 ASTM D ASTM D ASTM D IP 356 UOP 46


1319 4807 5623 1266 4294 445 95 4377

Page 12 of 37

AVIATION FUEL ANALYSIS TEST, UNIT Appearance Acidity mgKOH/g Acidity mgKOH/g Aniline Gravity Product Aniline Gravity Product Bromine Number Bromine Index Burning Characteristics Calorific Value Gross BTU/lb Calorific Value Gross BTU/lb Calorific Value Gross BTU/lb Calorific Value Gross BTU/lb Calorific Value Nett BTU/lb Char Value Colour Saybolt Conductivity Test Conductivity Test Copper Content Mg/Kg Copper Corrosion Test Rating Copper Corrosion Test Rating Density, kg/L Density, kg/L Density, kg/L Distillation Distillation Doctor Test Doctor Test Existent Gum mg/100 ml Flash Point, °C Freeze Point, °C Freeze Point, °C Hydrogen Content, % Wt. Lead Content, g/US Gal Lead Content, mg/L @ 15 °C Lubricity JFTOT Mercaptan Sulphur Content, ppm


METHOD Visual ASTM D IP 354 ASTM D IP 2 IP 129 ASTM D ASTM D ASTM D ASTM D ASTM D IP 12 ASTM D ASTM D ASTM D ASTM D IP 274 IP 225 ASTM D IP 154 ASTM D IP 160 ASTM D ASTM D IP 123 ASTM D IP 30 ASTM D IP 170 ASTM D IP 16 ASTM D IP 270 IP 224 ASTM D ASTM D ASTM D


3242 611

2710 187 1405 4809 240 4868 187 156 2624

130 1298 4052 86 4952 381 2386 3343

5001 3241 3227

Page 13 of 37

AVIATION FUEL ANALYSIS TEST, UNIT

METHOD

Microbiological Contamination Microseparometer ( MSEP), rating Naphthalene Content, % Vol. Particle Count Particulate Contamination, mg/Ltr Particulate Matter mg/Ltr Particulate Matter mg/Ltr Perioxide Number, mg/Kg Saturates,Aromatics & Olefins Saturates,Aromatics & Olefins R.V.P @ 100 oF psi R.V.P @ 100 oF psi Silver Corrosion Test Rating Smoke Point, mm Smoke Point, mm Specific Energy, net MJ/kg Sulphide Content, ppm Sulphur Content, ppm Wt Sulphur Content, % mass Sulphur Content, % Wt.* Sulphur Content, % Wt.* Sulphur Content, % Wt.* Thermal Stability (JFTOT) Tube Deposit Rating ( Visual) o

2

Viscosity, Kinematic @ - 20 C, mm /s Viscosity, Kinematic @ - 20 oC, mm2 /s Water Content, ppm Water Content, ppm Water Content, ppm Water Content, ppm Water Reaction Test Rating Water Reaction Test Rating


IP 385 ASTM D 3948 ASTM D 1840 IP 564 ASTM D 5452 ASTM D 2276 IP 216 ASTM D 3703 ASTM D 1319 ASTM D 2159 ASTM D 323 IP 69 IP 227 ASTM D 1322 IP 57 ASTM D 3338 FED STD 791 B ASTM D 5453 ASTM D 4294 IP 107 ASTM D 1266 ASTM D 3120 ASTM D 3241 ASTM D 3241 ASTM D 445 IP 71 ASTM D 4928 IP 386 ASTM D 4377 IP 356 ASTM D 1094 IP 289


Page 14 of 37

GASOLINE ANALYSIS METHOD

TEST, UNIT Acidity, mgKOH/g Alcohol in Gasoline, % Vol. API Gravity Appearance Aromatics Content, %Wt Aromatics Content, %Wt Benzene Content, % Vol. Benzene Content, % Vol. Bromine Index Bromine Number Colour Copper Corrosion Test Rating Copper Corrosion Test Rating Density, kg/L Density, kg/L Density, kg/L Distillation Distillation Doctor Test Doctor Test Existent Gun, mg/100 ml Fuel bound Nitrogen, %wt Nitrogen, ppm Wt Nitrogen, ppm Wt Induction Period Mins. Lead o Lead Content g/L @ 15 C Lead Content, g/US Gall Lead Content, g/US Gall Lead Content, mg/US Gall Mercaptan Sulphur Content ppm Mercaptan Sulphur Content ppm Mercaptan Sulphur Content ppm MON MTBE, %Vol Odour Olefins, %vol Potential Gum, mg/100 ml


