Reaction Attempts

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May 4, 2010 - solvent, concentration of limiting reactant, appearance of a precipitate, yield, etc.). The two sheets are connected via the use of a common ...

Reaction Attempts Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

The UsefulChem Project

Compiled and Performed by: Jean-Claude Bradley, Khalid Mirza, and Andrew Lang with Tim Bohinski, David Bulger, Alicia Merchant, Emily Messner, Marshall Moritz, Shannon Oseback, Rikesh Parikh, Mitesh Shah

Version: April 28, 2010 Licensed under a Creative Commons Attribution 2.5 License Data is available as CC0

1

Preface Reaction Attempts First Edition Data Source: the UsefulChem project Introduction Open Notebook Science (ONS) refers to the practice of making the full contents of a laboratory notebook and all associated raw data files available in near real time.[1] This represents an opportunity for everyone to benefit from work in progress in an open research group. However, in order to make use of the information, it must be easily discoverable. A simple strategy to increase discoverability is redundancy over multiple communication platforms. In another project - the Open Notebook Science Solubility Challenge[2] - we published non-aqueous solubility data in the form of physical and downloadable (PDF) books.[3] Although it is possible to search the solubility database using web query interfaces, exploration of a Google Spreadsheet, an XML feed, etc.[4], having a physical copy in the laboratory has proved to be very convenient in several instances. A similar format for reactions will also be useful.

The UsefulChem Project

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

UsefulChem started in 2005 as an organic chemistry Open Notebook Science project with a main goal of discovering new anti-malarial agents that can be prepared by simple and cheap syntheses.[5] Most of the reactions on UsefuChem are Ugi reactions, which involve the mixing of an amine, aldehyde, carboxylic acid and isonitrile in a solvent at room temperature generally for a few hours to days.[6] The multicomponent design of the Ugi reaction and the simple reaction conditions make it ideal for exploring large virtual libraries and selecting compounds of interest to make.[7] Isolation of the Ugi products can be immensely simpler, cheaper and readily scalable if they precipitate in pure form from the reaction mixture. To this end, much of the research in the UsefulChem project focuses on reaction conditions that lead to this outcome.[8] This is in fact the origin of the ONS Solubility Challenge discussed above.[9]

The Reaction Attempts Database In order to look for patterns in the reaction conditions which led to Ugi product precipitation, the CombiUgiResults Google Spreadsheet was set up.[10] Reactions indexed there can be sorted by precipitation outcome, solvent, reactant, concentration, etc. and links to the laboratory notebook pages can be followed for full details. However, this sheet is designed specifically for Ugi reactions and contains columns specifically for the aldehyde, amine, carboxylic acid and isonitrile. In order to enable the tracking of other types of reactions, the information in the CombiUgiResults sheet was reformatted into two other sheets: ReactionAttempts[11] (containing reagents and reactants) and RXIDsReactionAttempts[12] (containing reaction conditions and results, such as solvent, concentration of limiting reactant, appearance of a precipitate, yield, etc.). The two sheets are connected via the use of a common ReactionID. This format permits the representation of any type of reaction, with an unlimited number of reactants and products.[13] By definition, any Open Notebook Science project in a work in progress. The listing of a reaction in this database only means that the researcher attempted or is in the process of attempting it. Whatever the situation, a link to the laboratory notebook page is provided, where the most recent information is available. The philosophy used here is that partial information is always better than no information at all. Thus a researcher investigating the prior use a particular reactant in a Ugi reaction might find the report that a precipitate was obtained in methanol helpful for designing their own reactions, even if the characterization of the precipitate is still pending. At the very least, knowing that a certain researcher has at least attempted a similar reaction is enough information for initiating a discussion, which may lead to valuable insights.

Reaction Attempts on Chemspider Although SMILES[14] are provided in the spreadsheets, the primary key to identify compounds is the ChemSpider ID (CSID)[15]. This allows us to render molecule images in the book automatically. In the case of the ONS Solubility Challenge book[3], use of the CSID enables a convenient way to calculate various descriptors for displaying values in the book. In addition, the compounds in the Reaction Attempts database are indexed on ChemSpider as two Data Sources: ReactantsAttemptedReactions and ProductsAttemptedReactions[13]. In this way a substructure search for either reactants or products will identify indexed molecules. Clicking on the Syntheses tab in the ChemSpider record for a selected molecule will then reveal a list of hyperlinks to the relevant laboratory notebook pages.

Organization of the Book In keeping with the layout of the ONS Solubility Challenge Book, the reactants are listed in alphabetical order. Each entry displays the list of reactions where the reactant was used. This includes a scheme with all reactants and product as well as key metadata: the researcher, reaction type, solvent, limiting reactant concentration, observation of a precipitate, comments and a reference (links to the laboratory notebook page). In this edition, only Ugi reactions are included. The reaction schemes are laid out in the following order: carboxylic acid, amine, aldehyde and isonitrile. This should allow for easy comparison between schemes within a given record. Reactions where the Ugi product was isolated and characterized are marked with a green check and the percent yield is noted. Since the Ugi products do not have simple common names, they are not included as separate entries. However, all reactions where the synthesis of a specific Ugi product was attempted can be found by looking up the entries for any of the four reactants. Although this compilation is not exhaustive, it does cover the vast majority of reactions in the UsefulChem project to date. Future editions will include other reactions from UsefulChem and other sources.

Archive This edition is linked to the UsefulChem interactive data archive (ZIP)[16], (DVD)[17], ReactionAttempts (XLS)[18] and RXIDsReactionAttempts(XLS)[19] taken on 2010-04-27.

References 1. Open Notebook Science Wikipedia Entry http://en.wikipedia.org/wiki/Open_Notebook_Science 2. Open Notebook Science Solubility Challenge Wiki http://onschallenge.wikispaces.com 3. Bradley, J.-C. First Edition of ONS Solubility Challenge Book UsefulChem Blog (2009)

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Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

http://usefulchem.blogspot.com/2009/12/first-edition-of-ons-solubility.html 4. Open Notebook Science Solubility Challenge List of Experiments page http://onschallenge.wikispaces.com/list+of+experiments 5. UsefulChem Wiki http://usefulchem.wikispaces.com 6. Ugi Reaction Wikipedia Entry http://en.wikipedia.org/wiki/Ugi_reaction 7. Dömling, A., & Ugi, I. (2000). Multicomponent Reactions with Isocyanides. Angewandte Chemie International English Edition, 39(18), 3168-3210. doi: 10.1002/1521-3773(20000915)39:183.0.CO;2-U. 8. UsefulChem List of Experiments http://usefulchem.wikispaces.com/All+Reactions 9. Bradley, J.-C. Open Notebook Science Challenge UsefulChem Blog (2008) http://usefulchem.blogspot.com/2008/09/open-notebook-science-challenge.html 10. CombiUgiResults Google Spreadsheet http://spreadsheets.google.com/ccc?key=plwwufp30hfpUERhse9y5Kw 11. ReactionAttempts Google Spreadsheet http://spreadsheets.google.com/ccc?key=0Ak1R8T6wt4YQdG9NejNLcDNUMkVBVURGM01TR0NxdXc 12. RXIDsReactionAttempts Google Spreadsheet http://spreadsheets.google.com/ccc?key=0Ak1R8T6wt4YQdGVENVFMWjdzaGd2REJTTnA4RG5vblE 13. Bradley, J.-C. Reaction Attempts on ChemSpider UsefulChem Blog (2010) http://usefulchem.blogspot.com/2010/03/reaction-attempts-on-chemspider.html 14. SMILES Wikipedia Entry http://en.wikipedia.org/wiki/Simplified_molecular_input_line_entry_specification 15. ChemSpider Web Site http://www.chemspider.com/ 16. UC archive Drexel server (ZIP) http://showme.physics.drexel.edu/usefulchem/archives/usefulchem2010-04-27.zip 17. UC archive on lulu.com (DVD) http://www.lulu.com/product/dvd/usefulchem-archive/10791847 18. Bradley, J.-C.; Lang, A.. Reaction Attempts Reactants and Products. UsefulChem. 2010-04-27. URL:http://spreadsheets.google.com/pub?key=toMz3Kp3T2EAUDF3MSGCquw&output=xls. Accessed: 2010-04-27. (Archived by WebCite® at http://www.webcitation.org/5pIsFEbT9) 19. Bradley, J.-C.; Lang, A.. Reaction Attempts RXIDs. UsefulChem. 2010-04-27. URL:http://spreadsheets.google.com/pub?key=teD5QLZ7shgvDBSNp8DnonQ&output=xls. Accessed: 2010-04-27. (Archived by WebCite® at http://www.webcitation.org/5pIs2eh62)

Reactions 1-aminocyclohexane-1-carboxylic acid Reaction ID UCEXP233-1 Researcher David Bulger Reaction Type Ugi Solvent methanol Limiting Reactant 0.921 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp233

+

1-aminocyclohexane-1carboxylic acid

+

benzylamine

+

3,5-dimethoxybenzaldehyde



t-butyl isocyanide

24534439

Reaction ID UCEXP233-2 Researcher David Bulger Reaction Type Ugi Solvent methanol Limiting Reactant 0.92 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp233

+

1-aminocyclohexane-1carboxylic acid

+

benzylamine

+

3,5-dimethoxybenzaldehyde

Reaction ID UCEXP233-7 Researcher David Bulger Reaction Type Ugi Solvent methanol Limiting Reactant 1.02 M Precipitate No Comments -

3



cyclohexylisocyanide

24534440

Reference

http://usefulchem.wikispaces.com/Exp233

+

1-aminocyclohexane-1carboxylic acid

+

benzylamine

+

3,5-dimethoxybenzaldehyde



t-butyl isocyanide

24534439

Reaction ID UCEXP233-8

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Researcher David Bulger Reaction Type Ugi Solvent methanol Limiting Reactant 1.018 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp233

+

1-aminocyclohexane-1carboxylic acid

+

benzylamine

+

3,5-dimethoxybenzaldehyde



cyclohexylisocyanide

24534440

1-heptylamine Reaction ID UCEXP131-4 Researcher Rikesh Parikh Reaction Type Ugi Solvent methanol Limiting Reactant 0.612 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp131

+

Boc-Trp-OH

+

1-heptylamine

+

o-vanillin



benzyl isocyanide

21106061

Reaction ID UCEXP131-8 Researcher Rikesh Parikh Reaction Type Ugi Solvent methanol Limiting Reactant 0.618 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp131

+

Boc-Trp-OH

+

1-heptylamine

+

o-vanillin

Reaction ID UCEXP131-9 Researcher Reaction Type Solvent

Rikesh Parikh Ugi methanol

4



n-butyl isocyanide

21106065

Limiting Reactant 0.61 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp131

+

Boc-Trp-OH

+

+

1-heptylamine

o-vanillin



1-pentyl isocyanide

21106066

Reaction ID UCEXP148A-V1B153

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Researcher Khalid Mirza/ Emily Messner Reaction Type Ugi Solvent methanol Limiting Reactant 0.398 M Precipitate Yes but the aldehyde alone is not soluble in methanol Yield 50.1 % Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp148

+

crotonic acid

+

1-heptylamine

+

phenanthrene-9-carboxaldehyde



t-butyl isocyanide

21106058

Reaction ID UCEXP180 Researcher Shannon Oseback Reaction Type Ugi Solvent methanol Limiting Reactant 0.403 M Precipitate no and aldehyde alone not solube Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp180

+

acetic acid

+

1-heptylamine

+

phenanthrene-9-carboxaldehyde



n-butyl isocyanide

21105834

Reaction ID UCEXP182 Researcher Emily Messner Reaction Type Ugi Solvent methanol Limiting Reactant 0.398 M Precipitate Reactants Insoluble Comments Reference http://usefulchem.wikispaces.com/Exp182

+

furoic acid

+

1-heptylamine

+

phenanthrene-9-carboxaldehyde

Reaction ID UCEXP215A Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 0.661 M

5



n-butyl isocyanide

21168529

Precipitate Comments Reference

No http://usefulchem.wikispaces.com/Exp215

+

crotonic acid

+

1-heptylamine

+

phenanthrene-9-carboxaldehyde



t-butyl isocyanide

21106058

Reaction ID UCEXP231-8

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 0.833 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp231

+

glycolic acid

+

1-heptylamine

+

2-methoxy-1-naphthaldehyde



tosylmethyl isocyanide

24528188

Reaction ID UCExp236-15 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.614 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp236

+

3,3'-dichloropivalic acid

+

1-heptylamine

+

4-(trifluoromethyl)benzaldehyde



t-butyl isocyanide

24528288

Reaction ID UCExp238-08 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.74 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp238

+

crotonic acid

+

1-heptylamine

+

phenanthrene-9-carboxaldehyde

Reaction ID UCExp238-20 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.775 M Precipitate No Comments -

6



cyclohexylisocyanide

24528310

Reference

http://usefulchem.wikispaces.com/Exp238

+

crotonic acid

+

1-heptylamine

+

phenanthrene-9-carboxaldehyde



t-butyl isocyanide

21106058

Reaction ID UCExp238-32

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.572 M Precipitate Yes Product Awaiting Characterization Comments Reference http://usefulchem.wikispaces.com/Exp238

+

Boc-Gly-OH

+

1-heptylamine

+

phenanthrene-9-carboxaldehyde



cyclohexylisocyanide

24528332

Reaction ID UCExp238-44 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.6 M Precipitate Yes Product Awaiting Characterization Comments Reference http://usefulchem.wikispaces.com/Exp238

+

Boc-Gly-OH

+

1-heptylamine

+

phenanthrene-9-carboxaldehyde



t-butyl isocyanide

24528344

Reaction ID UCExp241-44 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.72 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp241

+

3,4methylenedioxyphenylacetic acid

+

1-heptylamine

+

4-(trifluoromethyl)benzaldehyde

Reaction ID UCExp241-47 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.715 M

7



n-butyl isocyanide

24528377

Precipitate Comments Reference

No http://usefulchem.wikispaces.com/Exp241

+

3,4methylenedioxyphenylacetic acid

+

1-heptylamine

+

4-(trifluoromethyl)benzaldehyde



t-butyl isocyanide

24528380

1-hexylamine

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCEXP130-2 Researcher Rikesh Parikh Reaction Type Ugi Solvent methanol Limiting Reactant 0.728 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp130

+

formic acid

+

1-hexylamine

+

2-naphthaldehyde



1-pentyl isocyanide

21106078

Reaction ID UCEXP131-6 Researcher Rikesh Parikh Reaction Type Ugi Solvent methanol Limiting Reactant 0.625 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp131

+

Boc-Trp-OH

+

1-hexylamine

+

o-vanillin



n-butyl isocyanide

21106063

Reaction ID UCEXP131-7 Researcher Rikesh Parikh Reaction Type Ugi Solvent methanol Limiting Reactant 0.617 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp131

+

Boc-Trp-OH

+

1-hexylamine

+

o-vanillin

Reaction ID UCEXP181-064V2 Researcher

Khalid Mirza

8



1-pentyl isocyanide

21106064

Reaction Type Ugi Solvent methanol Limiting Reactant 0.221 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

+

3-methylbut-2-enoic acid

+

1-hexylamine

+

3,4-dihydroxybenzaldehyde



tosylmethyl isocyanide

24528103

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCEXP181-078V2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.219 M Precipitate Reactants Insoluble Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

+

1-pyrenebutyric acid

+

1-hexylamine

+

2-hydroxybenzaldehyde



t-butyl isocyanide

24528114

Reaction ID UCEXP181-109V2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.22 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

+

4-hydroxybenzoic acid

+

1-hexylamine

+

3-methoxybenzaldehyde



tosylmethyl isocyanide

24528139

Reaction ID UCEXP229-2 Researcher David Bulger Reaction Type Ugi Solvent methanol Limiting Reactant 0.667 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp229

+

Boc-Trp-OH

+

1-hexylamine

+

benzaldehyde

Reaction ID UCExp236-07 Researcher Reaction Type Solvent

Khalid Mirza Ugi methanol

9



n-butyl isocyanide

24528183

Limiting Reactant 0.614 M Precipitate Yes Yield - % Comments Reference http://usefulchem.wikispaces.com/Exp236

+

3,3'-dichloropivalic acid

+

1-hexylamine

+

4-(trifluoromethyl)benzaldehyde



t-butyl isocyanide

24528280

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCExp236-28 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.631 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp236

+

methacrylic acid

+

1-hexylamine

+

4-(trifluoromethyl)benzaldehyde



t-butyl isocyanide

24528301

Reaction ID UCExp238-09 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.794 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp238

+

crotonic acid

+

1-hexylamine

+

phenanthrene-9-carboxaldehyde



cyclohexylisocyanide

24528311

Reaction ID UCExp238-21 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.831 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp238

+

crotonic acid

+

1-hexylamine

+

phenanthrene-9-carboxaldehyde

Reaction ID UCExp238-33 Researcher

Khalid Mirza

10



t-butyl isocyanide

24528321

Reaction Type Ugi Solvent THF Limiting Reactant 1.616 M Precipitate Yes Product Awaiting Characterization Comments Reference http://usefulchem.wikispaces.com/Exp238

+

Boc-Gly-OH

+

1-hexylamine

+

phenanthrene-9-carboxaldehyde



cyclohexylisocyanide

24528333

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCExp241-29 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.729 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp241

+

3,4methylenedioxyphenylacetic acid

+

1-hexylamine

+

4-(trifluoromethyl)benzaldehyde



n-butyl isocyanide

24528366

1-octylamine Reaction ID UCEXP131-5 Researcher Rikesh Parikh Reaction Type Ugi Solvent methanol Limiting Reactant 0.605 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp131

+

Boc-Trp-OH

+

1-octylamine

+

o-vanillin



benzyl isocyanide

21106062

Reaction ID UCEXP134-3 Researcher Rikesh Parikh Reaction Type Ugi Solvent methanol Limiting Reactant 0.612 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp134

+

Boc-Trp-OH

+

1-octylamine

+

o-vanillin

11



n-butyl isocyanide

21106072

Reaction ID UCEXP134-4 Researcher Rikesh Parikh Reaction Type Ugi Solvent methanol Limiting Reactant 0.604 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp134

+

Boc-Trp-OH

+

1-octylamine

+

o-vanillin



1-pentyl isocyanide

21106073

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

1-pentyl isocyanide Reaction ID UCEXP130-2 Researcher Rikesh Parikh Reaction Type Ugi Solvent methanol Limiting Reactant 0.728 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp130

+

formic acid

+

1-hexylamine

+

2-naphthaldehyde



1-pentyl isocyanide

21106078

Reaction ID UCEXP131-2 Researcher Rikesh Parikh Reaction Type Ugi Solvent methanol Limiting Reactant 0.623 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp131

+

Boc-Trp-OH

+

furfurylamine

+

veratraldehyde



1-pentyl isocyanide

21106068

Reaction ID UCEXP131-3 Researcher Rikesh Parikh Reaction Type Ugi Solvent methanol Limiting Reactant 0.614 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp131

+

+

+

12



Boc-Trp-OH

5-methylfurfurylamine

veratraldehyde

1-pentyl isocyanide

21106069

Reaction ID UCEXP131-7 Researcher Rikesh Parikh Reaction Type Ugi Solvent methanol Limiting Reactant 0.617 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp131

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

+

Boc-Trp-OH

+

1-hexylamine

+

o-vanillin



1-pentyl isocyanide

21106064

Reaction ID UCEXP131-9 Researcher Rikesh Parikh Reaction Type Ugi Solvent methanol Limiting Reactant 0.61 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp131

+

Boc-Trp-OH

+

1-heptylamine

+

o-vanillin



1-pentyl isocyanide

21106066

Reaction ID UCEXP134-2 Researcher Rikesh Parikh Reaction Type Ugi Solvent methanol Limiting Reactant 0.636 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp134

+

Boc-Trp-OH

+

1-propylamine

+

o-vanillin

Reaction ID UCEXP134-4 Researcher Rikesh Parikh Reaction Type Ugi Solvent methanol Limiting Reactant 0.604 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp134

13



1-pentyl isocyanide

21106071

+

Boc-Trp-OH

+

1-octylamine

+

o-vanillin



1-pentyl isocyanide

21106073

Reaction ID UCEXP225-3 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.888 M Precipitate Yes Product Pending Comments 0.5 mmol of isocyanide was added to 500uL of a 2M solution of aldehyde; amine and acid Reference http://usefulchem.wikispaces.com/Exp225

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

+

Boc-Gly-OH

+

furfurylamine

+

piperonal



1-pentyl isocyanide

24528159

Reaction ID UCEXP226-3 Researcher David Bulger Reaction Type Ugi Solvent THF Limiting Reactant 0.519 M Precipitate No Comments 0.5 mmol of isocyanide was added to 900uL of a 0.55M solution of aldehyde; amine and acid Reference http://usefulchem.wikispaces.com/Exp226

+

1-pyrenebutyric acid

+

5-methylfurfurylamine

+

benzaldehyde



1-pentyl isocyanide

24528167

Reaction ID UCEXP227-3 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 0.444 M Precipitate No Comments 0.5 mmol of isocyanide was added to 500uL of a 0.5M solution of aldehyde; amine and acid Reference http://usefulchem.wikispaces.com/Exp227

+

1-pyrenebutyric acid

+

furfurylamine

+

piperonal

Reaction ID UCEXP232-03 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.099 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

14



1-pentyl isocyanide

24528175

+

Boc-Gly-OH

+

+

furfurylamine

benzaldehyde



1-pentyl isocyanide

24528190

Reaction ID UCEXP232-08 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.083 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

+

Boc-Gly-OH

+

+

furfurylamine

4-methylbenzaldehyde



1-pentyl isocyanide

24528195

Reaction ID UCEXP232-13 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.029 M Precipitate Yes Product Pending Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+

4-(trifluoromethyl)benzaldehyde



1-pentyl isocyanide

24528200

Reaction ID UCEXP232-18 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.367 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+

crotonaldehyde

Reaction ID UCEXP232-23 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.008 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

15



1-pentyl isocyanide

24528204

+

Boc-Gly-OH

+

+

furfurylamine

diphenylacetaldehyde



1-pentyl isocyanide

24528209

Reaction ID UCEXP232-28 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.093 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

+

Boc-Gly-OH

+

furfurylamine

+

cyclohexancarboxaldehyde



1-pentyl isocyanide

24528214

Reaction ID UCEXP232-33 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.111 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

+

furfurylamine

2-furaldehyde



1-pentyl isocyanide

24528219

Reaction ID UCEXP232-38 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.081 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+

2-hydroxybenzaldehyde

Reaction ID UCEXP232-43 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.083 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

16



1-pentyl isocyanide

24528224

+

Boc-Gly-OH

+

+

furfurylamine

o-tolualdehyde



1-pentyl isocyanide

24528229

Reaction ID UCEXP232-48 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.067 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

+

Boc-Gly-OH

+

furfurylamine

+

4-methoxybenzaldehyde



1-pentyl isocyanide

24528234

Reaction ID UCEXP232-53 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.106 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+

hexanaldehyde



1-pentyl isocyanide

24528239

Reaction ID UCEXP232-58 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.109 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+

trans-2-hexenal

Reaction ID UCEXP232-63 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.07 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

17



1-pentyl isocyanide

24528243

+

Boc-Gly-OH

+

furfurylamine

+

2-phenylpropionaldehyde



1-pentyl isocyanide

24534418

Reaction ID UCEXP232-68 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.067 M Precipitate Yes Product Pending Comments Reference http://usefulchem.wikispaces.com/Exp232

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

+

Boc-Gly-OH

+

+

furfurylamine

m-anisaldehyde



1-pentyl isocyanide

24528253

Reaction ID UCEXP232-73 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.106 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

+

furfurylamine

2-ethylbutyraldehyde



1-pentyl isocyanide

24528258

Reaction ID UCExp240-06 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.559 M Precipitate Yes Yield - % Comments Reference http://usefulchem.wikispaces.com/Exp240

+

phenylacetic acid

+

furfurylamine

+

phenanthrene-9-carboxaldehyde

Reaction ID UCExp240-12 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.776 M Precipitate Yes but 48h Comments Reference http://usefulchem.wikispaces.com/Exp240

18



1-pentyl isocyanide

24528347

+

phenylacetic acid

+

5-methylfurfurylamine

+

phenanthrene-9-carboxaldehyde



1-pentyl isocyanide

24528351

Reaction ID UCExp241-12 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.563 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp241

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

+

+

3,4methylenedioxyphenylacetic acid

+

methylamine

veratraldehyde



1-pentyl isocyanide

24528358

Reaction ID UCExp241-13 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.563 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp241

+

+

3,4methylenedioxyphenylacetic acid

+

methylamine

veratraldehyde



1-pentyl isocyanide

24528358

Reaction ID UCExp242-10 Researcher Marshall Moritz Reaction Type Ugi Solvent benzene Limiting Reactant 0.424 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp242

+

phenylacetic acid

+

5-methylfurfurylamine

+

phenanthrene-9-carboxaldehyde

Reaction ID UCExp242-5 Researcher Marshall Moritz Reaction Type Ugi Solvent benzene Limiting Reactant 0.432 M Precipitate No Comments -

19



1-pentyl isocyanide

24528382

Reference

http://usefulchem.wikispaces.com/Exp242

+

phenylacetic acid

+

furfurylamine

+

phenanthrene-9-carboxaldehyde



1-pentyl isocyanide

24528386

1-propylamine Reaction ID UCEXP134-1

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Researcher Rikesh Parikh Reaction Type Ugi Solvent methanol Limiting Reactant 0.645 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp134

+

Boc-Trp-OH

+

+

1-propylamine

o-vanillin



n-butyl isocyanide

21106070

Reaction ID UCEXP134-2 Researcher Rikesh Parikh Reaction Type Ugi Solvent methanol Limiting Reactant 0.636 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp134

+

Boc-Trp-OH

+

+

1-propylamine

o-vanillin



1-pentyl isocyanide

21106071

Reaction ID UCEXP167A-V1B12 Researcher Tim Bohinsky Reaction Type Ugi Solvent methanol Limiting Reactant 0.403 M Precipitate Reactants Insoluble Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp167

+

3,4methylenedioxyphenylacetic acid

+

1-propylamine

+

phenanthrene-9-carboxaldehyde

Reaction ID UCEXP174G/V2B39 Researcher Reaction Type Solvent

Khalid Mirza Ugi methanol

20



n-butyl isocyanide

21105597

Limiting Reactant 0.222 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp174

+

3,4-dihydroxyphenylacetic acid

+

+

1-propylamine

4-methylbenzaldehyde



tosylmethyl isocyanide

21106199

Reaction ID UCEXP177

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Researcher Shannon Oseback Reaction Type Ugi Solvent methanol Limiting Reactant 0.224 M Precipitate Reactants Insoluble Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp177

+

phenylacetic acid

+

1-propylamine

+

phenanthrene-9-carboxaldehyde



n-butyl isocyanide

21105831

Reaction ID UCEXP181-063V2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.222 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

+

3,4-dihydroxyphenylacetic acid

+

1-propylamine

+

2-hydroxybenzaldehyde



tosylmethyl isocyanide

24528102

Reaction ID UCEXP181-076V2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.224 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

+

diphenylacetic acid

+

1-propylamine

+

3,4-dihydroxybenzaldehyde

Reaction ID UCExp236-13 Researcher Reaction Type Solvent

Khalid Mirza Ugi methanol

21



n-butyl isocyanide

24528112

Limiting Reactant 0.614 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp236

+

3,3'-dichloropivalic acid

+

1-propylamine

+

4-(trifluoromethyl)benzaldehyde



n-butyl isocyanide

24528286

Reaction ID UCExp238-11

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.965 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp238

+

crotonic acid

+

1-propylamine

+

phenanthrene-9-carboxaldehyde



cyclohexylisocyanide

24528313

Reaction ID UCExp238-23 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 2.009 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp238

+

crotonic acid

+

1-propylamine

+

phenanthrene-9-carboxaldehyde



t-butyl isocyanide

24528323

Reaction ID UCExp238-35 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.753 M Precipitate Yes Product Awaiting Characterization Comments Reference http://usefulchem.wikispaces.com/Exp238

+

Boc-Gly-OH

+

1-propylamine

+

phenanthrene-9-carboxaldehyde

Reaction ID UCExp241-40 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.749 M

22



cyclohexylisocyanide

24528335

Precipitate Comments Reference

No http://usefulchem.wikispaces.com/Exp241

+

3,4methylenedioxyphenylacetic acid

+

1-propylamine

+

2,4-dimethylbenzaldehyde



t-butyl isocyanide

24528375

1-pyrenebutyric acid

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCEXP147-3V2B6 Researcher Mitesh Shah Reaction Type Ugi Solvent methanol Limiting Reactant 0.662 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp+147

+

1-pyrenebutyric acid

+

methylamine

+

2-naphthaldehyde



t-butyl isocyanide

21105841

Reaction ID UCEXP171B/V2B2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.219 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp171

+

1-pyrenebutyric acid

+

5-methylfurfurylamine

+

o-vanillin



t-butyl isocyanide

21106056

Reaction ID UCEXP171D/V2B4 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.219 M Precipitate Yes Product No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp171

+

1-pyrenebutyric acid

+

benzylamine

+

o-vanillin

Reaction ID UCEXP171FV2B6

23



t-butyl isocyanide

21105846

Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.222 M Precipitate Yes but reactants initially insoluble Yield - % Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp171

+

1-pyrenebutyric acid

+

+

methylamine

2-naphthaldehyde



t-butyl isocyanide

21105841

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCEXP171KV2B11 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.222 M Precipitate Yes Yield - % Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp171

+

1-pyrenebutyric acid

+

methylamine

+

4-(dimethylamino)benzaldehyde



t-butyl isocyanide

21105842

Reaction ID UCEXP171LV2B-12 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.22 M Precipitate Reactants Insoluble Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp171

+

1-pyrenebutyric acid

+

methylamine

+

phenanthrene-9-carboxaldehyde



t-butyl isocyanide

21106039

Reaction ID UCEXP173B/V2B14 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.223 M Precipitate Yes but reactants initially insoluble Yield - % Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp173

+

1-pyrenebutyric acid

+

methylamine

+

4-methylbenzaldehyde

24



t-butyl isocyanide

21105844

Reaction ID UCEXP173C/V2B15 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.222 M Precipitate Reactants Insoluble Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp173

+

1-pyrenebutyric acid

+

methylamine

+

4-(trifluoromethyl)benzaldehyde



t-butyl isocyanide

21106044

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCEXP173D/V2B16 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.224 M Precipitate Reactants Insoluble Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp173

+

1-pyrenebutyric acid

+

methylamine

+

2-hydroxybenzaldehyde



n-butyl isocyanide

21106048

Reaction ID UCEXP173J/V2B22 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.224 M Precipitate Reactants Insoluble Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp173

+

1-pyrenebutyric acid

+

methylamine

+

3,4-dihydroxybenzaldehyde



t-butyl isocyanide

21106038

Reaction ID UCEXP173P/V2B28 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.222 M Precipitate Reactants Insoluble Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp173

+

1-pyrenebutyric acid

+

methylamine

+

3-methoxybenzaldehyde

Reaction ID UCEXP181-070V2

25



t-butyl isocyanide

21106050

Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.22 M Precipitate Reactants Insoluble Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

+

1-pyrenebutyric acid

+

+

3-chloroaniline

2-methylbenzaldehyde



n-butyl isocyanide

24528530

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCEXP181-078V2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.219 M Precipitate Reactants Insoluble Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

+

1-pyrenebutyric acid

+

1-hexylamine

+

2-hydroxybenzaldehyde



t-butyl isocyanide

24528114

Reaction ID UCEXP181-083V2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.221 M Precipitate Reactants Insoluble Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

+

1-pyrenebutyric acid

+

+

aniline

benzaldehyde



n-butyl isocyanide

21106208

Reaction ID UCEXP181-087V2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.222 M Precipitate Reactants Insoluble Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

+

1-pyrenebutyric acid

+

methylamine

+

2,4-dimethylbenzaldehyde

Reaction ID UCEXP215C Researcher Reaction Type

Khalid Mirza Ugi

26



t-butyl isocyanide

21106206

Solvent THF Limiting Reactant 0.662 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp215

+

1-pyrenebutyric acid

+

+

methylamine

2-naphthaldehyde



t-butyl isocyanide

21105841

Reaction ID UCEXP215D

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 0.66 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp215

+

1-pyrenebutyric acid

+

methylamine

+

4-(dimethylamino)benzaldehyde



t-butyl isocyanide

21105842

Reaction ID UCEXP222-5 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 0.898 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp222

+

1-pyrenebutyric acid

+

methylamine

+

4-(dimethylamino)benzaldehyde



t-butyl isocyanide

21105842

Reaction ID UCEXP222-6 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 0.898 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp222

+

1-pyrenebutyric acid

+

methylamine

+

4-methylbenzaldehyde

Reaction ID UCEXP226-1 Researcher David Bulger Reaction Type Ugi Solvent THF Limiting Reactant 0.523 M

27



t-butyl isocyanide

21105844

Precipitate Comments Reference

No 0.5 mmol of isocyanide was added to 900uL of a 0.55M solution of aldehyde; amine and acid http://usefulchem.wikispaces.com/Exp226

+

1-pyrenebutyric acid

+

5-methylfurfurylamine

+

benzaldehyde



t-butyl isocyanide

24528165

Reaction ID UCEXP226-2

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Researcher David Bulger Reaction Type Ugi Solvent THF Limiting Reactant 0.525 M Precipitate No Comments 0.5 mmol of isocyanide was added to 900uL of a 0.55M solution of aldehyde; amine and acid Reference http://usefulchem.wikispaces.com/Exp226

+

1-pyrenebutyric acid

+

5-methylfurfurylamine

+

benzaldehyde



n-butyl isocyanide

24528166

Reaction ID UCEXP226-3 Researcher David Bulger Reaction Type Ugi Solvent THF Limiting Reactant 0.519 M Precipitate No Comments 0.5 mmol of isocyanide was added to 900uL of a 0.55M solution of aldehyde; amine and acid Reference http://usefulchem.wikispaces.com/Exp226

+

1-pyrenebutyric acid

+

5-methylfurfurylamine

+

benzaldehyde



1-pentyl isocyanide

24528167

Reaction ID UCEXP226-4 Researcher David Bulger Reaction Type Ugi Solvent THF Limiting Reactant 0.52 M Precipitate No Comments 0.5 mmol of isocyanide was added to 900uL of a 0.55M solution of aldehyde; amine and acid Reference http://usefulchem.wikispaces.com/Exp226

+

1-pyrenebutyric acid

+

5-methylfurfurylamine

+

benzaldehyde



cyclohexylisocyanide

Reaction ID UCEXP226-5 Researcher David Bulger Reaction Type Ugi Solvent THF Limiting Reactant 0.52 M Precipitate No Comments 0.5 mmol of isocyanide was added to 900uL of a 0.55M solution of aldehyde; amine and acid

28

24528168

Reference

http://usefulchem.wikispaces.com/Exp226

+

1-pyrenebutyric acid

+

5-methylfurfurylamine

+

benzaldehyde



benzyl isocyanide

24528169

Reaction ID UCEXP226-6 Researcher David Bulger Reaction Type Ugi Solvent THF Limiting Reactant 0.501 M Precipitate No Comments 0.5 mmol of isocyanide was added to 900uL of a 0.55M solution of aldehyde; amine and acid Reference http://usefulchem.wikispaces.com/Exp226

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

+

1-pyrenebutyric acid

+

5-methylfurfurylamine

+

benzaldehyde



tosylmethyl isocyanide

24528170

Reaction ID UCEXP226-7 Researcher David Bulger Reaction Type Ugi Solvent THF Limiting Reactant 0.516 M Precipitate No Comments 0.5 mmol of isocyanide was added to 900uL of a 0.55M solution of aldehyde; amine and acid Reference http://usefulchem.wikispaces.com/Exp226

+

1-pyrenebutyric acid

+

5-methylfurfurylamine

+



2-morpholinoethyl isocyanide

benzaldehyde

24528171

Reaction ID UCEXP226-8 Researcher David Bulger Reaction Type Ugi Solvent THF Limiting Reactant 0.434 M Precipitate No Comments 0.5 mmol of isocyanide was added to 500uL of a 0.5M solution of aldehyde; amine and acid Reference http://usefulchem.wikispaces.com/Exp226

+

1-pyrenebutyric acid

+

5-methylfurfurylamine

+

benzaldehyde

Reaction ID UCEXP227-1 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 0.261 M Precipitate No

29



2-chloro-6methylphenyl isocyanide

24528172

Comments Reference

0.5 mmol of isocyanide was added to 500uL of a 0.5M solution of aldehyde; amine and acid http://usefulchem.wikispaces.com/Exp227

+

1-pyrenebutyric acid

+

furfurylamine

+

piperonal



t-butyl isocyanide

24528173

Reaction ID UCEXP227-2

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 0.453 M Precipitate No Comments 0.5 mmol of isocyanide was added to 500uL of a 0.5M solution of aldehyde; amine and acid Reference http://usefulchem.wikispaces.com/Exp227

+

1-pyrenebutyric acid

+

furfurylamine

+

piperonal



n-butyl isocyanide

24528174

Reaction ID UCEXP227-3 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 0.444 M Precipitate No Comments 0.5 mmol of isocyanide was added to 500uL of a 0.5M solution of aldehyde; amine and acid Reference http://usefulchem.wikispaces.com/Exp227

+

1-pyrenebutyric acid

+

furfurylamine

+

piperonal



1-pentyl isocyanide

24528175

Reaction ID UCEXP227-4 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 0.445 M Precipitate No Comments 0.5 mmol of isocyanide was added to 500uL of a 0.5M solution of aldehyde; amine and acid Reference http://usefulchem.wikispaces.com/Exp227

+

1-pyrenebutyric acid

+

furfurylamine

+

piperonal



cyclohexylisocyanide

Reaction ID UCEXP227-5 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 0.446 M Precipitate No Comments 0.5 mmol of isocyanide was added to 500uL of a 0.5M solution of aldehyde; amine and acid Reference http://usefulchem.wikispaces.com/Exp227

30

24528176

+

1-pyrenebutyric acid

+

furfurylamine

+

piperonal



benzyl isocyanide

24528177

Reaction ID UCEXP227-6 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 0.251 M Precipitate No Comments 0.5 mmol of isocyanide was added to 500uL of a 0.5M solution of aldehyde; amine and acid Reference http://usefulchem.wikispaces.com/Exp227

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

+

1-pyrenebutyric acid

+

furfurylamine

+

piperonal



tosylmethyl isocyanide

24528178

Reaction ID UCEXP227-7 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 0.439 M Precipitate No Comments 0.5 mmol of isocyanide was added to 500uL of a 0.5M solution of aldehyde; amine and acid Reference http://usefulchem.wikispaces.com/Exp227

+

1-pyrenebutyric acid

+

furfurylamine

+



2-morpholinoethyl isocyanide

piperonal

24528179

Reaction ID UCEXP227-8 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 0.434 M Precipitate No Comments 0.5 mmol of isocyanide was added to 500uL of a 0.5M solution of aldehyde; amine and acid Reference http://usefulchem.wikispaces.com/Exp227

+

1-pyrenebutyric acid

+

furfurylamine

+

piperonal

Reaction ID UCEXP228-7 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 0.67 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp228

31



2-chloro-6methylphenyl isocyanide

24528180

+

1-pyrenebutyric acid

+

methylamine

+

4-methylbenzaldehyde



t-butyl isocyanide

21105844

Reaction ID UCEXP231-3 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 0.75 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp231

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

+

1-pyrenebutyric acid

+

methylamine

+

2-naphthaldehyde



t-butyl isocyanide

21105841

Reaction ID UCEXP231-7 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 0.667 M Precipitate Yes Product Pending Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp231

+

1-pyrenebutyric acid

+

furfurylamine

+

2-furaldehyde



n-butyl isocyanide

24528187

1,1,3,3-tetramethylbutyl isocyanide Reaction ID UCEXP232-05 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.098 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde

Reaction ID UCEXP232-10 Researcher Reaction Type Solvent

Khalid Mirza Ugi methanol

32



1,1,3,3tetramethylbutyl isocyanide

24528192

Limiting Reactant 1.083 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

+

furfurylamine



1,1,3,3tetramethylbutyl isocyanide

4-methylbenzaldehyde

24528197

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCEXP232-15 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.028 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+



1,1,3,3tetramethylbutyl isocyanide

4-(trifluoromethyl)benzaldehyde

24528201

Reaction ID UCEXP232-20 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.366 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+



1,1,3,3tetramethylbutyl isocyanide

crotonaldehyde

24528206

Reaction ID UCEXP232-25 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.008 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+

diphenylacetaldehyde

33



1,1,3,3tetramethylbutyl isocyanide

24528211

Reaction ID UCEXP232-30 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.092 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+



1,1,3,3tetramethylbutyl isocyanide

cyclohexancarboxaldehyde

24528216

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCEXP232-35 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.11 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

+

furfurylamine



1,1,3,3tetramethylbutyl isocyanide

2-furaldehyde

24528221

Reaction ID UCEXP232-40 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.081 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+



1,1,3,3tetramethylbutyl isocyanide

2-hydroxybenzaldehyde

24528226

Reaction ID UCEXP232-45 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.083 M Precipitate Yes Product Pending Comments Reference http://usefulchem.wikispaces.com/Exp232

+

+

+

34



Boc-Gly-OH

furfurylamine

1,1,3,3tetramethylbutyl isocyanide

o-tolualdehyde

24528231

Reaction ID UCEXP232-50

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.066 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+



1,1,3,3tetramethylbutyl isocyanide

4-methoxybenzaldehyde

24528236

Reaction ID UCEXP232-55 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.106 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+



1,1,3,3tetramethylbutyl isocyanide

hexanaldehyde

24528241

Reaction ID UCEXP232-60 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.109 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+

trans-2-hexenal

Reaction ID UCEXP232-65 Researcher Reaction Type

Khalid Mirza Ugi

35



1,1,3,3tetramethylbutyl isocyanide

24528245

Solvent methanol Limiting Reactant 1.069 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+



1,1,3,3tetramethylbutyl isocyanide

2-phenylpropionaldehyde

24534420

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCEXP232-70 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.067 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

+

furfurylamine



1,1,3,3tetramethylbutyl isocyanide

m-anisaldehyde

24528255

Reaction ID UCEXP232-75 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.105 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

+

furfurylamine



1,1,3,3tetramethylbutyl isocyanide

2-ethylbutyraldehyde

24528260

Reaction ID UCExp240-04 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.458 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp240

+

phenylacetic acid

+

furfurylamine

+

phenanthrene-9-carboxaldehyde

36



1,1,3,3tetramethylbutyl isocyanide

21782583

Reaction ID UCExp240-10 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.646 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp240

+

phenylacetic acid

+

5-methylfurfurylamine

+



1,1,3,3tetramethylbutyl isocyanide

phenanthrene-9-carboxaldehyde

24528349

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCExp241-10 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.548 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp241

+

3,4methylenedioxyphenylacetic acid

+

methylamine

+



1,1,3,3tetramethylbutyl isocyanide

veratraldehyde

24528357

Reaction ID UCExp241-11 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.548 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp241

+

3,4methylenedioxyphenylacetic acid

+

methylamine

+



1,1,3,3tetramethylbutyl isocyanide

veratraldehyde

24528357

Reaction ID UCExp242-4 Researcher Marshall Moritz Reaction Type Ugi Solvent benzene Limiting Reactant 0.414 M Precipitate Yes Product No Comments Reference http://usefulchem.wikispaces.com/Exp242

+

+

+

37



phenylacetic acid

furfurylamine

1,1,3,3tetramethylbutyl isocyanide

phenanthrene-9-carboxaldehyde

24528385

Reaction ID UCExp242-9

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Researcher Marshall Moritz Reaction Type Ugi Solvent benzene Limiting Reactant 0.406 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp242

+

phenylacetic acid

+

5-methylfurfurylamine

+



1,1,3,3tetramethylbutyl isocyanide

phenanthrene-9-carboxaldehyde

24528390

Reaction ID UCExp245-09 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.492 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp245

+

3,4methylenedioxyphenylacetic acid

+

furfurylamine

+



1,1,3,3tetramethylbutyl isocyanide

piperonal

24528395

Reaction ID UCExp245-10 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.683 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp245

+

3,4methylenedioxyphenylacetic acid

+

furfurylamine

+

piperonal

Reaction ID UCExp245-15 Researcher Reaction Type

Khalid Mirza Ugi

38



1,1,3,3tetramethylbutyl isocyanide

24528395

Solvent methanol Limiting Reactant 0.486 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp245

+

3,4methylenedioxyphenylacetic acid

+

5-methylfurfurylamine

+



1,1,3,3tetramethylbutyl isocyanide

piperonal

24528398

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCExp245-16 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.673 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp245

+

3,4methylenedioxyphenylacetic acid

+

5-methylfurfurylamine

+



1,1,3,3tetramethylbutyl isocyanide

piperonal

24528398

Reaction ID UCExp245-25 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.509 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp245

+

cbz-proline

+

furfurylamine

+



1,1,3,3tetramethylbutyl isocyanide

piperonal

24528403

Reaction ID UCExp245-26 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.038 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp245

+

cbz-proline

+

furfurylamine

+

piperonal

39



1,1,3,3tetramethylbutyl isocyanide

24528403

Reaction ID UCExp245-29 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.503 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp245

+

cbz-proline

+

5-methylfurfurylamine

+



1,1,3,3tetramethylbutyl isocyanide

piperonal

24528405

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCExp245-30 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.013 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp245

+

cbz-proline

+

5-methylfurfurylamine

+



1,1,3,3tetramethylbutyl isocyanide

piperonal

24528405

Reaction ID UCExp245-35 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.492 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp245

+

3,4methylenedioxyphenylacetic acid

+

furfurylamine

+



1,1,3,3tetramethylbutyl isocyanide

piperonal

24528408

Reaction ID UCExp245-36 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.683 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp245

+

+

+

40



3,4methylenedioxyphenylacetic acid

furfurylamine

1,1,3,3tetramethylbutyl isocyanide

piperonal

24528408

2-chloro-6-methylphenyl isocyanide Reaction ID UCEXP225-8

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.868 M Precipitate No Comments 0.5 mmol of isocyanide was added to 500uL of a 2M solution of aldehyde; amine and acid Reference http://usefulchem.wikispaces.com/Exp225

+

Boc-Gly-OH

+

furfurylamine

+



2-chloro-6methylphenyl isocyanide

piperonal

24528164

Reaction ID UCEXP226-8 Researcher David Bulger Reaction Type Ugi Solvent THF Limiting Reactant 0.434 M Precipitate No Comments 0.5 mmol of isocyanide was added to 500uL of a 0.5M solution of aldehyde; amine and acid Reference http://usefulchem.wikispaces.com/Exp226

+

1-pyrenebutyric acid

+

5-methylfurfurylamine

+



2-chloro-6methylphenyl isocyanide

benzaldehyde

24528172

Reaction ID UCEXP227-8 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 0.434 M Precipitate No Comments 0.5 mmol of isocyanide was added to 500uL of a 0.5M solution of aldehyde; amine and acid Reference http://usefulchem.wikispaces.com/Exp227

+

1-pyrenebutyric acid

+

furfurylamine

+

piperonal

41



2-chloro-6methylphenyl isocyanide

24528180

2-chloroaniline Reaction ID UCEXP173N/V2B26 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.217 M Precipitate Reactants Insoluble Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp173

+

decanoic acid

+

+

2-chloroaniline

o-vanillin



tosylmethyl isocyanide

21105847

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCEXP181-081V2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.224 M Precipitate Reactants Insoluble Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

+

3,4-dihydroxyphenylacetic acid

+

+

2-chloroaniline

2-naphthaldehyde



t-butyl isocyanide

24528117

Reaction ID UCEXP181-092V2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.217 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

+

decanoic acid

+

2-chloroaniline

+

3-methoxybenzaldehyde



tosylmethyl isocyanide

24528124

Reaction ID UCEXP181-099V2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.221 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

+

+

+

42



4-hydroxybenzoic acid

2-chloroaniline

4-methoxybenzaldehyde

tosylmethyl isocyanide

24528130

Reaction ID UCEXP181-122V2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.22 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

+

4-hydroxybenzoic acid

+

+

2-chloroaniline

veratraldehyde



tosylmethyl isocyanide

24534443

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCExp236-09 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.614 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp236

+

3,3'-dichloropivalic acid

+

2-chloroaniline

+

4-(trifluoromethyl)benzaldehyde



t-butyl isocyanide

24528282

Reaction ID UCExp238-01 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.881 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp238

+

crotonic acid

+

2-chloroaniline

+

phenanthrene-9-carboxaldehyde



cyclohexylisocyanide

24528303

Reaction ID UCExp238-13 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.921 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp238

+

crotonic acid

+

2-chloroaniline

+

phenanthrene-9-carboxaldehyde

43



t-butyl isocyanide

24528315

Reaction ID UCExp238-25 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.686 M Precipitate Yes Product Awaiting Characterization Comments Reference http://usefulchem.wikispaces.com/Exp238

+

Boc-Gly-OH

+

2-chloroaniline

+

phenanthrene-9-carboxaldehyde



cyclohexylisocyanide

24528325

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCExp238-37 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.718 M Precipitate Yes but solvent evaporated Comments Reference http://usefulchem.wikispaces.com/Exp238