ASTM D 1093 ASTM D 4815 ASTM D 287 Visual ASTM D 1319 ASTM D 5580 ASTM D 3606 ASTM D D5580 ASTM D 2710 IP 129 VISUAL ASTM D 130 IP 154 ASTM D 1298 IP 160 ASTM D 4052 ASTM D 86 IP 123 IP 30 ASTM D 4952 ASTM D 381 ASTM D3228 ASTM D 4629 ASTM D 5762 ASTM D 525 UOP 350 IP 224 ASTM D 3341 ASTM D 3237 IP 270 ASTM D 3227 ASTM D 5623 IP 342 ASTM D 2700 ASTM D 4815 Olfactory ASTM D 6293 ASTM D 381


Page 15 of 37

GASOLINE ANALYSIS METHOD

TEST, UNIT TVP o

R.V.P @ 100 F psi o

ASTM D 5191 IP 69

R.V.P @ 100 F psi RON Sulphur, % mass ppm Sulphur, % Wt. *

ASTM D 323

Sulphur, ppm Wt Sulphur, %wt TV/L 20 ( Summer ) Vapour liquid Ratio * Washed gum, mg/100 ml

ASTM ASTM ASTM ASTM ASTM


ASTM D 2699 ASTM D 2622 ASTM D 1266 D D D D D


5453 4294 4814 2533 381

Page 16 of 37

BUNKER FUEL, DIESEL OIL & LONG RESIDUE TEST, UNIT Appearance Accelerated Stability Test (oxidation stability) Accelerated Stability Test Strong Acid Number mg KOH/g Strong Acid Number mg KOH/g o

Aniline Point, C Aniline Point, oC Aluminium, mg/kg Ash Content, % Wt. Ash Content, % Wt. Asphaltine Content, % Wt. Aniline Point on Distillate Fraction Aniline Point on Distillate Fraction B.S. & Water, % Vol. B.S. & Water, % Vol. Bromine Number Bromine Number Bromine Number on Distillate Fraction Bromine Number on Distillate Fraction Bromine Number on Distillate Fraction Calorific Value, BTU/Ib (MJ/Kg) Calorific Value, BTU/Ib (MJ/Kg) Calorific Value, BTU/Ib (MJ/Kg) Nett Calorific Value (Calc) Calorific Value CCS (Apparent Viscosity) C.C.A.I Cetane Index Cetane Index Cetane Index Cetane Number Cloud Point, oC Cloud Point, oC Cold Filter Plugging Point, oC Colour Colour Compatibility/Stability Test Rating


METHOD Visual ASTM D 2274 IP 388 ASTM D 974 ASTM D 664 ASTM D 611 IP 2 ASTM D5184 IP 4 ASTM D 482 IP 143 ASTM D 611 IP 2 ASTM D 1796 ASTM D 2701 IP 130 ASTM D 1159 IP 129 ASTM D 1159 IP 130 ASTM D 240 IP 12 CALCULATED ASTM D 4868 ISO 8217 ASTM D 5293 CALCULATED ASTM D 976 ASTM D 4737 IP 380 ASTM D 613 IP 219 ASTM D 2500 IP 309 ASTM D 1500 IP 196 ASTM D 4740


Page 17 of 37

BUNKER FUEL, DIESEL OIL & LONG RESIDUE TEST, UNIT Compatibility Test Rating, % Vol. Carbon Residue Carbon Residue Carbon Residue as 10% bottom, % Wt Carbon Residue as 10% bottom, % Wt Copper Corrosion Test Rating Copper Corrosion Test Rating Density, Kg/L (For F.O - Bunkers) Density, Kg/L (For F.O - Bunkers) Density, Kg/L Distillation, oC Distillation, oC Distillation, oC Explositivity Flocculation Ratio as Xylene % v/v Flash Point, oC Flash Point, oC Furfuraldehyde Hydrogen Content * Lubricity Metals, ppm Metals Microbiological Analysis Nitrogen Content, ppm Wt. Nitrogen Content, ppm Wt. Nitrogen Content, % Wt. Particle count/100 ml Particulate Matter, mg/Ltr Particulate Matter, mg/Ltr Poly Aromatic hydrocarbon (PAH) Pour Point, oC Pour Point, oC Peptisation Test p Value Ramsbottom Carbon Residue, % Ramsbottom Carbon Residue, % Ramsbottom Carbon Residue on Ramsbottom Carbon Residue on Sediment by Extraction, % Wt. Sediment by Extraction, % Wt. Geo-Chem Middle East