+

Boc-Gly-OH

+

2-chloroaniline

+

phenanthrene-9-carboxaldehyde



t-butyl isocyanide

24528337

Reaction ID UCExp241-31 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.743 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp241

+

3,4methylenedioxyphenylacetic acid

+

2-chloroaniline

+

4-(trifluoromethyl)benzaldehyde



n-butyl isocyanide

24528368

2-ethylbutyraldehyde Reaction ID UCEXP232-71 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.106 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

+

+

+

44



Boc-Gly-OH

furfurylamine

2-ethylbutyraldehyde

t-butyl isocyanide

24528256

Reaction ID UCEXP232-72 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.105 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

+

Boc-Gly-OH

+

furfurylamine

+

2-ethylbutyraldehyde



n-butyl isocyanide

24528257

Reaction ID UCEXP232-73 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.106 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+

2-ethylbutyraldehyde



1-pentyl isocyanide

24528258

Reaction ID UCEXP232-74 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.105 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+

2-ethylbutyraldehyde

Reaction ID UCEXP232-75 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.105 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

45



cyclohexylisocyanide

24528259

+

Boc-Gly-OH

+

furfurylamine

+



1,1,3,3tetramethylbutyl isocyanide

2-ethylbutyraldehyde

24528260

2-furaldehyde

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCEXP231-7 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 0.667 M Precipitate Yes Product Pending Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp231

+

1-pyrenebutyric acid

+

furfurylamine

+

2-furaldehyde



n-butyl isocyanide

24528187

Reaction ID UCEXP232-31 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.11 M Precipitate Yes Product Pending Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+

2-furaldehyde



t-butyl isocyanide

24528217

Reaction ID UCEXP232-32 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.11 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+

2-furaldehyde

Reaction ID UCEXP232-33 Researcher Reaction Type

Khalid Mirza Ugi

46



n-butyl isocyanide

24528218

Solvent methanol Limiting Reactant 1.111 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+

2-furaldehyde



1-pentyl isocyanide

24528219

Reaction ID UCEXP232-34

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.11 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+

2-furaldehyde



cyclohexylisocyanide

24528220

Reaction ID UCEXP232-35 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.11 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+



1,1,3,3tetramethylbutyl isocyanide

2-furaldehyde

24528221

Reaction ID UCExp241-03 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.512 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp241

+

3,4methylenedioxyphenylacetic acid

+

methylamine

+

2-furaldehyde

47



benzyl isocyanide

24534403

2-hydroxybenzaldehyde Reaction ID UCEXP171IV2B9 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.221 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp171

+

3,4methylenedioxyphenylacetic acid

+

aniline

+

2-hydroxybenzaldehyde



tosylmethyl isocyanide

21106055

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCEXP173D/V2B16 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.224 M Precipitate Reactants Insoluble Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp173

+

1-pyrenebutyric acid

+

methylamine

+

2-hydroxybenzaldehyde



n-butyl isocyanide

21106048

Reaction ID UCEXP174D/V2B35 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.221 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp174

+

benzoic acid

+

furfurylamine

+

2-hydroxybenzaldehyde



tosylmethyl isocyanide

21106202

Reaction ID UCEXP174E/V2B36 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.223 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp174

+

Boc-Trp-OH

+

methylamine

+

2-hydroxybenzaldehyde

48



n-butyl isocyanide

21106201

Reaction ID UCEXP174Q/V2B50 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.222 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp174

+

butyric acid

+

3-chloroaniline

+

2-hydroxybenzaldehyde



tosylmethyl isocyanide

21106191

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCEXP174R/V2B51 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.221 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp174

+

mandelic acid

+

3-chloroaniline

+

2-hydroxybenzaldehyde



tosylmethyl isocyanide

21106190

Reaction ID UCEXP174T/V2B53 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.219 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp174

+

2,5-dimethoxyphenylacetic acid

+

aniline

+

2-hydroxybenzaldehyde



tosylmethyl isocyanide

21106185

Reaction ID UCEXP181-063V2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.222 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

+

3,4-dihydroxyphenylacetic acid

+

1-propylamine

+

2-hydroxybenzaldehyde

49



tosylmethyl isocyanide

24528102

Reaction ID UCEXP181-078V2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.219 M Precipitate Reactants Insoluble Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

+

1-pyrenebutyric acid

+

1-hexylamine

+

2-hydroxybenzaldehyde



t-butyl isocyanide

24528114

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCEXP181-085V2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.219 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

+

2,5-dimethoxyphenylacetic acid

+

3-chloroaniline

+

2-hydroxybenzaldehyde



tosylmethyl isocyanide

24528120

Reaction ID UCEXP181-089V2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.221 M Precipitate Reactants Insoluble Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

+

hexanoic acid

+

3-chloroaniline

+

2-hydroxybenzaldehyde



tosylmethyl isocyanide

24528122

Reaction ID UCEXP181-093V2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.221 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

+

hexanoic acid

+

aniline

+

2-hydroxybenzaldehyde

50



tosylmethyl isocyanide

24528125

Reaction ID UCEXP181-097V2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.221 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

+

3,4-dihydroxyphenylacetic acid

+

furfurylamine

+

2-hydroxybenzaldehyde



tosylmethyl isocyanide

24528128

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCEXP181-107V2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.222 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

+

phenylpropynoic acid

+

aniline

+

2-hydroxybenzaldehyde



tosylmethyl isocyanide

24528137

Reaction ID UCEXP181-110V2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.222 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

+

3,4-dihydroxyphenylacetic acid

+

aniline

+

2-hydroxybenzaldehyde



tosylmethyl isocyanide

24528140

Reaction ID UCEXP181-124V2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.219 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

+

3-(4methoxyphenyl)propionic acid

+

benzylamine

+

2-hydroxybenzaldehyde

51



tosylmethyl isocyanide

24528152

Reaction ID UCEXP232-36 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.081 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+

2-hydroxybenzaldehyde



t-butyl isocyanide

24528222

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCEXP232-37 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.081 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+

2-hydroxybenzaldehyde



n-butyl isocyanide

24528223

Reaction ID UCEXP232-38 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.081 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+

2-hydroxybenzaldehyde



1-pentyl isocyanide

24528224

Reaction ID UCEXP232-39 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.081 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

Reaction ID UCEXP232-40

+

2-hydroxybenzaldehyde

52



cyclohexylisocyanide

24528225

Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.081 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+



1,1,3,3tetramethylbutyl isocyanide

2-hydroxybenzaldehyde

24528226

2-hydroxybenzaldehyde Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCEXP171EV2B5 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.22 M Precipitate Reactants Insoluble Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp171

+

3,4methylenedioxyphenylacetic acid

+

3-chloroaniline

+

2-hydroxybenzaldehyde



tosylmethyl isocyanide

21106047

Reaction ID UCEXP173A/V2B13 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.221 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp173

+

4-chlorophenylacetic acid

+

aniline

+

2-hydroxybenzaldehyde



tosylmethyl isocyanide

21106046

Reaction ID UCEXP181-057V2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.224 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

+

+

+

53



phenylpropynoic acid

methylamine

2-hydroxybenzaldehyde

tosylmethyl isocyanide

24528098

Reaction ID UCEXP181-060V2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.221 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

+

phenylpropynoic acid

+

furfurylamine

+

2-hydroxybenzaldehyde



tosylmethyl isocyanide

24528100

2-methoxy-1-naphthaldehyde Reaction ID UCEXP231-8 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 0.833 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp231

+

glycolic acid

+

1-heptylamine

+

2-methoxy-1-naphthaldehyde



tosylmethyl isocyanide

24528188

2-methylbenzaldehyde Reaction ID UCEXP181-059V2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.225 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

+

4-hydroxybenzoic acid

+

methylamine

+

2-methylbenzaldehyde

Reaction ID UCEXP181-070V2 Researcher Reaction Type Solvent

Khalid Mirza Ugi methanol

54



tosylmethyl isocyanide

24528099

Limiting Reactant 0.22 M Precipitate Reactants Insoluble Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

+

1-pyrenebutyric acid

+

3-chloroaniline

+

2-methylbenzaldehyde



n-butyl isocyanide

24528530

2-morpholinoethyl isocyanide

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCEXP225-7 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.879 M Precipitate No Comments 0.5 mmol of isocyanide was added to 500uL of a 2M solution of aldehyde; amine and acid Reference http://usefulchem.wikispaces.com/Exp225

+

Boc-Gly-OH

+

furfurylamine

+



2-morpholinoethyl isocyanide

piperonal

24528163

Reaction ID UCEXP226-7 Researcher David Bulger Reaction Type Ugi Solvent THF Limiting Reactant 0.516 M Precipitate No Comments 0.5 mmol of isocyanide was added to 900uL of a 0.55M solution of aldehyde; amine and acid Reference http://usefulchem.wikispaces.com/Exp226

+

1-pyrenebutyric acid

+

5-methylfurfurylamine

+



2-morpholinoethyl isocyanide

benzaldehyde

24528171

Reaction ID UCEXP227-7 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 0.439 M Precipitate No Comments 0.5 mmol of isocyanide was added to 500uL of a 0.5M solution of aldehyde; amine and acid Reference http://usefulchem.wikispaces.com/Exp227

+

1-pyrenebutyric acid

+

furfurylamine

+

piperonal

55



2-morpholinoethyl isocyanide

24528179

2-naphthaldehyde Reaction ID UCEXP130-1 Researcher Rikesh Parikh Reaction Type Ugi Solvent methanol Limiting Reactant 0.751 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp130

+

formic acid

+

5-methylfurfurylamine

+

2-naphthaldehyde



n-butyl isocyanide

21106081

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCEXP130-2 Researcher Rikesh Parikh Reaction Type Ugi Solvent methanol Limiting Reactant 0.728 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp130

+

formic acid

+

1-hexylamine

+

2-naphthaldehyde



1-pentyl isocyanide

21106078

Reaction ID UCEXP130-4 Researcher Rikesh Parikh Reaction Type Ugi Solvent methanol Limiting Reactant 0.725 M Precipitate Yes Product Not Determined Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp130

+

formic acid

+

furfurylamine

+

2-naphthaldehyde



benzyl isocyanide

21106080

Reaction ID UCEXP130-5 Researcher Rikesh Parikh Reaction Type Ugi Solvent methanol Limiting Reactant 0.734 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp130

+

+

+

56



formic acid

furfurylamine

2-naphthaldehyde

n-butyl isocyanide

21106079

Reaction ID UCEXP147-3V2B6 Researcher Mitesh Shah Reaction Type Ugi Solvent methanol Limiting Reactant 0.662 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp+147

+

1-pyrenebutyric acid

+

methylamine

+

2-naphthaldehyde



t-butyl isocyanide

21105841

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCEXP171FV2B6 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.222 M Precipitate Yes but reactants initially insoluble Yield - % Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp171

+

1-pyrenebutyric acid

+

methylamine

+

2-naphthaldehyde



t-butyl isocyanide

21105841

Reaction ID UCEXP171GV2B7 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.218 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp171

+

3,4-dihydroxyphenylacetic acid

+

furfurylamine

+

2-naphthaldehyde



tosylmethyl isocyanide

21106054

Reaction ID UCEXP173H/V2B20 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.22 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp173

+

+

+

57



3,4-dihydroxyphenylacetic acid

5-methylfurfurylamine

2-naphthaldehyde

tosylmethyl isocyanide

21106053

Reaction ID UCEXP174H/V2B40 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.223 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp174

+

2,4,6-trihydroxybenzoic acid

+

methylamine

+

2-naphthaldehyde



tosylmethyl isocyanide

21106188

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCEXP181-069V2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.221 M Precipitate Reactants Insoluble Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

+

2,4,6-trihydroxybenzoic acid

+

aniline

+

2-naphthaldehyde



tosylmethyl isocyanide

24528108

Reaction ID UCEXP181-081V2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.224 M Precipitate Reactants Insoluble Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

+

3,4-dihydroxyphenylacetic acid

+

2-chloroaniline

+

2-naphthaldehyde



t-butyl isocyanide

24528117

Reaction ID UCEXP181-106V2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.224 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

+

+

+

58



4-hydroxybenzoic acid

methylamine

2-naphthaldehyde

tosylmethyl isocyanide

24528136

Reaction ID UCEXP181-108V2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.223 M Precipitate Yes Product No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

+

+

D-(−)-Quinic acid

methylamine

+

2-naphthaldehyde



tosylmethyl isocyanide

24528138

Reaction ID UCEXP181-115V2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.224 M Precipitate Reactants Insoluble Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

+

3,4-dihydroxyphenylacetic acid

+

3-chloroaniline

+

2-naphthaldehyde



t-butyl isocyanide

24528144

Reaction ID UCEXP215C Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 0.662 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp215

+

1-pyrenebutyric acid

+

methylamine

+

2-naphthaldehyde

Reaction ID UCEXP231-3 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 0.75 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp231

59



t-butyl isocyanide

21105841

+

+

1-pyrenebutyric acid

+

methylamine

2-naphthaldehyde



t-butyl isocyanide

21105841

2-phenylbutyric acid Reaction ID UCEXP174M/V2B45

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.22 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp174

+

2-phenylbutyric acid

+

3-chloroaniline

+

3,4-dihydroxybenzaldehyde



tosylmethyl isocyanide

21106194

2-phenylpropionaldehyde Reaction ID UCEXP232-61 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.069 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+

2-phenylpropionaldehyde



t-butyl isocyanide

24534409

Reaction ID UCEXP232-62 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.069 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+

2-phenylpropionaldehyde

Reaction ID UCEXP232-63 Researcher Reaction Type Solvent

Khalid Mirza Ugi methanol

60



n-butyl isocyanide

24534417

Limiting Reactant 1.07 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+

2-phenylpropionaldehyde



1-pentyl isocyanide

24534418

Reaction ID UCEXP232-64

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.069 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+

2-phenylpropionaldehyde



cyclohexylisocyanide

24534419

Reaction ID UCEXP232-65 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.069 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+



1,1,3,3tetramethylbutyl isocyanide

2-phenylpropionaldehyde

24534420

2,3-dihydroxybenzoic acid Reaction ID UCEXP147-1V2B1 Researcher Mitesh Shah Reaction Type Ugi Solvent methanol Limiting Reactant 0.659 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp147

+

2,3-dihydroxybenzoic acid

+

methylamine

+

4,7-dimethoxy-1-naphthaldehyde

Reaction ID UCEXP171A/V2B1

61



tosylmethyl isocyanide

21105839

Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.221 M Precipitate Yes Product Impurities found Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp171

+

2,3-dihydroxybenzoic acid

+

methylamine

+

4,7-dimethoxy-1-naphthaldehyde



tosylmethyl isocyanide

21105839

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCEXP173F/V2B18 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.219 M Precipitate no and aldehyde alone not solube Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp173

+

2,3-dihydroxybenzoic acid

+

furfurylamine

+

phenanthrene-9-carboxaldehyde



t-butyl isocyanide

21106041

Reaction ID UCEXP181-098V2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.226 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

+

2,3-dihydroxybenzoic acid

+

methylamine

+

4-hydroxybenzaldehyde



tosylmethyl isocyanide

24528129

Reaction ID UCEXP181-112V2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.224 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

+

2,3-dihydroxybenzoic acid

+

methylamine

+

4-methoxybenzaldehyde

Reaction ID UCEXP181-116V2 Researcher

Khalid Mirza

62



tosylmethyl isocyanide

24528141

Reaction Type Ugi Solvent methanol Limiting Reactant 0.225 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

+

2,3-dihydroxybenzoic acid

+

+

methylamine

4-chlorobenzaldehyde



tosylmethyl isocyanide

24528145

2,4-dimethylbenzaldehyde

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCEXP181-087V2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.222 M Precipitate Reactants Insoluble Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

+

1-pyrenebutyric acid

+

methylamine

+

2,4-dimethylbenzaldehyde



t-butyl isocyanide

21106206

Reaction ID UCExp236-18 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.858 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp236

+

3,3'-dichloropivalic acid

+

methylamine

+

2,4-dimethylbenzaldehyde



t-butyl isocyanide

24528291

Reaction ID UCExp236-27 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.617 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp236

+

3,3'-dichloropivalic acid

+

t-butylamine

+

2,4-dimethylbenzaldehyde

Reaction ID UCExp241-18

63



t-butyl isocyanide

24528300

Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.571 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp241

+

3,4methylenedioxyphenylacetic acid

+

methylamine

+

2,4-dimethylbenzaldehyde



t-butyl isocyanide

24528361

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCExp241-26 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.573 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp241

+

3,4methylenedioxyphenylacetic acid

+

methylamine

+

2,4-dimethylbenzaldehyde



n-butyl isocyanide

24528365

Reaction ID UCExp241-35 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.737 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp241

+

3,4methylenedioxyphenylacetic acid

+

t-butylamine

+

2,4-dimethylbenzaldehyde



t-butyl isocyanide

24528371

Reaction ID UCExp241-40 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.749 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp241

+

+

+

64



3,4methylenedioxyphenylacetic acid

1-propylamine

2,4-dimethylbenzaldehyde

t-butyl isocyanide

24528375

Reaction ID UCExp241-46 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.736 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp241

+

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

3,4methylenedioxyphenylacetic acid

+

3-chloroaniline

+

2,4-dimethylbenzaldehyde



t-butyl isocyanide

24528379

Reaction ID UCExp241-48 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.734 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp241

+

3,4methylenedioxyphenylacetic acid

+

benzylamine

+

2,4-dimethylbenzaldehyde



t-butyl isocyanide

24528381

2,4-dimethylbenzaldehyde Reaction ID UCEXP228-3 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.551 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp228

+

Boc-Trp-OH

+

octadecylamine

+

2,4-dimethylbenzaldehyde

2,4,6-trihydroxybenzoic acid Reaction ID UCEXP151-1V2B10 Researcher Mitesh Shah Reaction Type Ugi Solvent methanol Limiting Reactant 0.694 M Precipitate No

65



n-butyl isocyanide

24534188

Comments Reference

Protocol from Explan005 followed http://usefulchem.wikispaces.com/Exp151

+

2,4,6-trihydroxybenzoic acid

+

methylamine

+

3,4-dihydroxybenzaldehyde



tosylmethyl isocyanide

21106049

Reaction ID UCEXP171C/V2B3

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.222 M Precipitate Reactants Insoluble Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp171

+

2,4,6-trihydroxybenzoic acid

+

methylamine

+

phenanthrene-9-carboxaldehyde



tosylmethyl isocyanide

21106040

Reaction ID UCEXP171HV2B8 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.223 M Precipitate Yes Product No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp171

+

2,4,6-trihydroxybenzoic acid

+

methylamine

+

3,5-dimethoxybenzaldehyde



tosylmethyl isocyanide

21105832

Reaction ID UCEXP171JV2B10 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.225 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp171

+

2,4,6-trihydroxybenzoic acid

+

methylamine

+

3,4-dihydroxybenzaldehyde

Reaction ID UCEXP174H/V2B40 Researcher Reaction Type Solvent

Khalid Mirza Ugi methanol

66



tosylmethyl isocyanide

21106049

Limiting Reactant 0.223 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp174

+

2,4,6-trihydroxybenzoic acid

+

+

methylamine

2-naphthaldehyde



tosylmethyl isocyanide

21106188

Reaction ID UCEXP174L/V2B44

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.224 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp174

+

2,4,6-trihydroxybenzoic acid

+

methylamine

+

4-methoxybenzaldehyde



tosylmethyl isocyanide

21106195

Reaction ID UCEXP181-056V2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.219 M Precipitate Reactants Insoluble Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

+

2,4,6-trihydroxybenzoic acid

+

furfurylamine

+

phenanthrene-9-carboxaldehyde



n-butyl isocyanide

24528097

Reaction ID UCEXP181-066V2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.225 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

+

2,4,6-trihydroxybenzoic acid

+

methylamine

+

3-hydroxybenzaldehyde

Reaction ID UCEXP181-069V2 Researcher Reaction Type

Khalid Mirza Ugi

67



tosylmethyl isocyanide

24528105

Solvent methanol Limiting Reactant 0.221 M Precipitate Reactants Insoluble Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

+

2,4,6-trihydroxybenzoic acid

+

+

aniline

2-naphthaldehyde



tosylmethyl isocyanide

24528108

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCEXP181-077V2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.225 M Precipitate Reactants Insoluble Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

+

2,4,6-trihydroxybenzoic acid

+

5-methylfurfurylamine

+

3-methoxybenzaldehyde



n-butyl isocyanide

24528113

Reaction ID UCEXP181-079V2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.218 M Precipitate Reactants Insoluble Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

+

2,4,6-trihydroxybenzoic acid

+

furfurylamine

+

phenanthrene-9-carboxaldehyde



t-butyl isocyanide

24528115

Reaction ID UCEXP181-080V2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.221 M Precipitate Yes Product Not determined Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

+

2,4,6-trihydroxybenzoic acid

+

aniline

Reaction ID UCEXP181-101V2

+

3-methoxybenzaldehyde

68



tosylmethyl isocyanide

24528116

Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.221 M Precipitate Reactants Insoluble Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

+

2,4,6-trihydroxybenzoic acid

+

methylamine

+

4,7-dimethoxy-1-naphthaldehyde



tosylmethyl isocyanide

24528132

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCEXP181-111V2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.226 M Precipitate Reactants Insoluble Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

+

2,4,6-trihydroxybenzoic acid

+

methylamine

+

phenanthrene-9-carboxaldehyde



t-butyl isocyanide

24528534

Reaction ID UCEXP181-114V2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.223 M Precipitate Reactants Insoluble Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

+

2,4,6-trihydroxybenzoic acid

+

5-methylfurfurylamine

+

phenanthrene-9-carboxaldehyde



n-butyl isocyanide

24528143

Reaction ID UCEXP181-117V2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.22 M Precipitate Reactants Insoluble Comments Protocol from Explan005 followed; hydrate of acid used Reference http://usefulchem.wikispaces.com/Exp181

+

2,4,6-trihydroxybenzoic acid

+

furfurylamine

+

veratraldehyde

69



tosylmethyl isocyanide

24534442

Reaction ID UCEXP181-120V2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.222 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

+

2,4,6-trihydroxybenzoic acid

+

+

3,5Bis(trifluoromethyl)benzaldehyde

methylamine



tosylmethyl isocyanide

24528149

2,5-dimethoxyphenylacetic acid Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCEXP174T/V2B53 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.219 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp174

+

2,5-dimethoxyphenylacetic acid

+

aniline

+

2-hydroxybenzaldehyde



tosylmethyl isocyanide

21106185

Reaction ID UCEXP181-085V2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.219 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

+

2,5-dimethoxyphenylacetic acid

+

3-chloroaniline

+

2-hydroxybenzaldehyde

2,6-dihydroxybenzoic acid Reaction ID UCEXP181-055V2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.223 M Precipitate no and aldehyde alone not solube Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

70



tosylmethyl isocyanide

24528120

+

2,6-dihydroxybenzoic acid

+

5-methylfurfurylamine

+

phenanthrene-9-carboxaldehyde



n-butyl isocyanide

24528096

Reaction ID UCEXP181-072V2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.224 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

+

2,6-dihydroxybenzoic acid

+

methylamine

+

4-(trifluoromethyl)benzaldehyde



tosylmethyl isocyanide

21106207

3-(4-methoxyphenyl)propionic acid Reaction ID UCEXP155B-V1B159 Researcher Emily Messner Reaction Type Ugi Solvent methanol Limiting Reactant 0.674 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp155

+

3-(4methoxyphenyl)propionic acid

+

+

5-methylfurfurylamine

benzaldehyde



t-butyl isocyanide

21106074

Reaction ID UCEXP181-124V2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.219 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

+

3-(4methoxyphenyl)propionic acid

+

benzylamine

+

2-hydroxybenzaldehyde

3-chloroaniline 71



tosylmethyl isocyanide

24528152

Reaction ID UCEXP171EV2B5 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.22 M Precipitate Reactants Insoluble Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp171

+

3,4methylenedioxyphenylacetic acid

+

3-chloroaniline

+

2-hydroxybenzaldehyde



tosylmethyl isocyanide

21106047

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCEXP174M/V2B45 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.22 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp174

+

2-phenylbutyric acid

+

3-chloroaniline

+

3,4-dihydroxybenzaldehyde



tosylmethyl isocyanide

21106194

Reaction ID UCEXP174Q/V2B50 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.222 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp174

+

butyric acid

+

3-chloroaniline

+

2-hydroxybenzaldehyde



tosylmethyl isocyanide

21106191

Reaction ID UCEXP174R/V2B51 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.221 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp174

+

mandelic acid

+

3-chloroaniline

+

2-hydroxybenzaldehyde

72



tosylmethyl isocyanide

21106190

Reaction ID UCEXP181-070V2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.22 M Precipitate Reactants Insoluble Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

+

1-pyrenebutyric acid

+

+

3-chloroaniline

2-methylbenzaldehyde



n-butyl isocyanide

24528530

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCEXP181-085V2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.219 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

+

2,5-dimethoxyphenylacetic acid

+

3-chloroaniline

+

2-hydroxybenzaldehyde



tosylmethyl isocyanide

24528120

Reaction ID UCEXP181-089V2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.221 M Precipitate Reactants Insoluble Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

+

hexanoic acid

+

3-chloroaniline

+

2-hydroxybenzaldehyde



tosylmethyl isocyanide

24528122

Reaction ID UCEXP181-113V2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.219 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

+

3,4-dihydroxyphenylacetic acid

+

3-chloroaniline

+

veratraldehyde

73



tosylmethyl isocyanide

24528142

Reaction ID UCEXP181-115V2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.224 M Precipitate Reactants Insoluble Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

+

3,4-dihydroxyphenylacetic acid

+

+

3-chloroaniline

2-naphthaldehyde



t-butyl isocyanide

24528144

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCEXP181-121V2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.221 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

+

4-chlorophenylacetic acid

+

3-chloroaniline

+

3,4-dihydroxybenzaldehyde



tosylmethyl isocyanide

24528150

Reaction ID UCEXP215G Researcher Khalid Mirza Reaction Type Ugi Solvent THF + methanol Limiting Reactant 0.291 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp215

+

chloroacetic acid

+

+

5-bromo-2thiophenecarboxaldehyde

3-chloroaniline



benzyl isocyanide

24528156

Reaction ID UCExp236-02 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.614 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp236

+

3,3'-dichloropivalic acid

+

3-chloroaniline

+

4-(trifluoromethyl)benzaldehyde

74



n-butyl isocyanide

24528276

Reaction ID UCExp236-08 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.65 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp236

+

formic acid

+

3-chloroaniline

+

4-(trifluoromethyl)benzaldehyde



t-butyl isocyanide

24528281

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCExp236-23 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.631 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp236

+

methacrylic acid

+

3-chloroaniline

+

4-(trifluoromethyl)benzaldehyde



n-butyl isocyanide

24528296

Reaction ID UCExp236-25 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.615 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp236

+

3,3'-dichloropivalic acid

+

+

5-bromo-2thiophenecarboxaldehyde

3-chloroaniline



t-butyl isocyanide

24528298

Reaction ID UCExp238-02 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.879 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp238

+

crotonic acid

+

3-chloroaniline

+

phenanthrene-9-carboxaldehyde

Reaction ID UCExp238-14

75



cyclohexylisocyanide

24528304

Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.919 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp238

+

crotonic acid

+

3-chloroaniline

+

phenanthrene-9-carboxaldehyde



t-butyl isocyanide

24528316

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCExp238-26 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.684 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp238

+

Boc-Gly-OH

+

3-chloroaniline

+

phenanthrene-9-carboxaldehyde



cyclohexylisocyanide

24528326

Reaction ID UCExp238-38 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.716 M Precipitate Yes but solvent evaporated Comments Reference http://usefulchem.wikispaces.com/Exp238

+

Boc-Gly-OH

+

3-chloroaniline

+

phenanthrene-9-carboxaldehyde



t-butyl isocyanide

24528338

Reaction ID UCExp241-33 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.747 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp241

+

3,4methylenedioxyphenylacetic acid

+

3-chloroaniline

+

5-bromo-2thiophenecarboxaldehyde

Reaction ID UCExp241-46

76



t-butyl isocyanide

24528370

Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.736 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp241

+

3,4methylenedioxyphenylacetic acid

+

3-chloroaniline

+

2,4-dimethylbenzaldehyde



t-butyl isocyanide

24528379

3-hydroxybenzaldehyde Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCEXP173I/V3B21 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.225 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp173

+

3,4-dihydroxyphenylacetic acid

+

methylamine

+

3-hydroxybenzaldehyde



tosylmethyl isocyanide

21106052

Reaction ID UCEXP173L/V2B24 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.221 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp173

+

3,4-dihydroxyphenylacetic acid

+

furfurylamine

+

3-hydroxybenzaldehyde



tosylmethyl isocyanide

21106051

Reaction ID UCEXP174N/V2B46 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.223 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp174

+

+

+

77



Boc-Trp-OH

methylamine

3-hydroxybenzaldehyde

n-butyl isocyanide

21106193

Reaction ID UCEXP181-066V2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.225 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

+

+

2,4,6-trihydroxybenzoic acid

methylamine

+

3-hydroxybenzaldehyde



tosylmethyl isocyanide

24528105

Reaction ID UCEXP181-086V2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.225 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

+

+

4-hydroxybenzoic acid

methylamine

+

3-hydroxybenzaldehyde



tosylmethyl isocyanide

24528121

Reaction ID UCEXP181-102V2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.221 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

+

3,4-dihydroxyphenylacetic acid

+

5-methylfurfurylamine

+

3-hydroxybenzaldehyde

3-hydroxybenzaldehyde Reaction ID UCEXP228-2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.265 M

78



tosylmethyl isocyanide

24528533

Precipitate Comments Reference

No Protocol from Explan005 followed http://usefulchem.wikispaces.com/Exp228

+

+

Boc-Trp-OH

octadecylamine

+

3-hydroxybenzaldehyde



n-butyl isocyanide

24528182

3-methoxybenzaldehyde

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCEXP173P/V2B28 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.222 M Precipitate Reactants Insoluble Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp173

+

+

1-pyrenebutyric acid

methylamine

+

3-methoxybenzaldehyde



t-butyl isocyanide

21106050

Reaction ID UCEXP174B/V2B33 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.22 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp174

+

+

3,4-dihydroxyphenylacetic acid

furfurylamine

+

3-methoxybenzaldehyde



tosylmethyl isocyanide

21106204

Reaction ID UCEXP174P/V2B49 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.22 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp174

+

3,4-dihydroxyphenylacetic acid

+

5-methylfurfurylamine

+

3-methoxybenzaldehyde

Reaction ID UCEXP181-077V2 Researcher

Khalid Mirza

79



tosylmethyl isocyanide

21106192

Reaction Type Ugi Solvent methanol Limiting Reactant 0.225 M Precipitate Reactants Insoluble Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

+

2,4,6-trihydroxybenzoic acid

+

5-methylfurfurylamine

+

3-methoxybenzaldehyde



n-butyl isocyanide

24528113

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCEXP181-080V2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.221 M Precipitate Yes Product Not determined Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

+

2,4,6-trihydroxybenzoic acid

+

aniline

+

3-methoxybenzaldehyde



tosylmethyl isocyanide

24528116

Reaction ID UCEXP181-084V2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.225 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

+

mandelic acid

+

benzylamine

+

3-methoxybenzaldehyde



n-butyl isocyanide

24528119

Reaction ID UCEXP181-092V2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.217 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

+

decanoic acid

+

2-chloroaniline

+

3-methoxybenzaldehyde

Reaction ID UCEXP181-096V2

80



tosylmethyl isocyanide

24528124

Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.224 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

+

4-hydroxybenzoic acid

+

methylamine

+

3-methoxybenzaldehyde



tosylmethyl isocyanide

24528127

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCEXP181-109V2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.22 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

+

4-hydroxybenzoic acid

+

1-hexylamine

+

3-methoxybenzaldehyde



tosylmethyl isocyanide

24528139

3-methylbut-2-enoic acid Reaction ID UCEXP181-064V2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.221 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

+

3-methylbut-2-enoic acid

+

1-hexylamine

+

3,4-dihydroxybenzaldehyde



tosylmethyl isocyanide

24528103

3,3'-dichloropivalic acid Reaction ID UCExp236-01 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.614 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp236

+

+

+

81



3,3'-dichloropivalic acid

t-butylamine

4-(trifluoromethyl)benzaldehyde

n-butyl isocyanide

24528275

Reaction ID UCExp236-02 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.614 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp236

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

+

3,3'-dichloropivalic acid

+

3-chloroaniline

+

4-(trifluoromethyl)benzaldehyde



n-butyl isocyanide

24528276

Reaction ID UCExp236-03 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.614 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp236

+

3,3'-dichloropivalic acid

+

benzylamine

+

4-(trifluoromethyl)benzaldehyde



n-butyl isocyanide

24528277

Reaction ID UCExp236-07 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.614 M Precipitate Yes Yield - % Comments Reference http://usefulchem.wikispaces.com/Exp236

+

3,3'-dichloropivalic acid

+

1-hexylamine

+

4-(trifluoromethyl)benzaldehyde

Reaction ID UCExp236-09 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.614 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp236

82



t-butyl isocyanide

24528280

+

3,3'-dichloropivalic acid

+

2-chloroaniline

+

4-(trifluoromethyl)benzaldehyde



t-butyl isocyanide

24528282

Reaction ID UCExp236-13 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.614 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp236

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

+

3,3'-dichloropivalic acid

+

1-propylamine

+

4-(trifluoromethyl)benzaldehyde



n-butyl isocyanide

24528286

Reaction ID UCExp236-14 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.856 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp236

+

3,3'-dichloropivalic acid

+

+

5-bromo-2thiophenecarboxaldehyde

methylamine



t-butyl isocyanide

24528287

Reaction ID UCExp236-15 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.614 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp236

+

3,3'-dichloropivalic acid

+

1-heptylamine

+

4-(trifluoromethyl)benzaldehyde

Reaction ID UCExp236-17 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.614 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp236

83



t-butyl isocyanide

24528288

+

+

3,3'-dichloropivalic acid

aniline

+

4-(trifluoromethyl)benzaldehyde



n-butyl isocyanide

24528290

Reaction ID UCExp236-18 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.858 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp236

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

+

3,3'-dichloropivalic acid

+

methylamine

+

2,4-dimethylbenzaldehyde



t-butyl isocyanide

24528291

Reaction ID UCExp236-22 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.614 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp236

+

3,3'-dichloropivalic acid

+

+

5-bromo-2thiophenecarboxaldehyde

t-butylamine



t-butyl isocyanide

24528295

Reaction ID UCExp236-25 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.615 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp236

+

3,3'-dichloropivalic acid

+

3-chloroaniline

+

5-bromo-2thiophenecarboxaldehyde

Reaction ID UCExp236-26 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.612 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp236

84



t-butyl isocyanide

24528298

+

3,3'-dichloropivalic acid

+

+

5-bromo-2thiophenecarboxaldehyde

benzylamine



t-butyl isocyanide

24528299

Reaction ID UCExp236-27 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.617 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp236

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

+

3,3'-dichloropivalic acid

+

t-butylamine

+

2,4-dimethylbenzaldehyde



t-butyl isocyanide

24528300

Reaction ID UCExp236-29 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.614 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp236

+

3,3'-dichloropivalic acid

+

cyclohexylamine

+

4-(trifluoromethyl)benzaldehyde



t-butyl isocyanide

24528302

3,4-dihydroxybenzaldehyde Reaction ID UCEXP151-1V2B10 Researcher Mitesh Shah Reaction Type Ugi Solvent methanol Limiting Reactant 0.694 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp151

+

2,4,6-trihydroxybenzoic acid

+

methylamine

+

3,4-dihydroxybenzaldehyde

Reaction ID UCEXP171JV2B10 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.225 M

85



tosylmethyl isocyanide

21106049

Precipitate Comments Reference

No Protocol from Explan005 followed http://usefulchem.wikispaces.com/Exp171

+

2,4,6-trihydroxybenzoic acid

+

methylamine

+

3,4-dihydroxybenzaldehyde



tosylmethyl isocyanide

21106049

Reaction ID UCEXP173E/V2B17

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.223 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp173

+

Boc-Trp-OH

+

methylamine

+

3,4-dihydroxybenzaldehyde



t-butyl isocyanide

21106045

Reaction ID UCEXP173J/V2B22 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.224 M Precipitate Reactants Insoluble Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp173

+

1-pyrenebutyric acid

+

methylamine

+

3,4-dihydroxybenzaldehyde



t-butyl isocyanide

21106038

Reaction ID UCEXP174I/V2B41 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.224 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp174

+

methacrylic acid

+

aniline

+

3,4-dihydroxybenzaldehyde

Reaction ID UCEXP174M/V2B45 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.22 M Precipitate No

86



tosylmethyl isocyanide

21106198

Comments Reference

Protocol from Explan005 followed http://usefulchem.wikispaces.com/Exp174

+

2-phenylbutyric acid

+

3-chloroaniline

+

3,4-dihydroxybenzaldehyde



tosylmethyl isocyanide

21106194

Reaction ID UCEXP181-064V2

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.221 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

+

3-methylbut-2-enoic acid

+

1-hexylamine

+

3,4-dihydroxybenzaldehyde



tosylmethyl isocyanide

24528103

Reaction ID UCEXP181-074V2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.226 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

+

3,4-dihydroxyphenylacetic acid

+

aniline

+

3,4-dihydroxybenzaldehyde



t-butyl isocyanide

24528110

Reaction ID UCEXP181-076V2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.224 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

+

diphenylacetic acid

+

1-propylamine

+

3,4-dihydroxybenzaldehyde

Reaction ID UCEXP181-082V2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.221 M Precipitate No Comments Protocol from Explan005 followed

87



n-butyl isocyanide

24528112

Reference

http://usefulchem.wikispaces.com/Exp181

+

3,4-dihydroxyphenylacetic acid

+

furfurylamine

+

3,4-dihydroxybenzaldehyde



tosylmethyl isocyanide

24528118

Reaction ID UCEXP181-088V2

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.222 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

+

diphenylacetic acid

+

5-methylfurfurylamine

+

3,4-dihydroxybenzaldehyde



n-butyl isocyanide

24528532

Reaction ID UCEXP181-090V2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.226 M Precipitate Reactants Insoluble Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

+

4-nitrobenzoic acid

+

methylamine

+

3,4-dihydroxybenzaldehyde



tosylmethyl isocyanide

24528123

Reaction ID UCEXP181-105V2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.221 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

+

4-chlorophenylacetic acid

+

t-butylamine

+

3,4-dihydroxybenzaldehyde

Reaction ID UCEXP181-119V2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.226 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

88



tosylmethyl isocyanide

24528135

+

+

diphenylacetic acid

methylamine

+

3,4-dihydroxybenzaldehyde



n-butyl isocyanide

24528148

Reaction ID UCEXP181-121V2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.221 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

+

+

4-chlorophenylacetic acid

3-chloroaniline

+

3,4-dihydroxybenzaldehyde



tosylmethyl isocyanide

24528150

3,4-dihydroxyphenyl acetic acid Reaction ID UCEXP174J/V2B42 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.221 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp174

+

3,4-dihydroxyphenyl acetic acid

+

+

5-methylfurfurylamine

4-chlorobenzaldehyde



tosylmethyl isocyanide

21106197

3,4-dihydroxyphenylacetic acid Reaction ID UCEXP160C-V1B19 Researcher Emily Messner Reaction Type Ugi Solvent methanol Limiting Reactant 0.388 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp160

+

3,4-dihydroxyphenylacetic acid

+

furfurylamine

+

phenanthrene-9-carboxaldehyde

Reaction ID UCEXP171GV2B7 Researcher

Khalid Mirza

89



n-butyl isocyanide

21105579

Reaction Type Ugi Solvent methanol Limiting Reactant 0.218 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp171

+

3,4-dihydroxyphenylacetic acid

+

+

furfurylamine

2-naphthaldehyde



tosylmethyl isocyanide

21106054

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCEXP173H/V2B20 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.22 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp173

+

3,4-dihydroxyphenylacetic acid

+

+

5-methylfurfurylamine

2-naphthaldehyde



tosylmethyl isocyanide

21106053

Reaction ID UCEXP173I/V3B21 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.225 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp173

+

3,4-dihydroxyphenylacetic acid

+

methylamine

+

3-hydroxybenzaldehyde



tosylmethyl isocyanide

21106052

Reaction ID UCEXP173L/V2B24 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.221 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp173

+

3,4-dihydroxyphenylacetic acid

+

furfurylamine

+

3-hydroxybenzaldehyde

Reaction ID UCEXP173M/V2B25

90



tosylmethyl isocyanide

21106051

Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.22 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp173

+

3,4-dihydroxyphenylacetic acid

+

furfurylamine

+

4-chlorobenzaldehyde



tosylmethyl isocyanide

21106043

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCEXP173O/V2B27 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.222 M Precipitate Yes Product pending Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp173

+

3,4-dihydroxyphenylacetic acid

+

furfurylamine

+

benzaldehyde



tosylmethyl isocyanide

21105843

Reaction ID UCEXP173Q/V2B29 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.22 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp173

+

3,4-dihydroxyphenylacetic acid

+

furfurylamine

+

4-methylbenzaldehyde



tosylmethyl isocyanide

21106042

Reaction ID UCEXP174A/V2B31 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.221 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp174

+

3,4-dihydroxyphenylacetic acid

+

5-methylfurfurylamine

+

benzaldehyde

91



tosylmethyl isocyanide

21106189

Reaction ID UCEXP174B/V2B33 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.22 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp174

+

3,4-dihydroxyphenylacetic acid

+

furfurylamine

+

3-methoxybenzaldehyde



tosylmethyl isocyanide

21106204

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCEXP174F/V2B38 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.222 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp174

+

3,4-dihydroxyphenylacetic acid

+

methylamine

+

veratraldehyde



tosylmethyl isocyanide

21106200

Reaction ID UCEXP174G/V2B39 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.222 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp174

+

3,4-dihydroxyphenylacetic acid

+

1-propylamine

+

4-methylbenzaldehyde



tosylmethyl isocyanide

21106199

Reaction ID UCEXP174P/V2B49 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.22 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp174

+

+

+

3,4-dihydroxyphenylacetic

92



5-methylfurfurylamine

acid

3-methoxybenzaldehyde

tosylmethyl isocyanide

21106192

Reaction ID UCEXP174U/V2B54 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.22 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp174

+

3,4-dihydroxyphenylacetic acid

+

furfurylamine

+

4-methoxybenzaldehyde



tosylmethyl isocyanide

21106187

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCEXP181-063V2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.222 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

+

3,4-dihydroxyphenylacetic acid

+

1-propylamine

+

2-hydroxybenzaldehyde



tosylmethyl isocyanide

24528102

Reaction ID UCEXP181-067V2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.221 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

+

3,4-dihydroxyphenylacetic acid

+

furfurylamine

+

4-hydroxybenzaldehyde



tosylmethyl isocyanide

24528106

Reaction ID UCEXP181-068V2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.224 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

+

+

+

93



3,4-dihydroxyphenylacetic acid

methylamine

o-vanillin

tosylmethyl isocyanide

24528107

Reaction ID UCEXP181-074V2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.226 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

+

3,4-dihydroxyphenylacetic acid

+

aniline

+

3,4-dihydroxybenzaldehyde



t-butyl isocyanide

24528110

Reaction ID UCEXP181-081V2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.224 M Precipitate Reactants Insoluble Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

+

3,4-dihydroxyphenylacetic acid

+

+

2-chloroaniline

2-naphthaldehyde



t-butyl isocyanide

24528117

Reaction ID UCEXP181-082V2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.221 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

+

3,4-dihydroxyphenylacetic acid

+

furfurylamine

+

3,4-dihydroxybenzaldehyde

Reaction ID UCEXP181-094V2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.217 M Precipitate No Comments Protocol from Explan005 followed

94



tosylmethyl isocyanide

24528118

Reference

http://usefulchem.wikispaces.com/Exp181

+

+

3,4-dihydroxyphenylacetic acid

furfurylamine

+

3,5-dimethoxybenzaldehyde



tosylmethyl isocyanide

24528126

Reaction ID UCEXP181-097V2

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.221 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

+

+

3,4-dihydroxyphenylacetic acid

furfurylamine

+

2-hydroxybenzaldehyde



tosylmethyl isocyanide

24528128

Reaction ID UCEXP181-102V2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.221 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

+

3,4-dihydroxyphenylacetic acid

+

5-methylfurfurylamine

+

3-hydroxybenzaldehyde



tosylmethyl isocyanide

24528533

Reaction ID UCEXP181-110V2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.222 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

+

3,4-dihydroxyphenylacetic acid

+

aniline

+

2-hydroxybenzaldehyde

Reaction ID UCEXP181-113V2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.219 M Precipitate No

95



tosylmethyl isocyanide

24528140

Comments Reference

Protocol from Explan005 followed http://usefulchem.wikispaces.com/Exp181

+

3,4-dihydroxyphenylacetic acid

+

+

3-chloroaniline

veratraldehyde



tosylmethyl isocyanide

24528142

Reaction ID UCEXP181-115V2

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.224 M Precipitate Reactants Insoluble Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

+

3,4-dihydroxyphenylacetic acid

+

+

3-chloroaniline

2-naphthaldehyde



t-butyl isocyanide

24528144

Reaction ID UCEXP181-118V2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.224 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

+

3,4-dihydroxyphenylacetic acid

+

+

5-bromo-2thiophenecarboxaldehyde

methylamine



tosylmethyl isocyanide

24528147

Reaction ID UCEXP181-123V2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.214 M Precipitate no and aldehyde alone not solube Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

+

3,4-dihydroxyphenylacetic acid

+

furfurylamine

+

phenanthrene-9-carboxaldehyde

3,4-methylenedioxyphenylacetic acid Reaction ID UCEXP167A-V1B12

96



tosylmethyl isocyanide

24528151

Researcher Tim Bohinsky Reaction Type Ugi Solvent methanol Limiting Reactant 0.403 M Precipitate Reactants Insoluble Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp167

+

3,4methylenedioxyphenylacetic acid

+

1-propylamine

+

phenanthrene-9-carboxaldehyde



n-butyl isocyanide

21105597

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCEXP171EV2B5 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.22 M Precipitate Reactants Insoluble Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp171

+

3,4methylenedioxyphenylacetic acid

+

3-chloroaniline

+

2-hydroxybenzaldehyde



tosylmethyl isocyanide

21106047

Reaction ID UCEXP171IV2B9 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.221 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp171

+

3,4methylenedioxyphenylacetic acid

+

aniline

+

2-hydroxybenzaldehyde



tosylmethyl isocyanide

21106055

Reaction ID UCExp241-01 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.502 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp241

+

+

+

97



3,4methylenedioxyphenylacetic acid

methylamine

4-methoxybenzaldehyde

benzyl isocyanide

24534407

Reaction ID UCExp241-02 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.502 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp241

+

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

3,4methylenedioxyphenylacetic acid

+

methylamine

+

m-anisaldehyde



benzyl isocyanide

24534408

Reaction ID UCExp241-03 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.512 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp241

+

3,4methylenedioxyphenylacetic acid

+

methylamine

+

2-furaldehyde



benzyl isocyanide

24534403

Reaction ID UCExp241-04 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.525 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp241

+

3,4methylenedioxyphenylacetic acid

+

methylamine

+

veratraldehyde

Reaction ID UCExp241-05 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.525 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp241

98



n-butyl isocyanide

24528355

+

3,4methylenedioxyphenylacetic acid

+

methylamine

+

veratraldehyde



n-butyl isocyanide

24528355

Reaction ID UCExp241-06

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.523 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp241

+

3,4methylenedioxyphenylacetic acid

+

methylamine

+

veratraldehyde



t-butyl isocyanide

24528356

Reaction ID UCExp241-07 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.523 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp241

+

3,4methylenedioxyphenylacetic acid

+

methylamine

+

veratraldehyde



t-butyl isocyanide

24528356

Reaction ID UCExp241-08 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.52 M Precipitate YES Yield - % Comments Reference http://usefulchem.wikispaces.com/Exp241

+

3,4methylenedioxyphenylacetic acid

+

methylamine

+

veratraldehyde

Reaction ID UCExp241-09 Researcher

Khalid Mirza

99



cyclohexylisocyanide

21782465

Reaction Type Ugi Solvent methanol Limiting Reactant 0.564 M Precipitate YES Yield - % Comments Reference http://usefulchem.wikispaces.com/Exp241

+

3,4methylenedioxyphenylacetic acid

+

methylamine

+

veratraldehyde



cyclohexylisocyanide

21782465

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCExp241-10 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.548 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp241

+

3,4methylenedioxyphenylacetic acid

+

methylamine

+



1,1,3,3tetramethylbutyl isocyanide

veratraldehyde

24528357

Reaction ID UCExp241-11 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.548 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp241

+

3,4methylenedioxyphenylacetic acid

+

methylamine

+



1,1,3,3tetramethylbutyl isocyanide

veratraldehyde

24528357

Reaction ID UCExp241-12 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.563 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp241

+

+

+

100



3,4methylenedioxyphenylacetic acid

methylamine

veratraldehyde

1-pentyl isocyanide

24528358

Reaction ID UCExp241-13

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.563 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp241