Wt. Wt. 10% bottom,%wt 10% bottom,%wt

METHOD MOBIL ASTM D 189 IP 13 ASTM D 189 IP 13 ASTM D 130 IP 154 ASTM D 1298 IP 160 ASTM D 4052 ASTM D 86 ASTM D 1160 IP 123 SCDSTD791B SMS 305 FRS ASTM D 93 IP 34 IP 297 ASTM D 3178 ASTM D 6069 ASTM D 5863b ASTM D 3605 IP 385 ASTM D 4629 ASTM D 5762 ASTM D 3228 ISO 4406 ASTM D 6217 IP 440 IP 391 ASTM D 97 IP 15 TOTAL 631 LORI SMS 1600 ASTM D 524 IP 14 ASTM D 524 IP 14 ASTM D 473 IP 53


Page 18 of 37

BUNKER FUEL, DIESEL OIL & LONG RESIDUE TEST, UNIT Sediment by Hot Filtration, % Wt. Silicon, mg/kg Silicon, mg/kg Calcium, mg/kg Calcium, mg/kg Zinc, mg/kg Zinc, mg/kg Phosphorus, mg/kg Phosphorus, mg/kg Specific Gravity @ 60/60 oF Specific Gravity @ 60/60 oF Specific Gravity @ 60/60 oF Sulphur Content, % Wt. Sulphur Content, % Wt. Sulphur Content, ppm Wt. Sulphur Content, % Wt. Toluene Equivalence Total Sediment, % Wt. Total Sediment, % Wt. Total Sediment, % Wt. Total Sediment after Aging, % Wt Total Solids, mg/100ml Viscosity, Kinematic, mm 2 /s Viscosity, Kinematic, mm 2 /s Vanadium, ppm Water Content, % Vol. Water Content, % Vol. Wax Content, % Vol. Xylene Equivalent


METHOD SMS 2696 ASTM D 5184 IP 377 ASTM D 5184 IP 377 ASTM D 5184 IP 377 ASTM D 5184 IP 377 ASTM D 1298 IP 160 ASTM D 4052 ASTM D 4294 IP 336 ASTM D 5453 ASTM D 129 EXXON 79-004 ASTM D 4870 UOP 413 IP 375 IP 390 ASTM D 2276 ASTM D 445 ASTM D IP 7 ASTM D 5863 ASTM D 95 IP 74 UOP 46 BP 230


Page 19 of 37

ASPHALT & BITUMEN ANALYSIS TEST, UNIT Cement Mixing Distillation Distillation o

Ductility cm @ 25 C, cm Ductility cm @ 25 oC, cm o Flash Point, C Flash Point, oC Foam on heating o

Flash Point, C Mixing & compaction temperature Mixing & compaction temperature Penetration mm x 10 (-1) Penetration mm x 10 (-1) Penetration Index Particle Charge Particle Charge Rubber content Saybolt Furol, sfs Saybolt Furol Viscosity @ 25 oC Sieve Test Sieve Test Softening Point C/ F Softening Point C/ F Softening Point C/ F Solubility, % Wt. Solubility, % Wt. Storage Stability Storage Stability Specific Gravity @ 60/60 oF Specific Gravity @ 60/60 oF Specific Gravity @ 60/60 oF Spot Test Thin Film Oven Test/L.O.H. % Wt. Thin Film Oven Test/L.O.H. % Wt. Viscosity, Kinematic, cSt Viscosity, Kinematic, cSt Vacuum viscosity, Pa.S Water Content, % Vol. Water Content, % Vol. Wax Content, % Wt. Wax Content, % Wt