+

3,4methylenedioxyphenylacetic acid

+

methylamine

+

veratraldehyde



1-pentyl isocyanide

24528358

Reaction ID UCExp241-14 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.565 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp241

+

3,4methylenedioxyphenylacetic acid

+

methylamine

+

veratraldehyde



benzyl isocyanide

24528359

Reaction ID UCExp241-15 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.565 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp241

+

3,4methylenedioxyphenylacetic acid

+

methylamine

+

veratraldehyde

Reaction ID UCExp241-16 Researcher Reaction Type

Khalid Mirza Ugi

101



benzyl isocyanide

24528359

Solvent methanol Limiting Reactant 0.565 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp241

+

3,4methylenedioxyphenylacetic acid

+

+

methylamine

veratraldehyde



benzyl isocyanide

24528359

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCExp241-17 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.577 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp241

+

3,4methylenedioxyphenylacetic acid

+

+

5-bromo-2thiophenecarboxaldehyde

methylamine



t-butyl isocyanide

24528360

Reaction ID UCExp241-18 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.571 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp241

+

3,4methylenedioxyphenylacetic acid

+

methylamine

+

2,4-dimethylbenzaldehyde



t-butyl isocyanide

24528361

Reaction ID UCExp241-21 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.576 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp241

+

3,4methylenedioxyphenylacetic acid

+

methylamine

+

4-methylbenzaldehyde

102



t-butyl isocyanide

24528362

Reaction ID UCExp241-22 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.578 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp241

+

3,4methylenedioxyphenylacetic acid

+

+

methylamine

o-tolualdehyde



t-butyl isocyanide

24528363

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCExp241-23 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.559 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp241

+

3,4methylenedioxyphenylacetic acid

+

+

5-bromo-2thiophenecarboxaldehyde

methylamine



n-butyl isocyanide

24528364

Reaction ID UCExp241-26 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.573 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp241

+

3,4methylenedioxyphenylacetic acid

+

methylamine

+

2,4-dimethylbenzaldehyde



n-butyl isocyanide

24528365

Reaction ID UCExp241-29 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.729 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp241

+

+

+

103



3,4methylenedioxyphenylacetic acid

1-hexylamine

4-(trifluoromethyl)benzaldehyde

n-butyl isocyanide

24528366

Reaction ID UCExp241-30

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.717 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp241

+

3,4methylenedioxyphenylacetic acid

+

+

5-bromo-2thiophenecarboxaldehyde

butylamine



t-butyl isocyanide

24528367

Reaction ID UCExp241-31 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.743 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp241

+

3,4methylenedioxyphenylacetic acid

+

2-chloroaniline

+

4-(trifluoromethyl)benzaldehyde



n-butyl isocyanide

24528368

Reaction ID UCExp241-32 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.751 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp241

+

3,4methylenedioxyphenylacetic acid

+

aniline

+

4-(trifluoromethyl)benzaldehyde

Reaction ID UCExp241-33 Researcher Reaction Type

Khalid Mirza Ugi

104



n-butyl isocyanide

24528369

Solvent methanol Limiting Reactant 0.747 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp241

+

3,4methylenedioxyphenylacetic acid

+

+

5-bromo-2thiophenecarboxaldehyde

3-chloroaniline



t-butyl isocyanide

24528370

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCExp241-35 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.737 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp241

+

3,4methylenedioxyphenylacetic acid

+

t-butylamine

+

2,4-dimethylbenzaldehyde



t-butyl isocyanide

24528371

Reaction ID UCExp241-37 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.733 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp241

+

3,4methylenedioxyphenylacetic acid

+

cyclohexylamine

+

4-(trifluoromethyl)benzaldehyde



t-butyl isocyanide

24528373

Reaction ID UCExp241-39 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.721 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp241

+

3,4methylenedioxyphenylacetic acid

+

aniline

+

5-bromo-2thiophenecarboxaldehyde

105



t-butyl isocyanide

24528374

Reaction ID UCExp241-40 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.749 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp241

+

3,4methylenedioxyphenylacetic acid

+

1-propylamine

+

2,4-dimethylbenzaldehyde



t-butyl isocyanide

24528375

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCExp241-43 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.71 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp241

+

3,4methylenedioxyphenylacetic acid

+

furfurylamine

+

4-(trifluoromethyl)benzaldehyde



t-butyl isocyanide

24528376

Reaction ID UCExp241-44 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.72 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp241

+

3,4methylenedioxyphenylacetic acid

+

1-heptylamine

+

4-(trifluoromethyl)benzaldehyde



n-butyl isocyanide

24528377

Reaction ID UCExp241-45 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.748 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp241

+

+

+

106



3,4methylenedioxyphenylacetic acid

5-bromo-2thiophenecarboxaldehyde

t-butylamine

t-butyl isocyanide

24528378

Reaction ID UCExp241-46

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.736 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp241

+

3,4methylenedioxyphenylacetic acid

+

3-chloroaniline

+

2,4-dimethylbenzaldehyde



t-butyl isocyanide

24528379

Reaction ID UCExp241-47 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.715 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp241

+

3,4methylenedioxyphenylacetic acid

+

1-heptylamine

+

4-(trifluoromethyl)benzaldehyde



t-butyl isocyanide

24528380

Reaction ID UCExp241-48 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.734 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp241

+

3,4methylenedioxyphenylacetic acid

+

benzylamine

+

2,4-dimethylbenzaldehyde

Reaction ID UCExp245-01 Researcher Reaction Type

Khalid Mirza Ugi

107



t-butyl isocyanide

24528381

Solvent methanol Limiting Reactant 0.509 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp245

+

3,4methylenedioxyphenylacetic acid

+

furfurylamine

+

piperonal



n-butyl isocyanide

24528391

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCExp245-02 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.718 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp245

+

3,4methylenedioxyphenylacetic acid

+

furfurylamine

+

piperonal



n-butyl isocyanide

24528391

Reaction ID UCExp245-03 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.504 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp245

+

3,4methylenedioxyphenylacetic acid

+

5-methylfurfurylamine

+

piperonal



n-butyl isocyanide

24528392

Reaction ID UCExp245-04 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.706 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp245

+

3,4methylenedioxyphenylacetic acid

+

5-methylfurfurylamine

+

piperonal

108



n-butyl isocyanide

24528392

Reaction ID UCExp245-05 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.507 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp245

+

3,4methylenedioxyphenylacetic acid

+

furfurylamine

+

piperonal



t-butyl isocyanide

24528393

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCExp245-06 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.714 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp245

+

3,4methylenedioxyphenylacetic acid

+

furfurylamine

+

piperonal



t-butyl isocyanide

24528393

Reaction ID UCExp245-07 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.504 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp245

+

3,4methylenedioxyphenylacetic acid

+

furfurylamine

+

piperonal



cyclohexylisocyanide

24528394

Reaction ID UCExp245-08 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.708 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp245

+

+

+

109



3,4methylenedioxyphenylacetic acid

furfurylamine

piperonal

cyclohexylisocyanide

24528394

Reaction ID UCExp245-09

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.492 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp245

+

+

3,4methylenedioxyphenylacetic acid

furfurylamine

+



1,1,3,3tetramethylbutyl isocyanide

piperonal

24528395

Reaction ID UCExp245-10 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.683 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp245

+

+

3,4methylenedioxyphenylacetic acid

furfurylamine

+



1,1,3,3tetramethylbutyl isocyanide

piperonal

24528395

Reaction ID UCExp245-11 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.504 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp245

+

3,4methylenedioxyphenylacetic acid

+

5-methylfurfurylamine

+

piperonal

Reaction ID UCExp245-12 Researcher Reaction Type

Khalid Mirza Ugi

110



t-butyl isocyanide

24528396

Solvent methanol Limiting Reactant 0.706 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp245

+

3,4methylenedioxyphenylacetic acid

+

5-methylfurfurylamine

+

piperonal



t-butyl isocyanide

24528396

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCExp245-13 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.499 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp245

+

3,4methylenedioxyphenylacetic acid

+

5-methylfurfurylamine

+

piperonal



cyclohexylisocyanide

24528397

Reaction ID UCExp245-14 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.696 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp245

+

3,4methylenedioxyphenylacetic acid

+

5-methylfurfurylamine

+

piperonal



cyclohexylisocyanide

24528397

Reaction ID UCExp245-15 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.486 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp245

+

3,4methylenedioxyphenylacetic acid

+

5-methylfurfurylamine

+

piperonal

111



1,1,3,3tetramethylbutyl isocyanide

24528398

Reaction ID UCExp245-16 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.673 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp245

+

3,4methylenedioxyphenylacetic acid

+

5-methylfurfurylamine

+



1,1,3,3tetramethylbutyl isocyanide

piperonal

24528398

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCExp245-33 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.507 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp245

+

3,4methylenedioxyphenylacetic acid

+

furfurylamine

+

piperonal



t-butyl isocyanide

24528407

Reaction ID UCExp245-34 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.714 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp245

+

3,4methylenedioxyphenylacetic acid

+

furfurylamine

+

piperonal



t-butyl isocyanide

24528407

Reaction ID UCExp245-35 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.492 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp245

+

+

+

112



3,4methylenedioxyphenylacetic acid

furfurylamine

1,1,3,3tetramethylbutyl isocyanide

piperonal

24528408

Reaction ID UCExp245-36

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.683 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp245

+

3,4methylenedioxyphenylacetic acid

+

furfurylamine

+



1,1,3,3tetramethylbutyl isocyanide

piperonal

24528408

Reaction ID UCExp245-37 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.509 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp245

+

3,4methylenedioxyphenylacetic acid

+

furfurylamine

+

piperonal



n-butyl isocyanide

24528409

Reaction ID UCExp245-38 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.718 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp245

+

3,4methylenedioxyphenylacetic acid

+

furfurylamine

+

piperonal

Reaction ID UCExp245-39 Researcher Reaction Type

Khalid Mirza Ugi

113



n-butyl isocyanide

24528409

Solvent methanol Limiting Reactant 0.504 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp245

+

3,4methylenedioxyphenylacetic acid

+

+

5-methylfurfurylamine

piperonal



n-butyl isocyanide

24528410

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCExp245-40 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.706 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp245

+

3,4methylenedioxyphenylacetic acid

+

+

5-methylfurfurylamine

piperonal



n-butyl isocyanide

24528410

3,5-Bis(trifluoromethyl)benzaldehyde Reaction ID UCEXP181-120V2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.222 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

+

2,4,6-trihydroxybenzoic acid

+

+

3,5Bis(trifluoromethyl)benzaldehyde

methylamine



tosylmethyl isocyanide

24528149

Reaction ID UCEXP234-1 Researcher David Bulger Reaction Type Ugi Solvent methanol Limiting Reactant 1.004 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp234

+

+

+

114



phenylpropynoic acid

3,5Bis(trifluoromethyl)benzaldehyde

benzylamine

t-butyl isocyanide

24528266

Reaction ID UCEXP234-2 Researcher David Bulger Reaction Type Ugi Solvent methanol Limiting Reactant 1.002 M Precipitate Yes Product Pending Comments Reference http://usefulchem.wikispaces.com/Exp234

+

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

phenylpropynoic acid

+

+

3,5Bis(trifluoromethyl)benzaldehyde

benzylamine



cyclohexylisocyanide

23078614

Reaction ID UCEXP234-3 Researcher David Bulger Reaction Type Ugi Solvent methanol Limiting Reactant 1.004 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp234

+

phenylpropynoic acid

+

+

3,5Bis(trifluoromethyl)benzaldehyde

benzylamine



t-butyl isocyanide

24528266

Reaction ID UCEXP234-4 Researcher David Bulger Reaction Type Ugi Solvent methanol Limiting Reactant 1.002 M Precipitate Yes Product Pending Comments Reference http://usefulchem.wikispaces.com/Exp234

+

phenylpropynoic acid

+

benzylamine

+

3,5Bis(trifluoromethyl)benzaldehyde

3,5-dimethoxybenzaldehyde Reaction ID UCEXP171HV2B8 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.223 M Precipitate Yes Product No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp171

115



cyclohexylisocyanide

23078614

+

2,4,6-trihydroxybenzoic acid

+

methylamine

+

3,5-dimethoxybenzaldehyde



tosylmethyl isocyanide

21105832

Reaction ID UCEXP173G/V2B19

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.223 M Precipitate Yes Yield - % Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp173

+

phenylpropynoic acid

+

benzylamine

+

3,5-dimethoxybenzaldehyde



n-butyl isocyanide

21105845

Reaction ID UCEXP174O/V2B47 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.223 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp174

+

D-(−)-Quinic acid

+

5-methylfurfurylamine

+

3,5-dimethoxybenzaldehyde



t-butyl isocyanide

21106186

Reaction ID UCEXP181-062V2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.223 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

+

4-hydroxybenzoic acid

+

methylamine

+

3,5-dimethoxybenzaldehyde

Reaction ID UCEXP181-065V2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.223 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

116



tosylmethyl isocyanide

24528101

+

D-(−)-Quinic acid

+

benzylamine

+

3,5-dimethoxybenzaldehyde



t-butyl isocyanide

24528104

Reaction ID UCEXP181-094V2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.217 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

+

3,4-dihydroxyphenylacetic acid

+

furfurylamine

+

3,5-dimethoxybenzaldehyde



tosylmethyl isocyanide

24528126

Reaction ID UCEXP233-1 Researcher David Bulger Reaction Type Ugi Solvent methanol Limiting Reactant 0.921 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp233

+

1-aminocyclohexane-1carboxylic acid

+

benzylamine

+

3,5-dimethoxybenzaldehyde



t-butyl isocyanide

24534439

Reaction ID UCEXP233-10 Researcher David Bulger Reaction Type Ugi Solvent methanol Limiting Reactant 1.018 M Precipitate Yes Product Pending Comments Reference http://usefulchem.wikispaces.com/Exp233

+

phenylpropynoic acid

+

benzylamine

+

3,5-dimethoxybenzaldehyde

Reaction ID UCEXP233-11 Researcher David Bulger Reaction Type Ugi Solvent methanol Limiting Reactant 1.021 M Precipitate No Comments -

117



cyclohexylisocyanide

23078615

Reference

http://usefulchem.wikispaces.com/Exp233

+

Boc-Pro-OH

+

benzylamine

+

3,5-dimethoxybenzaldehyde



t-butyl isocyanide

24528262

Reaction ID UCEXP233-12 Researcher David Bulger Reaction Type Ugi Solvent methanol Limiting Reactant 1.018 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp233

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

+

Boc-Pro-OH

+

benzylamine

+

3,5-dimethoxybenzaldehyde



cyclohexylisocyanide

24528263

Reaction ID UCEXP233-2 Researcher David Bulger Reaction Type Ugi Solvent methanol Limiting Reactant 0.92 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp233

+

1-aminocyclohexane-1carboxylic acid

+

benzylamine

+

3,5-dimethoxybenzaldehyde



cyclohexylisocyanide

24534440

Reaction ID UCEXP233-3 Researcher David Bulger Reaction Type Ugi Solvent methanol Limiting Reactant 0.918 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp233

+

phenylpropynoic acid

+

benzylamine

+

3,5-dimethoxybenzaldehyde

Reaction ID UCEXP233-4 Researcher David Bulger Reaction Type Ugi Solvent methanol Limiting Reactant 0.917 M Precipitate Yes Product Pending Comments -

118



t-butyl isocyanide

24528265

Reference

http://usefulchem.wikispaces.com/Exp233

+

phenylpropynoic acid

+

benzylamine

+

3,5-dimethoxybenzaldehyde



cyclohexylisocyanide

23078615

Reaction ID UCEXP233-5 Researcher David Bulger Reaction Type Ugi Solvent methanol Limiting Reactant 0.919 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp233

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

+

Boc-Pro-OH

+

benzylamine

+

3,5-dimethoxybenzaldehyde



t-butyl isocyanide

24528262

Reaction ID UCEXP233-6 Researcher David Bulger Reaction Type Ugi Solvent methanol Limiting Reactant 0.917 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp233

+

Boc-Pro-OH

+

benzylamine

+

3,5-dimethoxybenzaldehyde



cyclohexylisocyanide

24528263

Reaction ID UCEXP233-7 Researcher David Bulger Reaction Type Ugi Solvent methanol Limiting Reactant 1.02 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp233

+

1-aminocyclohexane-1carboxylic acid

+

benzylamine

+

3,5-dimethoxybenzaldehyde

Reaction ID UCEXP233-8 Researcher David Bulger Reaction Type Ugi Solvent methanol Limiting Reactant 1.018 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp233

119



t-butyl isocyanide

24534439

+

1-aminocyclohexane-1carboxylic acid

+

benzylamine

+

3,5-dimethoxybenzaldehyde



cyclohexylisocyanide

24534440

Reaction ID UCEXP233-9 Researcher David Bulger Reaction Type Ugi Solvent methanol Limiting Reactant 1.021 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp233

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

+

phenylpropynoic acid

+

benzylamine

+

3,5-dimethoxybenzaldehyde



t-butyl isocyanide

24528265

Reaction ID UCEXP234-10 Researcher David Bulger Reaction Type Ugi Solvent methanol Limiting Reactant 0.916 M Precipitate Reactants insoluble Comments Reference http://usefulchem.wikispaces.com/Exp234

+

Boc-L-Serine

+

benzylamine

+

3,5-dimethoxybenzaldehyde



cyclohexylisocyanide

24528267

Reaction ID UCEXP234-11 Researcher David Bulger Reaction Type Ugi Solvent methanol Limiting Reactant 0.893 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp234

+

Boc-L-Threonine

+

glycine methyl ester hydrochloride

+

3,5-dimethoxybenzaldehyde

Reaction ID UCEXP234-12 Researcher David Bulger Reaction Type Ugi Solvent methanol Limiting Reactant 0.891 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp234

120



t-butyl isocyanide

24528268

+

+

glycine methyl ester hydrochloride

Boc-L-Threonine

+

3,5-dimethoxybenzaldehyde



cyclohexylisocyanide

24528269

Reaction ID UCEXP234-5 Researcher David Bulger Reaction Type Ugi Solvent methanol Limiting Reactant 0.918 M Precipitate Reactants insoluble Comments Reference http://usefulchem.wikispaces.com/Exp234

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

+

Fmoc-Diglycine

+

benzylamine

+

3,5-dimethoxybenzaldehyde



t-butyl isocyanide

24528270

Reaction ID UCEXP234-6 Researcher David Bulger Reaction Type Ugi Solvent methanol Limiting Reactant 0.916 M Precipitate Reactants insoluble Comments Reference http://usefulchem.wikispaces.com/Exp234

+

Fmoc-Diglycine

+

benzylamine

+

3,5-dimethoxybenzaldehyde



cyclohexylisocyanide

24528271

Reaction ID UCEXP234-7 Researcher David Bulger Reaction Type Ugi Solvent methanol Limiting Reactant 0.918 M Precipitate Reactants insoluble Comments Reference http://usefulchem.wikispaces.com/Exp234

+

Boc-diglycine

+

benzylamine

+

3,5-dimethoxybenzaldehyde

Reaction ID UCEXP234-8 Researcher David Bulger Reaction Type Ugi Solvent methanol Limiting Reactant 0.916 M Precipitate Reactants insoluble Comments Reference http://usefulchem.wikispaces.com/Exp234

121



t-butyl isocyanide

24528272

+

+

Boc-diglycine

benzylamine

+

3,5-dimethoxybenzaldehyde



cyclohexylisocyanide

24528273

Reaction ID UCEXP234-9 Researcher David Bulger Reaction Type Ugi Solvent methanol Limiting Reactant 0.918 M Precipitate Reactants insoluble Comments Reference http://usefulchem.wikispaces.com/Exp234

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

+

+

Boc-L-Serine

benzylamine

+

3,5-dimethoxybenzaldehyde



t-butyl isocyanide

24528274

4-(dimethylamino)benzaldehyde Reaction ID UCEXP171KV2B11 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.222 M Precipitate Yes Yield - % Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp171

+

1-pyrenebutyric acid

+

methylamine

+

4-(dimethylamino)benzaldehyde



t-butyl isocyanide

21105842

Reaction ID UCEXP181-104V2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.223 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

+

D-(−)-Quinic acid

+

methylamine

+

4-(dimethylamino)benzaldehyde

Reaction ID UCEXP215D Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 0.66 M Precipitate No

122



tosylmethyl isocyanide

24528134

Comments Reference

http://usefulchem.wikispaces.com/Exp215

+

+

1-pyrenebutyric acid

methylamine

+

4-(dimethylamino)benzaldehyde



t-butyl isocyanide

21105842

Reaction ID UCEXP222-5

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 0.898 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp222

+

+

1-pyrenebutyric acid

methylamine

+

4-(dimethylamino)benzaldehyde



t-butyl isocyanide

21105842

Reaction ID UCEXP228-5 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.372 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp228

+

Boc-Trp-OH

+

5-methylfurfurylamine

+

4-(dimethylamino)benzaldehyde



tosylmethyl isocyanide

24534191

4-(trifluoromethyl)benzaldehyde Reaction ID UCEXP173C/V2B15 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.222 M Precipitate Reactants Insoluble Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp173

+

1-pyrenebutyric acid

+

methylamine

+

4-(trifluoromethyl)benzaldehyde

Reaction ID UCEXP181-072V2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.224 M

123



t-butyl isocyanide

21106044

Precipitate Comments Reference

No Protocol from Explan005 followed http://usefulchem.wikispaces.com/Exp181

+

+

2,6-dihydroxybenzoic acid

methylamine

+

4-(trifluoromethyl)benzaldehyde



tosylmethyl isocyanide

21106207

Reaction ID UCEXP185-1

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.409 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp185

+

methacrylic acid

+

5-methylfurfurylamine

+

4-(trifluoromethyl)benzaldehyde



t-butyl isocyanide

21111670

Reaction ID UCEXP185-2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.409 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp185

+

+

methacrylic acid

benzylamine

+

4-(trifluoromethyl)benzaldehyde



t-butyl isocyanide

21111671

Reaction ID UCEXP187-1 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.057 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp187

+

methacrylic acid

+

5-methylfurfurylamine

+

4-(trifluoromethyl)benzaldehyde

Reaction ID UCEXP187-2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.06 M Precipitate Yes Yield - %

124



t-butyl isocyanide

21111670

Comments Reference

http://usefulchem.wikispaces.com/Exp187

+

methacrylic acid

+

benzylamine

+

4-(trifluoromethyl)benzaldehyde



t-butyl isocyanide

21111671

Reaction ID UCEXP187-3

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.064 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp187

+

methacrylic acid

+

t-butylamine

+

4-(trifluoromethyl)benzaldehyde



t-butyl isocyanide

21143155

Reaction ID UCEXP188-1 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.225 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp188

+

methacrylic acid

+

5-methylfurfurylamine

+

4-(trifluoromethyl)benzaldehyde



t-butyl isocyanide

21111670

Reaction ID UCEXP188-2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.225 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp188

+

methacrylic acid

+

benzylamine

+

4-(trifluoromethyl)benzaldehyde

Reaction ID UCEXP188-3 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.225 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp188

125



t-butyl isocyanide

21111671

+

+

methacrylic acid

t-butylamine

+

4-(trifluoromethyl)benzaldehyde



t-butyl isocyanide

21143155

Reaction ID UCEXP228-6 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.627 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp228

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

+

Boc-Trp-OH

+

5-methylfurfurylamine

+

4-(trifluoromethyl)benzaldehyde



n-butyl isocyanide

24534190

Reaction ID UCEXP231-4 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 2 M Precipitate Yes Product Pending Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp231

+

methoxy acetic ac id

+

5-methylfurfurylamine

+

4-(trifluoromethyl)benzaldehyde



n-butyl isocyanide

21486238

Reaction ID UCEXP232-11 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.029 M Precipitate Yes Product Pending Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+

4-(trifluoromethyl)benzaldehyde

Reaction ID UCEXP232-12 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.028 M Precipitate Yes Product Pending Comments -

126



t-butyl isocyanide

24528198

Reference

http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+

4-(trifluoromethyl)benzaldehyde



n-butyl isocyanide

24528199

Reaction ID UCEXP232-13

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.029 M Precipitate Yes Product Pending Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+

4-(trifluoromethyl)benzaldehyde



1-pentyl isocyanide

24528200

Reaction ID UCEXP232-14 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.028 M Precipitate Yes Product Pending Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+

4-(trifluoromethyl)benzaldehyde



cyclohexylisocyanide

21782441

Reaction ID UCEXP232-15 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.028 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+

4-(trifluoromethyl)benzaldehyde

Reaction ID UCExp235-1 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1 M

127



1,1,3,3tetramethylbutyl isocyanide

24528201

Precipitate Product Comments Reference

Yes No http://usefulchem.wikispaces.com/Exp235

+

Boc-Gly-OH

+

furfurylamine

+

4-(trifluoromethyl)benzaldehyde



t-butyl isocyanide

24528198

Reaction ID UCExp235-2

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1 M Precipitate Yes Product No Comments Reference http://usefulchem.wikispaces.com/Exp235

+

Boc-Gly-OH

+

furfurylamine

+

4-(trifluoromethyl)benzaldehyde



cyclohexylisocyanide

21782441

Reaction ID UCExp236-01 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.614 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp236

+

3,3'-dichloropivalic acid

+

t-butylamine

+

4-(trifluoromethyl)benzaldehyde



n-butyl isocyanide

24528275

Reaction ID UCExp236-02 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.614 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp236

+

3,3'-dichloropivalic acid

+

3-chloroaniline

+

4-(trifluoromethyl)benzaldehyde

Reaction ID UCExp236-03 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.614 M

128



n-butyl isocyanide

24528276

Precipitate Comments Reference

No http://usefulchem.wikispaces.com/Exp236

+

3,3'-dichloropivalic acid

+

benzylamine

+

4-(trifluoromethyl)benzaldehyde



n-butyl isocyanide

24528277

Reaction ID UCExp236-04

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.844 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp236

+

methacrylic acid

+

butylamine

+

4-(trifluoromethyl)benzaldehyde



t-butyl isocyanide

24528278

Reaction ID UCExp236-05 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.65 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp236

+

formic acid

+

t-butylamine

+

4-(trifluoromethyl)benzaldehyde



t-butyl isocyanide

24528279

Reaction ID UCExp236-07 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.614 M Precipitate Yes Yield - % Comments Reference http://usefulchem.wikispaces.com/Exp236

+

3,3'-dichloropivalic acid

+

1-hexylamine

+

4-(trifluoromethyl)benzaldehyde

Reaction ID UCExp236-08 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.65 M Precipitate No

129



t-butyl isocyanide

24528280

Comments Reference

http://usefulchem.wikispaces.com/Exp236

+

formic acid

+

3-chloroaniline

+

4-(trifluoromethyl)benzaldehyde



t-butyl isocyanide

24528281

Reaction ID UCExp236-09

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.614 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp236

+

3,3'-dichloropivalic acid

+

2-chloroaniline

+

4-(trifluoromethyl)benzaldehyde



t-butyl isocyanide

24528282

Reaction ID UCExp236-10 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.888 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp236

+

methacrylic acid

+

methylamine

+

4-(trifluoromethyl)benzaldehyde



n-butyl isocyanide

24528283

Reaction ID UCExp236-11 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.65 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp236

+

formic acid

+

benzylamine

+

4-(trifluoromethyl)benzaldehyde

Reaction ID UCExp236-12 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.636 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp236

130



t-butyl isocyanide

24528284

+

+

methacrylic acid

aniline

+

4-(trifluoromethyl)benzaldehyde



t-butyl isocyanide

24528285

Reaction ID UCExp236-13 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.614 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp236

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

+

3,3'-dichloropivalic acid

+

1-propylamine

+

4-(trifluoromethyl)benzaldehyde



n-butyl isocyanide

24528286

Reaction ID UCExp236-15 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.614 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp236

+

3,3'-dichloropivalic acid

+

1-heptylamine

+

4-(trifluoromethyl)benzaldehyde



t-butyl isocyanide

24528288

Reaction ID UCExp236-16 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.872 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp236

+

formic acid

+

butylamine

+

4-(trifluoromethyl)benzaldehyde

Reaction ID UCExp236-17 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.614 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp236

131



t-butyl isocyanide

24528289

+

+

3,3'-dichloropivalic acid

aniline

+

4-(trifluoromethyl)benzaldehyde



n-butyl isocyanide

24528290

Reaction ID UCExp236-19 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.927 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp236

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

+

formic acid

+

methylamine

+

4-(trifluoromethyl)benzaldehyde



n-butyl isocyanide

24528292

Reaction ID UCExp236-20 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.631 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp236

+

methacrylic acid

+

t-butylamine

+

4-(trifluoromethyl)benzaldehyde



n-butyl isocyanide

24528293

Reaction ID UCExp236-21 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.65 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp236

+

formic acid

+

aniline

+

4-(trifluoromethyl)benzaldehyde

Reaction ID UCExp236-23 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.631 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp236

132



t-butyl isocyanide

24528294

+

methacrylic acid

+

3-chloroaniline

+

4-(trifluoromethyl)benzaldehyde



n-butyl isocyanide

24528296

Reaction ID UCExp236-24 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.63 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp236

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

+

methacrylic acid

+

benzylamine

+

4-(trifluoromethyl)benzaldehyde



n-butyl isocyanide

24528297

Reaction ID UCExp236-28 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.631 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp236

+

methacrylic acid

+

1-hexylamine

+

4-(trifluoromethyl)benzaldehyde



t-butyl isocyanide

24528301

Reaction ID UCExp236-29 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.614 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp236

+

3,3'-dichloropivalic acid

+

cyclohexylamine

+

4-(trifluoromethyl)benzaldehyde

Reaction ID UCExp241-29 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.729 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp241

133



t-butyl isocyanide

24528302

+

3,4methylenedioxyphenylacetic acid

+

1-hexylamine

+

4-(trifluoromethyl)benzaldehyde



n-butyl isocyanide

24528366

Reaction ID UCExp241-31

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.743 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp241

+

3,4methylenedioxyphenylacetic acid

+

2-chloroaniline

+

4-(trifluoromethyl)benzaldehyde



n-butyl isocyanide

24528368

Reaction ID UCExp241-32 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.751 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp241

+

+

3,4methylenedioxyphenylacetic acid

aniline

+

4-(trifluoromethyl)benzaldehyde



n-butyl isocyanide

24528369

Reaction ID UCExp241-37 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.733 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp241

+

3,4methylenedioxyphenylacetic acid

+

cyclohexylamine

+

4-(trifluoromethyl)benzaldehyde

Reaction ID UCExp241-43 Researcher Reaction Type

Khalid Mirza Ugi

134



t-butyl isocyanide

24528373

Solvent methanol Limiting Reactant 0.71 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp241

+

3,4methylenedioxyphenylacetic acid

+

furfurylamine

+

4-(trifluoromethyl)benzaldehyde



t-butyl isocyanide

24528376

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCExp241-44 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.72 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp241

+

3,4methylenedioxyphenylacetic acid

+

1-heptylamine

+

4-(trifluoromethyl)benzaldehyde



n-butyl isocyanide

24528377

Reaction ID UCExp241-47 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.715 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp241

+

3,4methylenedioxyphenylacetic acid

+

1-heptylamine

+

4-(trifluoromethyl)benzaldehyde



t-butyl isocyanide

24528380

4-chlorobenzaldehyde Reaction ID UCEXP158B-V1B16 Researcher Emily Messner Reaction Type Ugi Solvent methanol Limiting Reactant 0.658 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp158

+

+

+

135



salicylic acid

5-methylfurfurylamine

4-chlorobenzaldehyde

tosylmethyl isocyanide

21106076

Reaction ID UCEXP173M/V2B25 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.22 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp173

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

+

3,4-dihydroxyphenylacetic acid

+

furfurylamine

+

4-chlorobenzaldehyde



tosylmethyl isocyanide

21106043

Reaction ID UCEXP174J/V2B42 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.221 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp174

+

3,4-dihydroxyphenyl acetic acid

+

5-methylfurfurylamine

+

4-chlorobenzaldehyde



tosylmethyl isocyanide

21106197

Reaction ID UCEXP181-100V2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.225 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

+

D-(−)-Quinic acid

+

methylamine

+

4-chlorobenzaldehyde

Reaction ID UCEXP181-116V2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.225 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

136



tosylmethyl isocyanide

24528131

+

2,3-dihydroxybenzoic acid

+

+

methylamine

4-chlorobenzaldehyde



tosylmethyl isocyanide

24528145

4-chlorophenylacetic acid Reaction ID UCEXP159C-V1B18

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Researcher Emily Messner Reaction Type Ugi Solvent methanol Limiting Reactant 0.661 M Precipitate Yes but the aldehyde alone is not soluble in methanol Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp159

+

4-chlorophenylacetic acid

+

benzylamine

+

phenanthrene-9-carboxaldehyde



n-butyl isocyanide

21106077

Reaction ID UCEXP173A/V2B13 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.221 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp173

+

4-chlorophenylacetic acid

+

aniline

+

2-hydroxybenzaldehyde



tosylmethyl isocyanide

21106046

Reaction ID UCEXP175D Researcher Khalid Mirza/ Emily Messner Reaction Type Ugi Solvent methanol Limiting Reactant 0.398 M Precipitate Yes but the aldehyde alone is not soluble in methanol Yield - % Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp175

+

4-chlorophenylacetic acid

+

benzylamine

+

phenanthrene-9-carboxaldehyde

Reaction ID UCEXP179 Researcher Shannon Oseback Reaction Type Ugi Solvent methanol Limiting Reactant 0.286 M Precipitate Reactants Insoluble

137



n-butyl isocyanide

21106077

Comments Reference

Protocol from Explan005 followed http://usefulchem.wikispaces.com/Exp179

+

+

4-chlorophenylacetic acid

aniline

+

phenanthrene-9-carboxaldehyde



t-butyl isocyanide

21105833

Reaction ID UCEXP181-105V2

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.221 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

+

+

4-chlorophenylacetic acid

t-butylamine

+

3,4-dihydroxybenzaldehyde



tosylmethyl isocyanide

24528135

Reaction ID UCEXP181-121V2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.221 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

+

4-chlorophenylacetic acid

+

3-chloroaniline

+

3,4-dihydroxybenzaldehyde



tosylmethyl isocyanide

24528150

Reaction ID UCEXP215E Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 0.715 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp215

+

4-chlorophenylacetic acid

+

methylamine

+

4-methylbenzaldehyde

Reaction ID UCEXP215F Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 0.661 M Precipitate Yes but not at room temperature Yield - % Comments -

138



t-butyl isocyanide

24528155

Reference

http://usefulchem.wikispaces.com/Exp215

+

4-chlorophenylacetic acid

+

benzylamine

+

phenanthrene-9-carboxaldehyde



n-butyl isocyanide

21106077

Reaction ID UCEXP217-1 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 0.384 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp217

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

+

4-chlorophenylacetic acid

+

benzylamine

+

phenanthrene-9-carboxaldehyde



n-butyl isocyanide

21106077

4-hydroxybenzaldehyde Reaction ID UCEXP181-067V2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.221 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

+

3,4-dihydroxyphenylacetic acid

+

furfurylamine

+

4-hydroxybenzaldehyde



tosylmethyl isocyanide

24528106

Reaction ID UCEXP181-098V2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.226 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

+

2,3-dihydroxybenzoic acid

+

methylamine

+

4-hydroxybenzaldehyde

4-hydroxybenzoic acid Reaction ID UCEXP181-059V2 Researcher

Khalid Mirza

139



tosylmethyl isocyanide

24528129

Reaction Type Ugi Solvent methanol Limiting Reactant 0.225 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

+

4-hydroxybenzoic acid

+

+

methylamine

2-methylbenzaldehyde



tosylmethyl isocyanide

24528099

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCEXP181-062V2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.223 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

+

4-hydroxybenzoic acid

+

methylamine

+

3,5-dimethoxybenzaldehyde



tosylmethyl isocyanide

24528101

Reaction ID UCEXP181-086V2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.225 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

+

4-hydroxybenzoic acid

+

methylamine

+

3-hydroxybenzaldehyde



tosylmethyl isocyanide

24528121

Reaction ID UCEXP181-096V2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.224 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

+

4-hydroxybenzoic acid

+

methylamine

+

3-methoxybenzaldehyde

Reaction ID UCEXP181-099V2 Researcher Reaction Type Solvent

Khalid Mirza Ugi methanol

140



tosylmethyl isocyanide

24528127

Limiting Reactant 0.221 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

+

4-hydroxybenzoic acid

+

2-chloroaniline

+

4-methoxybenzaldehyde



tosylmethyl isocyanide

24528130

Reaction ID UCEXP181-106V2

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.224 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

+

4-hydroxybenzoic acid

+

+

methylamine

2-naphthaldehyde



tosylmethyl isocyanide

24528136

Reaction ID UCEXP181-109V2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.22 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

+

4-hydroxybenzoic acid

+

1-hexylamine

+

3-methoxybenzaldehyde



tosylmethyl isocyanide

24528139

Reaction ID UCEXP181-122V2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.22 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

+

4-hydroxybenzoic acid

+

2-chloroaniline

+

veratraldehyde

4-methoxybenzaldehyde Reaction ID UCEXP174L/V2B44 Researcher Reaction Type

Khalid Mirza Ugi

141



tosylmethyl isocyanide

24534443

Solvent methanol Limiting Reactant 0.224 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp174

+

2,4,6-trihydroxybenzoic acid

+

methylamine

+

4-methoxybenzaldehyde



tosylmethyl isocyanide

21106195

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCEXP174U/V2B54 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.22 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp174

+

3,4-dihydroxyphenylacetic acid

+

furfurylamine

+

4-methoxybenzaldehyde



tosylmethyl isocyanide

21106187

Reaction ID UCEXP181-099V2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.221 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

+

4-hydroxybenzoic acid

+

2-chloroaniline

+

4-methoxybenzaldehyde



tosylmethyl isocyanide

24528130

Reaction ID UCEXP181-112V2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.224 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

+

2,3-dihydroxybenzoic acid

+

methylamine

+

4-methoxybenzaldehyde

Reaction ID UCEXP232-46 Researcher Reaction Type

Khalid Mirza Ugi

142



tosylmethyl isocyanide

24528141

Solvent methanol Limiting Reactant 1.066 M Precipitate Yes Product Pending Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+

4-methoxybenzaldehyde



t-butyl isocyanide

24528232

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCEXP232-47 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.066 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+

4-methoxybenzaldehyde



n-butyl isocyanide

24528233

Reaction ID UCEXP232-48 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.067 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+

4-methoxybenzaldehyde



1-pentyl isocyanide

24528234

Reaction ID UCEXP232-49 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.066 M Precipitate Yes Product Pending Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+

4-methoxybenzaldehyde

Reaction ID UCEXP232-50 Researcher Reaction Type

Khalid Mirza Ugi

143



cyclohexylisocyanide

24528235

Solvent methanol Limiting Reactant 1.066 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+



1,1,3,3tetramethylbutyl isocyanide

4-methoxybenzaldehyde

24528236

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCExp241-01 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.502 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp241

+

3,4methylenedioxyphenylacetic acid

+

methylamine

+

4-methoxybenzaldehyde



benzyl isocyanide

24534407

4-methylbenzaldehyde Reaction ID UCEXP173B/V2B14 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.223 M Precipitate Yes but reactants initially insoluble Yield - % Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp173

+

1-pyrenebutyric acid

+

methylamine

+

4-methylbenzaldehyde



t-butyl isocyanide

21105844

Reaction ID UCEXP173Q/V2B29 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.22 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp173

+

+

+

144



3,4-dihydroxyphenylacetic acid

furfurylamine

4-methylbenzaldehyde

tosylmethyl isocyanide

21106042

Reaction ID UCEXP174G/V2B39 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.222 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp174

+

3,4-dihydroxyphenylacetic acid

+

1-propylamine

+

4-methylbenzaldehyde



tosylmethyl isocyanide

21106199

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCEXP215E Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 0.715 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp215

+

4-chlorophenylacetic acid

+

methylamine

+

4-methylbenzaldehyde



t-butyl isocyanide

24528155

Reaction ID UCEXP222-6 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 0.898 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp222

+

1-pyrenebutyric acid

+

methylamine

+

4-methylbenzaldehyde



t-butyl isocyanide

21105844

Reaction ID UCEXP228-7 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 0.67 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp228

+

+

+

145



1-pyrenebutyric acid

methylamine

4-methylbenzaldehyde

t-butyl isocyanide

21105844

Reaction ID UCEXP229-1 Researcher David Bulger Reaction Type Ugi Solvent methanol Limiting Reactant 0.667 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp229

+

Boc-Trp-OH

+

octadecylamine

+

4-methylbenzaldehyde



t-butyl isocyanide

24534189

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCEXP231-1 Researcher Khalid Mirza Reaction Type Ugi Solvent acetonitrile Limiting Reactant 1.538 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp231

+

formic acid

+

benzylamine

+

4-methylbenzaldehyde



tosylmethyl isocyanide

24528186

Reaction ID UCEXP232-06 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.083 M Precipitate Yes Product Pending Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+

4-methylbenzaldehyde



t-butyl isocyanide

24528193

Reaction ID UCEXP232-07 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.082 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+

4-methylbenzaldehyde

146



n-butyl isocyanide

24528194

Reaction ID UCEXP232-08 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.083 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+

4-methylbenzaldehyde



1-pentyl isocyanide

24528195

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCEXP232-09 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.083 M Precipitate Yes Product Pending Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+

4-methylbenzaldehyde



cyclohexylisocyanide

24528196

Reaction ID UCEXP232-10 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.083 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+



1,1,3,3tetramethylbutyl isocyanide

4-methylbenzaldehyde

24528197

Reaction ID UCExp241-21 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.576 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp241

+

+

+

147



3,4methylenedioxyphenylacetic acid

methylamine

4-methylbenzaldehyde

t-butyl isocyanide

24528362

4-nitrobenzoic acid Reaction ID UCEXP181-090V2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.226 M Precipitate Reactants Insoluble Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

+

4-nitrobenzoic acid

+

+

methylamine

3,4-dihydroxybenzaldehyde



tosylmethyl isocyanide

24528123

4,7-dimethoxy-1-naphthaldehyde Reaction ID UCEXP147-1V2B1 Researcher Mitesh Shah Reaction Type Ugi Solvent methanol Limiting Reactant 0.659 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp147

+

2,3-dihydroxybenzoic acid

+

methylamine

+

4,7-dimethoxy-1-naphthaldehyde



tosylmethyl isocyanide

21105839

Reaction ID UCEXP171A/V2B1 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.221 M Precipitate Yes Product Impurities found Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp171

+

2,3-dihydroxybenzoic acid

+

methylamine

+

4,7-dimethoxy-1-naphthaldehyde

Reaction ID UCEXP174S/V2B52 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.225 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp174

148



tosylmethyl isocyanide

21105839

+

+

5-nitrosalicylic acid

methylamine

+

4,7-dimethoxy-1-naphthaldehyde



n-butyl isocyanide

21106203

Reaction ID UCEXP181-101V2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.221 M Precipitate Reactants Insoluble Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

+

+

2,4,6-trihydroxybenzoic acid

methylamine

+

4,7-dimethoxy-1-naphthaldehyde



tosylmethyl isocyanide

24528132

Reaction ID UCEXP228-1 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.253 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp228

+

Boc-Trp-OH

+

octadecylamine

+

4,7-dimethoxy-1-naphthaldehyde



tosylmethyl isocyanide

24528181

5-(trifluoromethyl)-2-furylmethylamine Reaction ID UCEXP109C Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.222 M Precipitate Yes Product Pending Comments Imine was preformed Reference http://usefulchem.wikispaces.com/Exp109

+

Boc-Gly-OH

+

5-(trifluoromethyl)-2furylmethylamine

+

benzaldehyde

5-bromo-2-thiophenecarboxaldehyde Reaction ID UCEXP181-118V2

149



benzyl isocyanide

21105565

Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.224 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

+

3,4-dihydroxyphenylacetic acid

+

+

5-bromo-2thiophenecarboxaldehyde

methylamine



tosylmethyl isocyanide

24528147

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCEXP215G Researcher Khalid Mirza Reaction Type Ugi Solvent THF + methanol Limiting Reactant 0.291 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp215

+

chloroacetic acid

+

+

5-bromo-2thiophenecarboxaldehyde

3-chloroaniline



benzyl isocyanide

24528156

Reaction ID UCExp236-14 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.856 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp236

+

3,3'-dichloropivalic acid

+

+

5-bromo-2thiophenecarboxaldehyde

methylamine



t-butyl isocyanide

24528287

Reaction ID UCExp236-22 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.614 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp236

+

3,3'-dichloropivalic acid

+

t-butylamine

+

5-bromo-2thiophenecarboxaldehyde

150



t-butyl isocyanide

24528295

Reaction ID UCExp236-25 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.615 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp236

+

3,3'-dichloropivalic acid

+

+

5-bromo-2thiophenecarboxaldehyde

3-chloroaniline



t-butyl isocyanide

24528298

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCExp236-26 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.612 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp236

+

3,3'-dichloropivalic acid

+

+

5-bromo-2thiophenecarboxaldehyde

benzylamine



t-butyl isocyanide

24528299

Reaction ID UCExp241-17 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.577 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp241

+

3,4methylenedioxyphenylacetic acid

+

+

5-bromo-2thiophenecarboxaldehyde

methylamine



t-butyl isocyanide

24528360

Reaction ID UCExp241-23 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.559 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp241

+

3,4-

+

+

151



methylenedioxyphenylacetic acid

5-bromo-2thiophenecarboxaldehyde

methylamine

n-butyl isocyanide

24528364

Reaction ID UCExp241-30 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.717 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp241

+

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

3,4methylenedioxyphenylacetic acid

+

+

5-bromo-2thiophenecarboxaldehyde

butylamine



t-butyl isocyanide

24528367

Reaction ID UCExp241-33 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.747 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp241

+

3,4methylenedioxyphenylacetic acid

+

+

5-bromo-2thiophenecarboxaldehyde

3-chloroaniline



t-butyl isocyanide

24528370

Reaction ID UCExp241-39 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.721 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp241

+

3,4methylenedioxyphenylacetic acid

+

aniline

+

5-bromo-2thiophenecarboxaldehyde

Reaction ID UCExp241-45 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.748 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp241

152



t-butyl isocyanide

24528374

+

+

3,4methylenedioxyphenylacetic acid

+

5-bromo-2thiophenecarboxaldehyde

t-butylamine



t-butyl isocyanide

24528378

5-methylfurfurylamine

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCEXP052E Researcher Alicia Holsey Reaction Type Ugi Solvent methanol Limiting Reactant 0.223 M Precipitate Yes Yield 32 % Comments 1M solutions of the starting materials was made Reference http://usefulchem.wikispaces.com/Exp052

+

Boc-Gly-OH

+

5-methylfurfurylamine

+

piperonal



t-butyl isocyanide

10481872

Reaction ID UCEXP064C Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.393 M Precipitate Yes Yield 43.8 % Comments Solution was made up to 4 mL - methanol amount probably closer to 3 mL Reference http://usefulchem.wikispaces.com/Exp064

+

Boc-Gly-OH

+

5-methylfurfurylamine

+

veratraldehyde



benzyl isocyanide

10481870

Reaction ID UCEXP086B Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.402 M Precipitate Yes Yield 38 % Comments Solution was made up to 4 mL - methanol amount probably closer to 3 mL Reference http://usefulchem.wikispaces.com/Exp086

+

Boc-Gly-OH

+

5-methylfurfurylamine

+

benzaldehyde

153



t-butyl isocyanide

10481766

Reaction ID UCEXP130-1 Researcher Rikesh Parikh Reaction Type Ugi Solvent methanol Limiting Reactant 0.751 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp130

+

formic acid

+

5-methylfurfurylamine

+

2-naphthaldehyde



n-butyl isocyanide

21106081

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCEXP130-3 Researcher Rikesh Parikh Reaction Type Ugi Solvent methanol Limiting Reactant 0.429 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp130

+

formic acid

+

5-methylfurfurylamine

+

benzaldehyde



tosylmethyl isocyanide

21106060

Reaction ID UCEXP131-3 Researcher Rikesh Parikh Reaction Type Ugi Solvent methanol Limiting Reactant 0.614 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp131

+

Boc-Trp-OH

+

5-methylfurfurylamine

+

veratraldehyde



1-pentyl isocyanide

21106069

Reaction ID UCEXP155B-V1B159 Researcher Emily Messner Reaction Type Ugi Solvent methanol Limiting Reactant 0.674 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp155

+

3-(4methoxyphenyl)propionic acid

+

5-methylfurfurylamine

+

benzaldehyde

154



t-butyl isocyanide

21106074

Reaction ID UCEXP158B-V1B16 Researcher Emily Messner Reaction Type Ugi Solvent methanol Limiting Reactant 0.658 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp158

+

salicylic acid

+

5-methylfurfurylamine

+

4-chlorobenzaldehyde



tosylmethyl isocyanide

21106076

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCEXP171B/V2B2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.219 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp171

+

1-pyrenebutyric acid

+

5-methylfurfurylamine

+

o-vanillin



t-butyl isocyanide

21106056

Reaction ID UCEXP173H/V2B20 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.22 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp173