METHOD ASTM D 6935 AASHTO T 78 ASTM D 402 AASHTO T 51 ASTM D 113 T 79 ASTM D 92 Visual IP 136 ASTM D 2493 ASTM D341 AASHTO T 49 ASTM D 5 Calculation ASTM D 244 AASHTO T 59 DM 500 ASTM D88 AASHTO T 72 AASHTO T 59 ASTM D 244 T 53 ASTM D 36 IP 58 AASHTO T 44 ASTM D 2042 AASHTO T 59 ASTM D 244 ASTM D 1298 AASHTO T 228 ASTM D 70 AASHTO T 102 AASHTO T 179 ASTM D 1754 AASHTO T 201 ASTM D 2170 ASTM D 2171 AASHTO T 55 ASTM D 95 DIN 52015 UOP 46


Page 20 of 37

LUBRICANT ANALYSIS TEST, UNIT Acid Number, mgKOH/g Acid Number, mgKOH/g Air Release Appearance Ash – Sulphated, % Wt. Ash – Sulphated, % Wt. Ash Content, % Wt Ash Content, % Wt. Bacteria Base Number, mgKOH/g Base Number, mgKOH/g Carbon Residue, % Wt. Carbon Residue, % Wt. Cloud Point, oC Cloud Point, oC Cold Cranking, oC * Colour Colour Conradson Carbon Residue, % Wt. Conradson Carbon Residue, % Wt. Demulsibility Test Density @ 15 °C, Kg/Ltr Density @ 15 oC Kg/ Ltr Density, kg/L Dissipation factor /TAN DELTA * DMSO Extract Emulsion Characteristics Fire Point Flash Point, oC Flash Point, oC Flash Point, oC Foaming Characteristics Foaming Characteristics Free Chloride, ppm Filterability Fuel Dilution Fuel Dilution Test (Gasoline) Fuel Dilution Test (Gasoline) Full Scan (13 Elements)


METHOD ASTM D 664 ASTM D 974 IP 313 Visual ASTM D 874 IP 163 ASTM D 482 IP 4 TEST KIT ASTM D 2896 IP 276 ASTM D 189 IP 13 ASTM D 2500 IP 219 ASTM D 5293 ASTM D 1500 IP 196 ASTM D 187 IP 13 ASTM D 2711 ASTM D 1298 IP 160 ASTM D 4052 BS 5737 IP 346 ASTM D 1401 ASTM D 92 IP 36 ASTM D 93 IP 34 ASTM D 892 IP 146 Argentometry ISO 13357-2 FTIR ASTM D 322, IP 23 IP 23 AAS


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LUBRICANT ANALYSIS TEST, UNIT Full Scan (13 Elements) Full Scan (21 Elements) Full Scan (21 Elements) Glycol Content, % Vol. Insolubles (Pentane), % Wt. Insolubles (Toluene), % Wt. Metals Additive, %wt Metals Additive, %wt Microbiological Contamination Nitrogen Content, % Wt. Oxidation / Nitration Oxidation Characteristics Oxidation Stability Particle Count + Sizing (microns) Particulate Matter, mg/100 ml Particulate Matter, mg/100 ml Phophrous, % Wt Phosphorous Content, % Wt. Phosphorous Content, % Wt. Pour Point, oC Pour Point, oC PQ Index Rotating pressure vessel oxidation test (RPVOT) Rust Prevention Characteristics Rust Prevention Characteristics Sediments, %Vol Sulphur Content, % Wt. Sulphur Content, % Wt. Sulphur, % mass Total Solids, % Wt. Total Solids, %wt Varnish Potential Patch Test Viscosity Index Viscosity Kinematic, cSt Viscosity Kinematic, cSt Viscosity, Kinematic, cSt Water Content, % Vol. Water Content, ppm


METHOD ASTM D 5185 AAS ASTM D 5185 FT IR ASTM D 893 ASTM D 893 ASTM D 4628 ASTM D 4951 TEST KIT ASTM D 3228 FT IR ASTM D 943 IP 280 AS – 4059/ ISO 4406 ASTM D 2276 IP 216 ASTM D 4951 ASTM D 1091 ASTM D 4047 ASTM D 97 IP 15 PQ Analyzer ASTM D 2272 ASTM D 655 IP 135 ASTM D 2273 ASTM D 129 ASTM D 4294 ASTM D 129 IP 316 ASTM D 2274 ASTM C.02 ASTM C.02 ASTM D2270 ASTM D 445 ASTM D 7042 IP 71 ASTM D 95 ASTM D 6304