+

3,4-dihydroxyphenylacetic acid

+

5-methylfurfurylamine

+

2-naphthaldehyde



tosylmethyl isocyanide

21106053

Reaction ID UCEXP174A/V2B31 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.221 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp174

+

3,4-dihydroxyphenylacetic acid

+

5-methylfurfurylamine

+

benzaldehyde

155



tosylmethyl isocyanide

21106189

Reaction ID UCEXP174J/V2B42 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.221 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp174

+

3,4-dihydroxyphenyl acetic acid

+

+

5-methylfurfurylamine

4-chlorobenzaldehyde



tosylmethyl isocyanide

21106197

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCEXP174O/V2B47 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.223 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp174

+

D-(−)-Quinic acid

+

5-methylfurfurylamine

+

3,5-dimethoxybenzaldehyde



t-butyl isocyanide

21106186

Reaction ID UCEXP174P/V2B49 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.22 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp174

+

3,4-dihydroxyphenylacetic acid

+

5-methylfurfurylamine

+

3-methoxybenzaldehyde



tosylmethyl isocyanide

21106192

Reaction ID UCEXP181-055V2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.223 M Precipitate no and aldehyde alone not solube Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

+

2,6-dihydroxybenzoic acid

+

5-methylfurfurylamine

+

phenanthrene-9-carboxaldehyde

156



n-butyl isocyanide

24528096

Reaction ID UCEXP181-077V2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.225 M Precipitate Reactants Insoluble Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

+

2,4,6-trihydroxybenzoic acid

+

5-methylfurfurylamine

+

3-methoxybenzaldehyde



n-butyl isocyanide

24528113

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCEXP181-088V2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.222 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

+

diphenylacetic acid

+

5-methylfurfurylamine

+

3,4-dihydroxybenzaldehyde



n-butyl isocyanide

24528532

Reaction ID UCEXP181-102V2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.221 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

+

3,4-dihydroxyphenylacetic acid

+

5-methylfurfurylamine

+

3-hydroxybenzaldehyde



tosylmethyl isocyanide

24528533

Reaction ID UCEXP181-114V2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.223 M Precipitate Reactants Insoluble Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

+

2,4,6-trihydroxybenzoic acid

+

5-methylfurfurylamine

+

phenanthrene-9-carboxaldehyde

157



n-butyl isocyanide

24528143

Reaction ID UCEXP185-1 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.409 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp185

+

methacrylic acid

+

5-methylfurfurylamine

+

4-(trifluoromethyl)benzaldehyde



t-butyl isocyanide

21111670

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCEXP187-1 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.057 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp187

+

methacrylic acid

+

5-methylfurfurylamine

+

4-(trifluoromethyl)benzaldehyde



t-butyl isocyanide

21111670

Reaction ID UCEXP188-1 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.225 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp188

+

methacrylic acid

+

5-methylfurfurylamine

+

4-(trifluoromethyl)benzaldehyde



t-butyl isocyanide

21111670

Reaction ID UCEXP226-1 Researcher David Bulger Reaction Type Ugi Solvent THF Limiting Reactant 0.523 M Precipitate No Comments 0.5 mmol of isocyanide was added to 900uL of a 0.55M solution of aldehyde; amine and acid Reference http://usefulchem.wikispaces.com/Exp226

+

1-pyrenebutyric acid

+

5-methylfurfurylamine

+

benzaldehyde

Reaction ID UCEXP226-2

158



t-butyl isocyanide

24528165

Researcher David Bulger Reaction Type Ugi Solvent THF Limiting Reactant 0.525 M Precipitate No Comments 0.5 mmol of isocyanide was added to 900uL of a 0.55M solution of aldehyde; amine and acid Reference http://usefulchem.wikispaces.com/Exp226

+

1-pyrenebutyric acid

+

5-methylfurfurylamine

+

benzaldehyde



n-butyl isocyanide

24528166

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCEXP226-3 Researcher David Bulger Reaction Type Ugi Solvent THF Limiting Reactant 0.519 M Precipitate No Comments 0.5 mmol of isocyanide was added to 900uL of a 0.55M solution of aldehyde; amine and acid Reference http://usefulchem.wikispaces.com/Exp226

+

1-pyrenebutyric acid

+

5-methylfurfurylamine

+

benzaldehyde



1-pentyl isocyanide

24528167

Reaction ID UCEXP226-4 Researcher David Bulger Reaction Type Ugi Solvent THF Limiting Reactant 0.52 M Precipitate No Comments 0.5 mmol of isocyanide was added to 900uL of a 0.55M solution of aldehyde; amine and acid Reference http://usefulchem.wikispaces.com/Exp226

+

1-pyrenebutyric acid

+

5-methylfurfurylamine

+

benzaldehyde



cyclohexylisocyanide

24528168

Reaction ID UCEXP226-5 Researcher David Bulger Reaction Type Ugi Solvent THF Limiting Reactant 0.52 M Precipitate No Comments 0.5 mmol of isocyanide was added to 900uL of a 0.55M solution of aldehyde; amine and acid Reference http://usefulchem.wikispaces.com/Exp226

+

1-pyrenebutyric acid

+

5-methylfurfurylamine

+

benzaldehyde

Reaction ID UCEXP226-6 Researcher Reaction Type

David Bulger Ugi

159



benzyl isocyanide

24528169

Solvent THF Limiting Reactant 0.501 M Precipitate No Comments 0.5 mmol of isocyanide was added to 900uL of a 0.55M solution of aldehyde; amine and acid Reference http://usefulchem.wikispaces.com/Exp226

+

1-pyrenebutyric acid

+

+

5-methylfurfurylamine

benzaldehyde



tosylmethyl isocyanide

24528170

Reaction ID UCEXP226-7

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Researcher David Bulger Reaction Type Ugi Solvent THF Limiting Reactant 0.516 M Precipitate No Comments 0.5 mmol of isocyanide was added to 900uL of a 0.55M solution of aldehyde; amine and acid Reference http://usefulchem.wikispaces.com/Exp226

+

1-pyrenebutyric acid

+

+

5-methylfurfurylamine



2-morpholinoethyl isocyanide

benzaldehyde

24528171

Reaction ID UCEXP226-8 Researcher David Bulger Reaction Type Ugi Solvent THF Limiting Reactant 0.434 M Precipitate No Comments 0.5 mmol of isocyanide was added to 500uL of a 0.5M solution of aldehyde; amine and acid Reference http://usefulchem.wikispaces.com/Exp226

+

1-pyrenebutyric acid

+

+

5-methylfurfurylamine



2-chloro-6methylphenyl isocyanide

benzaldehyde

24528172

Reaction ID UCEXP228-5 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.372 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp228

+

Boc-Trp-OH

+

5-methylfurfurylamine

+

4-(dimethylamino)benzaldehyde

Reaction ID UCEXP228-6 Researcher

Khalid Mirza

160



tosylmethyl isocyanide

24534191

Reaction Type Ugi Solvent methanol Limiting Reactant 0.627 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp228

+

Boc-Trp-OH

+

5-methylfurfurylamine

+

4-(trifluoromethyl)benzaldehyde



n-butyl isocyanide

24534190

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCEXP231-4 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 2 M Precipitate Yes Product Pending Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp231

+

methoxy acetic ac id

+

5-methylfurfurylamine

+

4-(trifluoromethyl)benzaldehyde



n-butyl isocyanide

21486238

Reaction ID UCExp240-07 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.839 M Precipitate Yes Yield - % Comments Reference http://usefulchem.wikispaces.com/Exp240

+

phenylacetic acid

+

5-methylfurfurylamine

+

phenanthrene-9-carboxaldehyde



n-butyl isocyanide

21782451

Reaction ID UCExp240-08 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.813 M Precipitate Yes but 48h Comments Reference http://usefulchem.wikispaces.com/Exp240

+

phenylacetic acid

+

5-methylfurfurylamine

+

phenanthrene-9-carboxaldehyde

Reaction ID UCExp240-09 Researcher

Khalid Mirza

161



t-butyl isocyanide

24528348

Reaction Type Ugi Solvent THF Limiting Reactant 1.78 M Precipitate Yes Yield - % Comments Reference http://usefulchem.wikispaces.com/Exp240

+

phenylacetic acid

+

5-methylfurfurylamine

+

phenanthrene-9-carboxaldehyde



cyclohexylisocyanide

21782450

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCExp240-10 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.646 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp240

+

phenylacetic acid

+

5-methylfurfurylamine

+



1,1,3,3tetramethylbutyl isocyanide

phenanthrene-9-carboxaldehyde

24528349

Reaction ID UCExp240-11 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.788 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp240

+

phenylacetic acid

+

5-methylfurfurylamine

+

phenanthrene-9-carboxaldehyde



benzyl isocyanide

24528350

Reaction ID UCExp240-12 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.776 M Precipitate Yes but 48h Comments Reference http://usefulchem.wikispaces.com/Exp240

+

phenylacetic acid

+

5-methylfurfurylamine

+

phenanthrene-9-carboxaldehyde

162



1-pentyl isocyanide

24528351

Reaction ID UCExp242-10 Researcher Marshall Moritz Reaction Type Ugi Solvent benzene Limiting Reactant 0.424 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp242

+

phenylacetic acid

+

5-methylfurfurylamine

+

phenanthrene-9-carboxaldehyde



1-pentyl isocyanide

24528382

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCExp242-6 Researcher Marshall Moritz Reaction Type Ugi Solvent benzene Limiting Reactant 0.431 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp242

+

phenylacetic acid

+

5-methylfurfurylamine

+

phenanthrene-9-carboxaldehyde



n-butyl isocyanide

24528387

Reaction ID UCExp242-7 Researcher Marshall Moritz Reaction Type Ugi Solvent benzene Limiting Reactant 0.428 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp242

+

phenylacetic acid

+

5-methylfurfurylamine

+

phenanthrene-9-carboxaldehyde



t-butyl isocyanide

24528388

Reaction ID UCExp242-8 Researcher Marshall Moritz Reaction Type Ugi Solvent benzene Limiting Reactant 0.424 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp242

+

phenylacetic acid

+

5-methylfurfurylamine

+

phenanthrene-9-carboxaldehyde

Reaction ID UCExp242-9

163



cyclohexylisocyanide

24528389

Researcher Marshall Moritz Reaction Type Ugi Solvent benzene Limiting Reactant 0.406 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp242

+

phenylacetic acid

+

5-methylfurfurylamine

+



1,1,3,3tetramethylbutyl isocyanide

phenanthrene-9-carboxaldehyde

24528390

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCExp245-03 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.504 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp245

+

3,4methylenedioxyphenylacetic acid

+

5-methylfurfurylamine

+

piperonal



n-butyl isocyanide

24528392

Reaction ID UCExp245-04 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.706 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp245

+

3,4methylenedioxyphenylacetic acid

+

5-methylfurfurylamine

+

piperonal



n-butyl isocyanide

24528392

Reaction ID UCExp245-11 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.504 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp245

+

3,4-

+

+

164



methylenedioxyphenylacetic acid

5-methylfurfurylamine

piperonal

t-butyl isocyanide

24528396

Reaction ID UCExp245-12 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.706 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp245

+

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

3,4methylenedioxyphenylacetic acid

+

5-methylfurfurylamine

+

piperonal



t-butyl isocyanide

24528396

Reaction ID UCExp245-13 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.499 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp245

+

3,4methylenedioxyphenylacetic acid

+

5-methylfurfurylamine

+

piperonal



cyclohexylisocyanide

24528397

Reaction ID UCExp245-14 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.696 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp245

+

3,4methylenedioxyphenylacetic acid

+

5-methylfurfurylamine

+

piperonal

Reaction ID UCExp245-15 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.486 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp245

165



cyclohexylisocyanide

24528397

+

3,4methylenedioxyphenylacetic acid

+

5-methylfurfurylamine

+



1,1,3,3tetramethylbutyl isocyanide

piperonal

24528398

Reaction ID UCExp245-16

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.673 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp245

+

3,4methylenedioxyphenylacetic acid

+

5-methylfurfurylamine

+



1,1,3,3tetramethylbutyl isocyanide

piperonal

24528398

Reaction ID UCExp245-19 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.496 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp245

+

cbz-proline

+

5-methylfurfurylamine

+

piperonal



n-butyl isocyanide

24528400

Reaction ID UCExp245-20 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.092 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp245

+

cbz-proline

+

5-methylfurfurylamine

+

piperonal

Reaction ID UCExp245-27 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.494 M Precipitate No Comments -

166



n-butyl isocyanide

24528400

Reference

http://usefulchem.wikispaces.com/Exp245

+

cbz-proline

+

5-methylfurfurylamine

+

piperonal



t-butyl isocyanide

24528404

Reaction ID UCExp245-28 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.082 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp245

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

+

cbz-proline

+

5-methylfurfurylamine

+

piperonal



t-butyl isocyanide

24528404

Reaction ID UCExp245-29 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.503 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp245

+

cbz-proline

+

5-methylfurfurylamine

+



1,1,3,3tetramethylbutyl isocyanide

piperonal

24528405

Reaction ID UCExp245-30 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.013 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp245

+

cbz-proline

+

5-methylfurfurylamine

+

piperonal

Reaction ID UCExp245-31 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.504 M Precipitate No

167



1,1,3,3tetramethylbutyl isocyanide

24528405

Comments Reference

http://usefulchem.wikispaces.com/Exp245

+

cbz-proline

+

5-methylfurfurylamine

+

piperonal



cyclohexylisocyanide

24528406

Reaction ID UCExp245-32

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.002 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp245

+

cbz-proline

+

5-methylfurfurylamine

+

piperonal



cyclohexylisocyanide

24528406

Reaction ID UCExp245-39 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.504 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp245

+

3,4methylenedioxyphenylacetic acid

+

5-methylfurfurylamine

+

piperonal



n-butyl isocyanide

24528410

Reaction ID UCExp245-40 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.706 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp245

+

3,4methylenedioxyphenylacetic acid

+

5-methylfurfurylamine

+

piperonal

5-nitrosalicylic acid Reaction ID UCEXP174C/V2B34

168



n-butyl isocyanide

24528410

Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.226 M Precipitate Yes but the aldehyde alone is not soluble in methanol Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp174

+

5-nitrosalicylic acid

+

methylamine

+

phenanthrene-9-carboxaldehyde



n-butyl isocyanide

21106205

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCEXP174S/V2B52 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.225 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp174

+

5-nitrosalicylic acid

+

methylamine

+

4,7-dimethoxy-1-naphthaldehyde



n-butyl isocyanide

21106203

acetic acid Reaction ID UCEXP180 Researcher Shannon Oseback Reaction Type Ugi Solvent methanol Limiting Reactant 0.403 M Precipitate no and aldehyde alone not solube Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp180

+

acetic acid

+

1-heptylamine

+

phenanthrene-9-carboxaldehyde



n-butyl isocyanide

21105834

aniline Reaction ID UCEXP164 Researcher Emily Messner/Shannon Oseback Reaction Type Ugi Solvent methanol Limiting Reactant 0.287 M Precipitate Reactants Insoluble Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp164

+

+

+

169



phenylacetic acid

aniline

phenanthrene-9-carboxaldehyde

n-butyl isocyanide

21106183

Reaction ID UCEXP171IV2B9 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.221 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp171

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

+

3,4methylenedioxyphenylacetic acid

+

aniline

+

2-hydroxybenzaldehyde



tosylmethyl isocyanide

21106055

Reaction ID UCEXP173A/V2B13 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.221 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp173

+

4-chlorophenylacetic acid

+

aniline

+

2-hydroxybenzaldehyde



tosylmethyl isocyanide

21106046

Reaction ID UCEXP174I/V2B41 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.224 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp174

+

methacrylic acid

+

aniline

+

3,4-dihydroxybenzaldehyde

Reaction ID UCEXP174T/V2B53 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.219 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp174

170



tosylmethyl isocyanide

21106198

+

2,5-dimethoxyphenylacetic acid

+

aniline

+

2-hydroxybenzaldehyde



tosylmethyl isocyanide

21106185

Reaction ID UCEXP179 Researcher Shannon Oseback Reaction Type Ugi Solvent methanol Limiting Reactant 0.286 M Precipitate Reactants Insoluble Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp179

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

+

4-chlorophenylacetic acid

+

aniline

+

phenanthrene-9-carboxaldehyde



t-butyl isocyanide

21105833

Reaction ID UCEXP181-069V2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.221 M Precipitate Reactants Insoluble Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

+

2,4,6-trihydroxybenzoic acid

+

+

aniline

2-naphthaldehyde



tosylmethyl isocyanide

24528108

Reaction ID UCEXP181-074V2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.226 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

+

3,4-dihydroxyphenylacetic acid

+

aniline

+

3,4-dihydroxybenzaldehyde

Reaction ID UCEXP181-080V2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.221 M Precipitate Yes Product Not determined Comments Protocol from Explan005 followed

171



t-butyl isocyanide

24528110

Reference

http://usefulchem.wikispaces.com/Exp181

+

2,4,6-trihydroxybenzoic acid

+

aniline

+

3-methoxybenzaldehyde



tosylmethyl isocyanide

24528116

Reaction ID UCEXP181-083V2

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.221 M Precipitate Reactants Insoluble Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

+

1-pyrenebutyric acid

+

+

aniline

benzaldehyde



n-butyl isocyanide

21106208

Reaction ID UCEXP181-093V2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.221 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

+

hexanoic acid

+

aniline

+

2-hydroxybenzaldehyde



tosylmethyl isocyanide

24528125

Reaction ID UCEXP181-107V2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.222 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

+

phenylpropynoic acid

+

aniline

+

2-hydroxybenzaldehyde

Reaction ID UCEXP181-110V2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.222 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

172



tosylmethyl isocyanide

24528137

+

3,4-dihydroxyphenylacetic acid

+

aniline

+

2-hydroxybenzaldehyde



tosylmethyl isocyanide

24528140

Reaction ID UCExp236-12 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.636 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp236

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

+

methacrylic acid

+

aniline

+

4-(trifluoromethyl)benzaldehyde



t-butyl isocyanide

24528285

Reaction ID UCExp236-17 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.614 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp236

+

3,3'-dichloropivalic acid

+

aniline

+

4-(trifluoromethyl)benzaldehyde



n-butyl isocyanide

24528290

Reaction ID UCExp236-21 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.65 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp236

+

formic acid

+

aniline

+

4-(trifluoromethyl)benzaldehyde

Reaction ID UCExp238-03 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.931 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp238

173



t-butyl isocyanide

24528294

+

crotonic acid

+

aniline

+

phenanthrene-9-carboxaldehyde



cyclohexylisocyanide

24528305

Reaction ID UCExp238-15 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.974 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp238

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

+

crotonic acid

+

aniline

+

phenanthrene-9-carboxaldehyde



t-butyl isocyanide

24528317

Reaction ID UCExp238-27 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.726 M Precipitate Yes Product Awaiting Characterization Comments Reference http://usefulchem.wikispaces.com/Exp238

+

Boc-Gly-OH

+

aniline

+

phenanthrene-9-carboxaldehyde



cyclohexylisocyanide

24528327

Reaction ID UCExp238-39 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.76 M Precipitate Yes Product Awaiting Characterization Comments Reference http://usefulchem.wikispaces.com/Exp238

+

Boc-Gly-OH

+

aniline

+

phenanthrene-9-carboxaldehyde

Reaction ID UCExp241-32 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.751 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp241

174



t-butyl isocyanide

24528339

+

+

3,4methylenedioxyphenylacetic acid

aniline

+

4-(trifluoromethyl)benzaldehyde



n-butyl isocyanide

24528369

Reaction ID UCExp241-39

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.721 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp241

+

+

3,4methylenedioxyphenylacetic acid

+

5-bromo-2thiophenecarboxaldehyde

aniline



t-butyl isocyanide

24528374

benzaldehyde Reaction ID UCEXP086B Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.402 M Precipitate Yes Yield 38 % Comments Solution was made up to 4 mL - methanol amount probably closer to 3 mL Reference http://usefulchem.wikispaces.com/Exp086

+

Boc-Gly-OH

+

5-methylfurfurylamine

+

benzaldehyde



t-butyl isocyanide

10481766

Reaction ID UCEXP099C Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.405 M Precipitate Yes Yield 47.2 % Comments Solution was made up to 4 mL - methanol amount probably closer to 3 mL Reference http://usefulchem.wikispaces.com/Exp099

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde

Reaction ID UCEXP108C Researcher

Khalid Mirza

175



t-butyl isocyanide

21106059

Reaction Type Ugi Solvent methanol Limiting Reactant 0.393 M Precipitate Yes Yield 20.4 % Comments Imine was preformed Reference http://usefulchem.wikispaces.com/Exp108

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde



benzyl isocyanide

21106009

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCEXP109C Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.222 M Precipitate Yes Product Pending Comments Imine was preformed Reference http://usefulchem.wikispaces.com/Exp109

+

+

5-(trifluoromethyl)-2furylmethylamine

Boc-Gly-OH

+

benzaldehyde



benzyl isocyanide

21105565

Reaction ID UCEXP130-3 Researcher Rikesh Parikh Reaction Type Ugi Solvent methanol Limiting Reactant 0.429 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp130

+

formic acid

+

5-methylfurfurylamine

+

benzaldehyde



tosylmethyl isocyanide

21106060

Reaction ID UCEXP155B-V1B159 Researcher Emily Messner Reaction Type Ugi Solvent methanol Limiting Reactant 0.674 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp155

+

3-(4methoxyphenyl)propionic acid

+

5-methylfurfurylamine

+

benzaldehyde

176



t-butyl isocyanide

21106074

Reaction ID UCEXP173O/V2B27 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.222 M Precipitate Yes Product pending Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp173

+

3,4-dihydroxyphenylacetic acid

+

furfurylamine

+

benzaldehyde



tosylmethyl isocyanide

21105843

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCEXP174A/V2B31 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.221 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp174

+

3,4-dihydroxyphenylacetic acid

+

5-methylfurfurylamine

+

benzaldehyde



tosylmethyl isocyanide

21106189

Reaction ID UCEXP181-071V2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.221 M Precipitate Yes Product No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

+

mandelic acid

+

benzylamine

+

benzaldehyde



tosylmethyl isocyanide

24528531

Reaction ID UCEXP181-073V2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.222 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

+

+

+

177



Boc-Trp-OH

methylamine

benzaldehyde

t-butyl isocyanide

24528109

Reaction ID UCEXP181-083V2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.221 M Precipitate Reactants Insoluble Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

+

+

1-pyrenebutyric acid

aniline

+

benzaldehyde



n-butyl isocyanide

21106208

Reaction ID UCEXP201-01 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.039 M Precipitate Yes Yield 50.73 % Comments Automated liquid handling Reference http://usefulchem.wikispaces.com/Exp201

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde



t-butyl isocyanide

21106059

Reaction ID UCEXP201-02 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.019 M Precipitate Yes Yield 59.07 % Comments Automated liquid handling Reference http://usefulchem.wikispaces.com/Exp201

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde

Reaction ID UCEXP201-03 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.018 M Precipitate Yes Yield 61.55 % Comments Automated liquid handling

178



t-butyl isocyanide

21106059

Reference

http://usefulchem.wikispaces.com/Exp201

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde



t-butyl isocyanide

21106059

Reaction ID UCEXP201-04

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.007 M Precipitate Yes Yield 60.31 % Comments Automated liquid handling Reference http://usefulchem.wikispaces.com/Exp201

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde



t-butyl isocyanide

21106059

Reaction ID UCEXP201-05 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.015 M Precipitate Yes Yield 60.2 % Comments Automated liquid handling Reference http://usefulchem.wikispaces.com/Exp201

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde



t-butyl isocyanide

21106059

Reaction ID UCEXP201-06 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.998 M Precipitate Yes Yield 69.22 % Comments Automated liquid handling Reference http://usefulchem.wikispaces.com/Exp201

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde

Reaction ID UCEXP201-07 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.289 M Precipitate Yes

179



t-butyl isocyanide

21106059

Yield Comments Reference

52.42 % Automated liquid handling http://usefulchem.wikispaces.com/Exp201

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde



t-butyl isocyanide

21106059

Reaction ID UCEXP201-08

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.287 M Precipitate Yes Yield 44.64 % Comments Automated liquid handling Reference http://usefulchem.wikispaces.com/Exp201

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde



t-butyl isocyanide

21106059

Reaction ID UCEXP201-09 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.287 M Precipitate Yes Yield 50.28 % Comments Automated liquid handling Reference http://usefulchem.wikispaces.com/Exp201

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde



t-butyl isocyanide

21106059

Reaction ID UCEXP201-10 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.286 M Precipitate Yes Yield 54.79 % Comments Automated liquid handling Reference http://usefulchem.wikispaces.com/Exp201