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GREASE ANALYSIS TEST, UNIT Alkalinity Appearance Consistency Complete Analysis o

Drop Point C o Drop Point C Evaporation Loss % Wt.* Oil Content Oil Separation % Wt.* Penetration ( Unworked) Penetration ( Unworked) Penetration (Worked) 10,000 Strokes Penetration (Worked) 10,000 Strokes Penetration (Worked) 60 Strokes Penetration (Worked) 60 Strokes Soap Content


METHOD ASTM D Visual ASTM D ASTM D ASTM D IP 132 ASTM D ASTM D ASTM D ASTM D IP 58 ASTM D IP 58 ASTM D IP 58 ASTM D


974 217 128 566 972 128 1742 217 217 217 128

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BASE OIL ANALYSIS TEST, UNIT Appearance Ash Content Ash Content Carbon Residue Carbon Residue Colour Colour Demulsibility Pour Point Pour Point Rust prevention characteristics Viscosity Index Viscosity, Kinematic cSt Viscosity, Kinematic cSt Viscosity, Kinematic cSt Water , ppm Water , ppm Water content %wt Water Separability, mins


METHOD Visual ASTM D 482 IP 4 ASTM D 189 IP 13 ASTM D 1500 IP 196 IP 19/1997 ASTM D 97 IP 15 ASTM D655 ASTM D 2270 ASTM D 445 ASTM D 7042 IP 71 ASTM D 1123B ASTM D 6304 ASTM D 6308 ASTM D 1401


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TRANSFORMER OIL ANALYSIS TEST, UNIT Appearance Breakdown Voltage Colour Copper Content Corrosive Sulphur Density @ 15 °C kg/Ltr o

Dissipation Factor @ 90 C Flash Point Furan Analysis Furan Analysis Induction period @120°C (Oxidation Stability) Inhibitor Content, % Wt Interfacial tension Neutralization value Particle Count/100 ml Particle Count/100 ml PCA PCB Content Pour Point °C o

Resistivity @ 90 C Sulphur Content Sludge Viscosity, Kinematic cSt Wear Metals Water Content Water Content

Dissolved Gas Analysis Dissolved Gas Analysis


METHOD Visual IEC 60156 ASTM D 1500 ICP ASTM D 1275 BS 148 IEC 60247 ASTM D 93 IEC 61198 ASTM D 5837 IEC 601125 b IEC 60666 ASTM D 971 ASTM D 974 ISO 4406 AS 4059 IP 348 IEC 61619 ASTM D97 ASTM D 1169 ASTM D 4294 ASTM D 1698 ASTM D445 ASTM D 5185 ASTM D 1533 IEC 60814

ASTM D 3612 IEC 60567


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PETROCHEMICALS, SOLVENTS & AROMATICS TEST, UNIT Acetone Content % Vol. Acid Acceptance Test Acidity Acidity as Acetic Acid % Wt. Acid Wash Colour Aldehyde Content % Wt. Aldehyde Content % Wt. Aldehyde Content % Wt. Aldehyde Content % Wt. Alkalinity as NH3 % Wt. Alkalinity & oil content, % mass Apperance Arsenic Ash Content % Wt. Aromatic content %Vol Bromine Number Bromine Index Carbonisable Substances Test Chloride Content ppm Chloride Content % Wt. Colour (Hazen) Colour (Saybolt) Copper Corrosion Test Copper Corrosion Test Density Kg/Ltr Distillation °C Distillation °C Doctor Test Ester Value Ethyl Benzene Flash Point °C Flash Point °C Flash Point °C Flash Point °C * Gas Chromatograph Analysis % Vol., %Wt Heptane Miscibility Test Hydroxyl Number mgKOH/gm Hydroxyl Number mgKOH/gm


METHOD ASTM D 1612 ASTM D 2106 Qualitative ASTM D 1613 ASTM D 848 BS 506 ASTM D 2119 ASTM D 2192 ASTM D 329 ASTM D 1614 ASTM D 128 Visual AAS cold vapour ASTM D 482 ASTM D 3257 IP 129 D 2710 ASTM E 346 Turbidimetry UOP 779 ASTM D 1209 ASTM D 156 ASTM D 130 ASTM D 849 ASTM D 4052 ASTM D 850 ASTM D 1078 ASTM D 4952 ASTM D 1617 GC IP 170 ASTM D 92 ASTM D 93 ASTM D 56 GC ASTM D 1476 ASTM D 1957 ASTM D 4274


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PETROCHEMICALS, SOLVENTS & AROMATICS TEST, UNIT Hydroxyl Number mgKOH/gm Hydrocarbons in Alcohols ppm Inhibitor Content , ppm Inhibitor Content , ppm Iron Content ppm Lead Content ppb Glycol Content Metals ppm Metals ppb Non Volatile Matter mg/100 mls Non aromatics Odour Oxidation Stability Mins Permanganate Time Mins Peroxide Content ppm PH Value Polymer Content , ppm Purity of glycols, %m/m Purity, %wt Residual Odour Residue on Evaporation % Wt. Refractive Index @ 20 °C * Saponification Value mgKOH/gm Saponification Value mgKOH/gm Solid content, %wt Solidification Point °C Solubility Specific Gravity @ 60/60 °F Total Sulphur ppm Total Sulphur ppm Thiophene & Carbon di Sulphide UV Transmittance Test Viscosity, Kinematic cSt Water Content %wt, Water Content ppm Water Content %wt, Water Content %wt, Water miscibility


METHOD SMS2116 BS 506 ASTM D 3125 ASTM D 4590 AAS, ICP IP 224 MIL-1-85470(AS) AAS/ICP UV Spectroscopy ASTM D 1353 ASTM D 2360 Sensory Evaluation ASTM D 525 ASTM D 1363 ASTM D 2340 Meter ASTM D 2121 ASTM E202 GC ASTM D 1296 ASTM D 1353 ASTM D 1218 IP 136 ASTM D 94 FTIR shell method ASTM D 852 ASTM D 1722 ASTM D 4052 ASTM D 3120 ASTM D 5453 ASTM D 5623 UV Spectroscopy ASTM D 445, IP 71 ASTM D 1364 ASTM E 1064 ASTM E 203 ASTM E 1062 ASTM D 1722


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GAS ANALYSIS LIQUIFIED PETROLEUM GASES / NATURAL GAS TEST, UNIT

METHOD

Component Analysis % Vol, Composition upto c6+, %mol Composition upto C14+, % mol Composition upto C30+, % mol (stabilised) Composition upto C36+, % mol Composition upto C30+, % mol (pressured) Copper Corrosion Test Cp Specific Heat @60°F, BTU/lb Evaporation Temp. F (95%) Evaporation Temp. F (95%) Gross Heat Value, BTU/[email protected]°F Gross Heat Value, BTU/[email protected]°F Hydrogen Sulphide ppm Hydrogen Sulphide ppm Hydrogen Sulphide ppm Liquified Petroleum Gases and Propane Concentration Mercaptan Sulphur ppm Mercaptan Sulphur ppm Mercury Molecular weight Molecular weight Moisture Test Moisture Test Net Heat Value, BTU/[email protected]°F Net Heat Value, BTU/[email protected]°F Oil Stain Test Oil Stain Test R.V.P. @) 100 °F Psig Specific Gravity @ 60/60 °F Specific Gravity, air=1 Specific Gravity, air=1 Sulphur Content ppm Sulphur Content ppm Total Sulphur Volatile Residue Water, ppm

Shaw moisture meter (ASTM D5454)

Wobbe Index Wobbe Index BTX analysis, % vol

ISO 6976 calculated GPA 2172 GPA 2286


GC ASTM D1945 ASTM D1945 GC GC GC ASTM D 1838 Calculated ASTM D 2158 IP 317 ISO 6976 calculated GPA 2172 UOP 403 ASTM D 5504 ASTM D 4810 (Dragger) ASTM D 2163 UOP 403 ASTM D 5623 ISO 6958 Calculation, ASTM D 3588 ASTM D 2713 IP 395 ISO 6976 calculated GPA 2172 ASTM D 2158 IP 317 ASTM D 1267 ASTM D 1070 ISO 6976 calculated GPA 2172 ASTM D 5504 ASTM D 6667 ASTM D3246 ASTM 1837


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FERTILIZER ANALYSIS TEST, UNIT Biuret Content Chloride Content Magnesium Chloride Moisture Content Nitrogen Content Nitrogen (Ammoniacal) Phosphorous Phosphorous (Citrate Soluble) Phosphorous (Water Soluble) Potassium Oxide Sodium Content Sodium Chloride Sieve Test Urea Content


METHOD AOAC, 2.088 IS2764 AAS AOAC 2.056 AOAC 2.056 KJELDAHL AOAC 2.020 AOAC 2.044 AOAC 2.040 AOAC 2.119 AOAC 2.178 AAS AOAC AOAC


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FIRE FIGHTING FOAM ANALYSIS TEST, UNIT Appearance Density @20°C, kg/L 25% drainage time(3% blend), min Expansion Coefficient Foam Concentration pH Value (30% Blend) pH Value (Neat) Purity %vol Sedimentation Value % Vol. o

Specific Gravity @ 60/60 F Specific Gravity @ 60/60 oF Stability Test Viscosity, Kinematic cSt Viscosity, Kinematic cSt


METHOD Visual ASTM D 4052 Volumetric Volumetric Refractometer Meter Meter GC ASTM D 2709 ASTM D 4052 ASTM D 1298 Volumetric ASTM D 445 IP 71


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FOOD ANALYSIS TEST, UNIT Acid Value Acid Value Amine value Amine value Amine value Ash Insoluble in dil.HCl Colour * Ethyl Alcohol content Foreign matter Gluten * Hydroxyl value Iodine value. Melting Point Metals (Cu, Cr, Fe & Ni) Moisture Moisture Peroxide value Phosphorous Refractive index * Residue on Evaporation Saponification value Saponification value Total Ash Total Protein * Volatile acids as acetic acid Weeviled grains


METHOD AOAC Da 14-48 AOAC Te 1a-64 AOAC Tf 2b-64 AOAC Tf 1b-64 AOAC Tf 3b-64 AOAC 941.12 AOAC Tb-64 AOAC 926.03 AOAC 971.32 AOAC 38.12 AOAC Cd 4-40 AOAC Cd 1-25 AOAC Cc1-25 AOCS Ca 15 AOAC 925.10 AOAC CaZe – 84 AOCS cd 8 – 53 AOCS Ja 5-55,Ca 12-55 AOCS Cc-7-25 AOAC 940.09 AOAC Cd 3c 1-25 AOAC T1 1a-64 AOAC 941.12 AOAC 920.87 AOAC 940.15 AOAC 977.16


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COOLANT ANALYSIS TEST, UNIT Reserve Alkalinity, ml Chloride Glycol Content, %wt Equilibrium boiling point Water Content Freezing Point Foaming pH

METHOD ASTM D1121 ASTM D 5827 GC ASTM D 1120 E 203 ASTM D 2386 ASTM D 1881

ASTM D 1287

DETERGENT ANALYSIS TEST, UNIT Moisture, %Wt

METHOD SASO/ gulf std.

HALON ANALYSIS TEST, UNIT Purity (Exclusive of N2), mol% Acidity, ppm/mass Water content, ppm/mass Non Volatile reside, %m/m Halogen Ion, Suspended matter or sediment,


METHOD ASTM ASTM ASTM ASTM ASTM ASTM

D D D D D D


5632 5632 5632 5632 5632 5632

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TEA ANALYSIS TEST, UNIT Moisture Content, %wt/wt Water Extract, %wt/wt Total Ash % by mass Ash soluble in Water, % of total ash Acid insoluble ash Alkalinity of water soluble ash Crude Fibre Dust % Metal magnetic impurities Lead, mg.Kg

METHOD SSA SSA SSA SSA SSA SSA SSA SSA SSA ICP

274 274 274 274 274 274 274 274 274

SUGAR ANALYSIS TEST, UNIT Colour Polarization,OZ Moisture, %Wt Ash content, %wt Invertase in Sugar


METHOD SASO SASO SASO SASO SASO

276 276 276 276 276


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AMBIENT AIR QUALITY/ INDOOR AIR QUALITY / NOISE MONITORING Description Method (1) AMBIENT AIR QUALITY MONITORING BY MOBILE STATION Respirable Dust (PM10)

EPA-EQPM 0798-122

Sulphur dioxide, SO2 Hydrogen Sulphide, H2S

EPA RFCA 0193-092 UV-FLUORESCENCE

Oxides of Nitrogen, NOx

EPA RFNA 1292-090

Carbon monoxide, CO

EPA RFCA 09923-088

Ozone, O3

EPA EQOA 0193-091

Methane & Non Methane Hydrocarbon Meteorological Data: Atmospheric Temperature, Relative Humidity, Wind Speed, Wind Direction,

FID GC Meteorological Sensor

Note 1: The foregoing tests are conducted by the analyzers mounted in a mobile vehicle

(2) INDOOR AIR QUALITY MONITORING Respirable Dust (PM10) Total Suspended Particles, TSP Sulphur dioxide, SO2 Oxides of Nitrogen, NOx Carbon monoxide, CO

Cyclonic Flow

Total Volatile Organic Compounds, VOC's

PID

West & Gaeke Sodium Arsenite Electro Chemical Sensor

Note 2:The above suggested parameters and test methods can be applied on short- term ambient air quality monitoring.

(3) NOISE MONITORING AMBIENT & INDUSTRIAL NOISE MONITORING


SOUND LEVEL METER


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STACK /FLUE GAS MONITORING

Reporting Parameters

Test Method

Average flue gas temperature Average meter temp

USEPA -2 USEPA -2

Flue or Stack gas pressure Volume of metered gas Total volume of condensate (Filter and probe wash) Pitot tube correction factor Average stack gas velocity Average pressure differential across orfice meter Diameter of sampling nozzle used Diameter of the stack Cross sectional area of stack Area of nozzle used Meter calibration factor Y Elapsed time of test CO2

USEPA -5 USEPA -5

O2 Total particulate matter SO2

ELECTRO CHEMICAL SENSOR

NO2 CO Stack height Load of the unit during test

USEPA -7

Fuel Consumption during the test run Iso Kinetic rate for the sampling run

-USEPA -5


USEPA -4 -USEPA -2 USEPA -2 USEPA -5 -USEPA -5 USEPA -5 -USEPA -5 ELECTRO CHEMICAL SENSOR

USEPA - 5 USEPA -6 & 8

ELECTRO CHEMICAL SENSOR ---


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MISCELLANEOUS ANALYSIS TEST

METHOD

Cereals Pulses & Spices Full Physical Analysis Cement

Visual/GRAVIMETRY

Full Chemical Analysis Lime Stone

ASTM C 114

Full Chemical Analysis Sulphur

ASTM C 25

Full Chemical Analysis (Excluding Teliurium, Selenium, Arsenic)

B.S. 4113



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CALIBRATION Calibration Field

Calibrator

Range & Specification

Best Capability

Temperature Liquid in Glass Thermometer

Fluke 9170 Fluke 9173

-45° C to + 140° C +50° C to + 700° C

±0. 1°C ±0. 15°C

Digital Thermometer Fluke 9170

-45° C to + 140° C

±0. 1°C

Fluke 9173

+50° C to + 700° C

±0. 15°C

Infra Red Thermometer

Fluke 9132

+50° C to + 500° C

±0. 65°C

Test Method used : BS 5074 : 1974

Pressure Hydraulic pressure Gauge/module

DH-Budenberg 580EHX

Pneumatic pressure DH-Budenberg Gauge/module PPS42

1 to 1400bar Dead Weights)

(

0 to 40bar (pressure Module)

0.025% of reading 0.025% of reading

Test Method used : BS EN 60051-1: 1999

Weighing Balance

Mettler Toledo Class - F 1 Test Method used : OIML R111-1: 2004

Weight Sets 1 mg to 20 kg

0.02% of reading

Reference Thermometer Temperature indicator

Fluke 1523

PRT: -200°C to +1000°C Thermocouple: 200°C to + 2315°C Precision Thermistors: 50°C to + 150° C

±0. 011°C ±0. 24°C for j,k,l,m ±0. 002°C

Test Method used : BS 5074: 1974 Total Station Storage Tanks Leica n/a Test Method used : EODR & API MPMS Chapter 2.2 A & 2.2 B



0.005% of reading

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