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde

Reaction ID UCEXP201-11 Researcher Reaction Type Solvent

Khalid Mirza Ugi methanol

180



t-butyl isocyanide

21106059

Limiting Reactant 0.287 M Precipitate Yes Yield 53.43 % Comments Automated liquid handling Reference http://usefulchem.wikispaces.com/Exp201

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde



t-butyl isocyanide

21106059

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCEXP201-12 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.286 M Precipitate Yes Yield 54.67 % Comments Automated liquid handling Reference http://usefulchem.wikispaces.com/Exp201

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde



t-butyl isocyanide

21106059

Reaction ID UCEXP201-13 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.074 M Precipitate Yes Yield 0.34 % Comments Automated liquid handling Reference http://usefulchem.wikispaces.com/Exp201

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde



t-butyl isocyanide

21106059

Reaction ID UCEXP201-14 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.074 M Precipitate Yes Yield 1.35 % Comments Automated liquid handling Reference http://usefulchem.wikispaces.com/Exp201

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde

181



t-butyl isocyanide

21106059

Reaction ID UCEXP201-15 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.074 M Precipitate Yes Yield 10.37 % Comments Automated liquid handling Reference http://usefulchem.wikispaces.com/Exp201

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde



t-butyl isocyanide

21106059

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCEXP201-16 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.074 M Precipitate Yes Yield 16.35 % Comments Automated liquid handling Reference http://usefulchem.wikispaces.com/Exp201

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde



t-butyl isocyanide

21106059

Reaction ID UCEXP201-17 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.074 M Precipitate Yes Yield 8.68 % Comments Automated liquid handling Reference http://usefulchem.wikispaces.com/Exp201

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde



t-butyl isocyanide

21106059

Reaction ID UCEXP201-18 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.074 M Precipitate Yes Yield 5.64 % Comments Automated liquid handling Reference http://usefulchem.wikispaces.com/Exp201

+

+

+

182



Boc-Gly-OH

furfurylamine

benzaldehyde

t-butyl isocyanide

21106059

Reaction ID UCEXP201-19 Researcher Khalid Mirza Reaction Type Ugi Solvent ethanol Limiting Reactant 0.289 M Precipitate Yes Yield 51.52 % Comments Automated liquid handling Reference http://usefulchem.wikispaces.com/Exp201

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde



t-butyl isocyanide

21106059

Reaction ID UCEXP201-20 Researcher Khalid Mirza Reaction Type Ugi Solvent ethanol Limiting Reactant 0.287 M Precipitate Yes Yield 46.78 % Comments Automated liquid handling Reference http://usefulchem.wikispaces.com/Exp201

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde



t-butyl isocyanide

21106059

Reaction ID UCEXP201-21 Researcher Khalid Mirza Reaction Type Ugi Solvent ethanol Limiting Reactant 0.287 M Precipitate Yes Yield 51.29 % Comments Automated liquid handling Reference http://usefulchem.wikispaces.com/Exp201

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde

Reaction ID UCEXP201-22 Researcher Khalid Mirza Reaction Type Ugi Solvent ethanol Limiting Reactant 0.286 M Precipitate Yes Yield 54.11 %

183



t-butyl isocyanide

21106059

Comments Reference

Automated liquid handling http://usefulchem.wikispaces.com/Exp201

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde



t-butyl isocyanide

21106059

Reaction ID UCEXP201-23

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Researcher Khalid Mirza Reaction Type Ugi Solvent ethanol Limiting Reactant 0.287 M Precipitate Yes Yield 55.91 % Comments Automated liquid handling Reference http://usefulchem.wikispaces.com/Exp201

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde



t-butyl isocyanide

21106059

Reaction ID UCEXP201-24 Researcher Khalid Mirza Reaction Type Ugi Solvent ethanol Limiting Reactant 0.286 M Precipitate Yes Yield 58.28 % Comments Automated liquid handling Reference http://usefulchem.wikispaces.com/Exp201

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde



t-butyl isocyanide

21106059

Reaction ID UCEXP201-25 Researcher Khalid Mirza Reaction Type Ugi Solvent ethanol Limiting Reactant 0.074 M Precipitate Yes Yield 1.24 % Comments Automated liquid handling Reference http://usefulchem.wikispaces.com/Exp201

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde

Reaction ID UCEXP201-26 Researcher Khalid Mirza Reaction Type Ugi Solvent ethanol Limiting Reactant 0.074 M

184



t-butyl isocyanide

21106059

Precipitate Yield Comments Reference

Yes 2.25 % Automated liquid handling http://usefulchem.wikispaces.com/Exp201

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde



t-butyl isocyanide

21106059

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCEXP201-27 Researcher Khalid Mirza Reaction Type Ugi Solvent ethanol Limiting Reactant 0.074 M Precipitate Yes Yield 7.78 % Comments Automated liquid handling Reference http://usefulchem.wikispaces.com/Exp201

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde



t-butyl isocyanide

21106059

Reaction ID UCEXP201-28 Researcher Khalid Mirza Reaction Type Ugi Solvent ethanol Limiting Reactant 0.074 M Precipitate Yes Yield 1.13 % Comments Automated liquid handling Reference http://usefulchem.wikispaces.com/Exp201

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde



t-butyl isocyanide

21106059

Reaction ID UCEXP201-29 Researcher Khalid Mirza Reaction Type Ugi Solvent ethanol Limiting Reactant 0.074 M Precipitate Yes Yield 0.79 % Comments Automated liquid handling Reference http://usefulchem.wikispaces.com/Exp201

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde

185



t-butyl isocyanide

21106059

Reaction ID UCEXP201-30 Researcher Khalid Mirza Reaction Type Ugi Solvent ethanol Limiting Reactant 0.074 M Precipitate Yes Yield 0.23 % Comments Automated liquid handling Reference http://usefulchem.wikispaces.com/Exp201

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde



t-butyl isocyanide

21106059

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCEXP201-31 Researcher Khalid Mirza Reaction Type Ugi Solvent acetonitrile Limiting Reactant 0.289 M Precipitate Yes Yield 39.23 % Comments Automated liquid handling Reference http://usefulchem.wikispaces.com/Exp201

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde



t-butyl isocyanide

21106059

Reaction ID UCEXP201-32 Researcher Khalid Mirza Reaction Type Ugi Solvent acetonitrile Limiting Reactant 0.287 M Precipitate Yes Yield 40.58 % Comments Automated liquid handling Reference http://usefulchem.wikispaces.com/Exp201

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde



t-butyl isocyanide

21106059

Reaction ID UCEXP201-33 Researcher Khalid Mirza Reaction Type Ugi Solvent acetonitrile Limiting Reactant 0.287 M Precipitate Yes Yield 43.85 % Comments Automated liquid handling Reference http://usefulchem.wikispaces.com/Exp201

+

+

+

186



Boc-Gly-OH

furfurylamine

benzaldehyde

t-butyl isocyanide

21106059

Reaction ID UCEXP201-34 Researcher Khalid Mirza Reaction Type Ugi Solvent acetonitrile Limiting Reactant 0.286 M Precipitate Yes Yield 35.4 % Comments Automated liquid handling Reference http://usefulchem.wikispaces.com/Exp201

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde



t-butyl isocyanide

21106059

Reaction ID UCEXP201-35 Researcher Khalid Mirza Reaction Type Ugi Solvent acetonitrile Limiting Reactant 0.287 M Precipitate Yes Yield 41.37 % Comments Automated liquid handling Reference http://usefulchem.wikispaces.com/Exp201

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde



t-butyl isocyanide

21106059

Reaction ID UCEXP201-36 Researcher Khalid Mirza Reaction Type Ugi Solvent acetonitrile Limiting Reactant 0.286 M Precipitate Yes Yield 39.23 % Comments Automated liquid handling Reference http://usefulchem.wikispaces.com/Exp201

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde

Reaction ID UCEXP201-37 Researcher Khalid Mirza Reaction Type Ugi Solvent acetonitrile Limiting Reactant 0.074 M Precipitate Yes Yield 0.68 %

187



t-butyl isocyanide

21106059

Comments Reference

Automated liquid handling http://usefulchem.wikispaces.com/Exp201

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde



t-butyl isocyanide

21106059

Reaction ID UCEXP201-38

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Researcher Khalid Mirza Reaction Type Ugi Solvent acetonitrile Limiting Reactant 0.074 M Precipitate Yes Yield 1.8 % Comments Automated liquid handling Reference http://usefulchem.wikispaces.com/Exp201

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde



t-butyl isocyanide

21106059

Reaction ID UCEXP201-39 Researcher Khalid Mirza Reaction Type Ugi Solvent acetonitrile Limiting Reactant 0.002 M Precipitate Yes Yield 1.01 % Comments Automated liquid handling Reference http://usefulchem.wikispaces.com/Exp201

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde



t-butyl isocyanide

21106059

Reaction ID UCEXP201-40 Researcher Khalid Mirza Reaction Type Ugi Solvent acetonitrile Limiting Reactant 0.074 M Precipitate Yes Yield 0.9 % Comments Automated liquid handling Reference http://usefulchem.wikispaces.com/Exp201

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde

Reaction ID UCEXP201-41 Researcher Khalid Mirza Reaction Type Ugi Solvent acetonitrile Limiting Reactant 0.074 M

188



t-butyl isocyanide

21106059

Precipitate Yield Comments Reference

Yes 1.01 % Automated liquid handling http://usefulchem.wikispaces.com/Exp201

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde



t-butyl isocyanide

21106059

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCEXP201-42 Researcher Khalid Mirza Reaction Type Ugi Solvent acetonitrile Limiting Reactant 0.074 M Precipitate Yes Yield 0.45 % Comments Automated liquid handling Reference http://usefulchem.wikispaces.com/Exp201

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde



t-butyl isocyanide

21106059

Reaction ID UCEXP201-43 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 0.289 M Precipitate Yes Yield 6.54 % Comments Automated liquid handling Reference http://usefulchem.wikispaces.com/Exp201

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde



t-butyl isocyanide

21106059

Reaction ID UCEXP201-44 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 0.287 M Precipitate Yes Yield 7.89 % Comments Automated liquid handling Reference http://usefulchem.wikispaces.com/Exp201

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde

189



t-butyl isocyanide

21106059

Reaction ID UCEXP201-45 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 0.287 M Precipitate Yes Yield 10.03 % Comments Automated liquid handling Reference http://usefulchem.wikispaces.com/Exp201

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde



t-butyl isocyanide

21106059

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCEXP201-46 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 0.286 M Precipitate Yes Yield 9.92 % Comments Automated liquid handling Reference http://usefulchem.wikispaces.com/Exp201

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde



t-butyl isocyanide

21106059

Reaction ID UCEXP201-47 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 0.287 M Precipitate Yes Yield 7.44 % Comments Automated liquid handling Reference http://usefulchem.wikispaces.com/Exp201

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde



t-butyl isocyanide

21106059

Reaction ID UCEXP201-48 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 0.286 M Precipitate Yes Yield 12.06 % Comments Automated liquid handling Reference http://usefulchem.wikispaces.com/Exp201

+

+

+

190



Boc-Gly-OH

furfurylamine

benzaldehyde

t-butyl isocyanide

21106059

Reaction ID UCEXP217-3 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 0.383 M Precipitate Yes Product Pending Comments Reference http://usefulchem.wikispaces.com/Exp217

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde



t-butyl isocyanide

21106059

Reaction ID UCEXP217-4 Researcher Khalid Mirza Reaction Type Ugi Solvent DMSO Limiting Reactant 0.383 M Precipitate Yes Product Pending Comments Reference http://usefulchem.wikispaces.com/Exp217

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde



t-butyl isocyanide

21106059

Reaction ID UCEXP222-1 Researcher Khalid Mirza Reaction Type Ugi Solvent DMSO Limiting Reactant 0.898 M Precipitate Yes Yield - % Comments Reference http://usefulchem.wikispaces.com/Exp222

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde

Reaction ID UCEXP222-2 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 0.898 M Precipitate Yes Yield - %

191



t-butyl isocyanide

21106059

Comments Reference

http://usefulchem.wikispaces.com/Exp222

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde



t-butyl isocyanide

21106059

Reaction ID UCEXP222-3

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Researcher Khalid Mirza Reaction Type Ugi Solvent DMSO Limiting Reactant 0.473 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp222

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde



t-butyl isocyanide

21106059

Reaction ID UCEXP222-4 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 0.473 M Precipitate Yes Yield - % Comments Reference http://usefulchem.wikispaces.com/Exp222

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde



t-butyl isocyanide

21106059

Reaction ID UCEXP226-1 Researcher David Bulger Reaction Type Ugi Solvent THF Limiting Reactant 0.523 M Precipitate No Comments 0.5 mmol of isocyanide was added to 900uL of a 0.55M solution of aldehyde; amine and acid Reference http://usefulchem.wikispaces.com/Exp226

+

1-pyrenebutyric acid

+

5-methylfurfurylamine

+

benzaldehyde



t-butyl isocyanide

Reaction ID UCEXP226-2 Researcher David Bulger Reaction Type Ugi Solvent THF Limiting Reactant 0.525 M Precipitate No Comments 0.5 mmol of isocyanide was added to 900uL of a 0.55M solution of aldehyde; amine and acid

192

24528165

Reference

http://usefulchem.wikispaces.com/Exp226

+

1-pyrenebutyric acid

+

5-methylfurfurylamine

+

benzaldehyde



n-butyl isocyanide

24528166

Reaction ID UCEXP226-3 Researcher David Bulger Reaction Type Ugi Solvent THF Limiting Reactant 0.519 M Precipitate No Comments 0.5 mmol of isocyanide was added to 900uL of a 0.55M solution of aldehyde; amine and acid Reference http://usefulchem.wikispaces.com/Exp226

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

+

1-pyrenebutyric acid

+

5-methylfurfurylamine

+

benzaldehyde



1-pentyl isocyanide

24528167

Reaction ID UCEXP226-4 Researcher David Bulger Reaction Type Ugi Solvent THF Limiting Reactant 0.52 M Precipitate No Comments 0.5 mmol of isocyanide was added to 900uL of a 0.55M solution of aldehyde; amine and acid Reference http://usefulchem.wikispaces.com/Exp226

+

1-pyrenebutyric acid

+

5-methylfurfurylamine

+

benzaldehyde



cyclohexylisocyanide

24528168

Reaction ID UCEXP226-5 Researcher David Bulger Reaction Type Ugi Solvent THF Limiting Reactant 0.52 M Precipitate No Comments 0.5 mmol of isocyanide was added to 900uL of a 0.55M solution of aldehyde; amine and acid Reference http://usefulchem.wikispaces.com/Exp226

+

1-pyrenebutyric acid

+

5-methylfurfurylamine

+

benzaldehyde



benzyl isocyanide

Reaction ID UCEXP226-6 Researcher David Bulger Reaction Type Ugi Solvent THF Limiting Reactant 0.501 M Precipitate No Comments 0.5 mmol of isocyanide was added to 900uL of a 0.55M solution of aldehyde; amine and acid Reference http://usefulchem.wikispaces.com/Exp226

193

24528169

+

1-pyrenebutyric acid

+

5-methylfurfurylamine

+

benzaldehyde



tosylmethyl isocyanide

24528170

Reaction ID UCEXP226-7 Researcher David Bulger Reaction Type Ugi Solvent THF Limiting Reactant 0.516 M Precipitate No Comments 0.5 mmol of isocyanide was added to 900uL of a 0.55M solution of aldehyde; amine and acid Reference http://usefulchem.wikispaces.com/Exp226

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

+

1-pyrenebutyric acid

+

5-methylfurfurylamine

+



2-morpholinoethyl isocyanide

benzaldehyde

24528171

Reaction ID UCEXP226-8 Researcher David Bulger Reaction Type Ugi Solvent THF Limiting Reactant 0.434 M Precipitate No Comments 0.5 mmol of isocyanide was added to 500uL of a 0.5M solution of aldehyde; amine and acid Reference http://usefulchem.wikispaces.com/Exp226

+

1-pyrenebutyric acid

+

5-methylfurfurylamine

+



2-chloro-6methylphenyl isocyanide

benzaldehyde

24528172

Reaction ID UCEXP228-4 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.634 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp228

+

Boc-Trp-OH

+

octadecylamine

+

benzaldehyde

Reaction ID UCEXP229-2 Researcher David Bulger Reaction Type Ugi Solvent methanol Limiting Reactant 0.667 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp229

194



n-butyl isocyanide

24534192

+

Boc-Trp-OH

+

1-hexylamine

+

benzaldehyde



n-butyl isocyanide

24528183

Reaction ID UCEXP232-01 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.098 M Precipitate Yes Product Pending Comments Reference http://usefulchem.wikispaces.com/Exp232

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde



t-butyl isocyanide

21106059

Reaction ID UCEXP232-02 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.098 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde



n-butyl isocyanide

24528189

Reaction ID UCEXP232-03 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.099 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde

Reaction ID UCEXP232-04 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.098 M Precipitate Yes Product Pending Comments Reference http://usefulchem.wikispaces.com/Exp232

195



1-pentyl isocyanide

24528190

+

Boc-Gly-OH

+

+

furfurylamine

benzaldehyde



cyclohexylisocyanide

24528191

Reaction ID UCEXP232-05 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.098 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

+

Boc-Gly-OH

+

+

furfurylamine



1,1,3,3tetramethylbutyl isocyanide

benzaldehyde

24528192

benzoic acid Reaction ID UCEXP174D/V2B35 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.221 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp174

+

benzoic acid

+

furfurylamine

+

2-hydroxybenzaldehyde



tosylmethyl isocyanide

21106202

benzyl isocyanide Reaction ID UCEXP064C Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.393 M Precipitate Yes Yield 43.8 % Comments Solution was made up to 4 mL - methanol amount probably closer to 3 mL Reference http://usefulchem.wikispaces.com/Exp064

+

Boc-Gly-OH

+

5-methylfurfurylamine

+

veratraldehyde

Reaction ID UCEXP108C

196



benzyl isocyanide

10481870

Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.393 M Precipitate Yes Yield 20.4 % Comments Imine was preformed Reference http://usefulchem.wikispaces.com/Exp108

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde



benzyl isocyanide

21106009

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCEXP109C Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.222 M Precipitate Yes Product Pending Comments Imine was preformed Reference http://usefulchem.wikispaces.com/Exp109

+

+

5-(trifluoromethyl)-2furylmethylamine

Boc-Gly-OH

+

benzaldehyde



benzyl isocyanide

21105565

Reaction ID UCEXP130-4 Researcher Rikesh Parikh Reaction Type Ugi Solvent methanol Limiting Reactant 0.725 M Precipitate Yes Product Not Determined Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp130

+

formic acid

+

furfurylamine

+

2-naphthaldehyde



benzyl isocyanide

21106080

Reaction ID UCEXP131-4 Researcher Rikesh Parikh Reaction Type Ugi Solvent methanol Limiting Reactant 0.612 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp131

+

Boc-Trp-OH

+

1-heptylamine

+

o-vanillin

197



benzyl isocyanide

21106061

Reaction ID UCEXP131-5 Researcher Rikesh Parikh Reaction Type Ugi Solvent methanol Limiting Reactant 0.605 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp131

+

Boc-Trp-OH

+

+

1-octylamine

o-vanillin



benzyl isocyanide

21106062

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCEXP215G Researcher Khalid Mirza Reaction Type Ugi Solvent THF + methanol Limiting Reactant 0.291 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp215

+

chloroacetic acid

+

+

5-bromo-2thiophenecarboxaldehyde

3-chloroaniline



benzyl isocyanide

24528156

Reaction ID UCEXP225-5 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.891 M Precipitate Yes Product Pending Comments 0.5 mmol of isocyanide was added to 500uL of a 2M solution of aldehyde; amine and acid Reference http://usefulchem.wikispaces.com/Exp225

+

Boc-Gly-OH

+

furfurylamine

+

piperonal



benzyl isocyanide

24528161

Reaction ID UCEXP226-5 Researcher David Bulger Reaction Type Ugi Solvent THF Limiting Reactant 0.52 M Precipitate No Comments 0.5 mmol of isocyanide was added to 900uL of a 0.55M solution of aldehyde; amine and acid Reference http://usefulchem.wikispaces.com/Exp226

+

1-pyrenebutyric acid

+

5-methylfurfurylamine

+

benzaldehyde

198



benzyl isocyanide

24528169

Reaction ID UCEXP227-5 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 0.446 M Precipitate No Comments 0.5 mmol of isocyanide was added to 500uL of a 0.5M solution of aldehyde; amine and acid Reference http://usefulchem.wikispaces.com/Exp227

+

1-pyrenebutyric acid

+

+

furfurylamine

piperonal



benzyl isocyanide

24528177

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCExp240-05 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.568 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp240

+

phenylacetic acid

+

furfurylamine

+

phenanthrene-9-carboxaldehyde



benzyl isocyanide

24528346

Reaction ID UCExp240-11 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.788 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp240

+

phenylacetic acid

+

5-methylfurfurylamine

+

phenanthrene-9-carboxaldehyde



benzyl isocyanide

24528350

Reaction ID UCExp241-01 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.502 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp241

+

3,4methylenedioxyphenylacetic acid

+

methylamine

+

4-methoxybenzaldehyde

199



benzyl isocyanide

24534407

Reaction ID UCExp241-02 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.502 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp241

+

3,4methylenedioxyphenylacetic acid

+

methylamine

+

m-anisaldehyde



benzyl isocyanide

24534408

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCExp241-03 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.512 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp241

+

3,4methylenedioxyphenylacetic acid

+

methylamine

+

2-furaldehyde



benzyl isocyanide

24534403

Reaction ID UCExp241-14 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.565 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp241

+

3,4methylenedioxyphenylacetic acid

+

methylamine

+

veratraldehyde



benzyl isocyanide

24528359

Reaction ID UCExp241-15 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.565 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp241

+

+

+

200



3,4methylenedioxyphenylacetic acid

methylamine

veratraldehyde

benzyl isocyanide

24528359

Reaction ID UCExp241-16

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.565 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp241

+

3,4methylenedioxyphenylacetic acid

+

+

methylamine

veratraldehyde



benzyl isocyanide

24528359

benzylamine Reaction ID UCEXP150D-V1B155 Researcher Khalid Mirza/ Emily Messner Reaction Type Ugi Solvent methanol Limiting Reactant 0.404 M Precipitate Yes but the aldehyde alone is not soluble in methanol Yield 59 % Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp150

+

crotonic acid

+

benzylamine

+

phenanthrene-9-carboxaldehyde



t-butyl isocyanide

21105601

Reaction ID UCEXP156B-V1B155 Researcher Emily Messner Reaction Type Ugi Solvent methanol Limiting Reactant 0.678 M Precipitate Yes but reactants initially insoluble Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp156

+

crotonic acid

+

benzylamine

+

phenanthrene-9-carboxaldehyde

Reaction ID UCEXP159C-V1B18 Researcher Reaction Type

Emily Messner Ugi

201



t-butyl isocyanide

21106075

Solvent methanol Limiting Reactant 0.661 M Precipitate Yes but the aldehyde alone is not soluble in methanol Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp159

+

4-chlorophenylacetic acid

+

benzylamine

+

phenanthrene-9-carboxaldehyde



n-butyl isocyanide

21106077

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCEXP171D/V2B4 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.219 M Precipitate Yes Product No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp171

+

1-pyrenebutyric acid

+

+

benzylamine

o-vanillin



t-butyl isocyanide

21105846

Reaction ID UCEXP173G/V2B19 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.223 M Precipitate Yes Yield - % Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp173

+

phenylpropynoic acid

+

benzylamine

+

3,5-dimethoxybenzaldehyde



n-butyl isocyanide

21105845

Reaction ID UCEXP175D Researcher Khalid Mirza/ Emily Messner Reaction Type Ugi Solvent methanol Limiting Reactant 0.398 M Precipitate Yes but the aldehyde alone is not soluble in methanol Yield - % Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp175

+

4-chlorophenylacetic acid

+

benzylamine

+

phenanthrene-9-carboxaldehyde

Reaction ID UCEXP181-065V2 Researcher

Khalid Mirza

202



n-butyl isocyanide

21106077

Reaction Type Ugi Solvent methanol Limiting Reactant 0.223 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

+

D-(−)-Quinic acid

+

benzylamine

+

3,5-dimethoxybenzaldehyde



t-butyl isocyanide

24528104

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCEXP181-071V2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.221 M Precipitate Yes Product No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

+

mandelic acid

+

+

benzylamine

benzaldehyde



tosylmethyl isocyanide

24528531

Reaction ID UCEXP181-084V2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.225 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

+

mandelic acid

+

benzylamine

+

3-methoxybenzaldehyde



n-butyl isocyanide

24528119

Reaction ID UCEXP181-124V2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.219 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

+

3-(4methoxyphenyl)propionic acid

+

benzylamine

+

2-hydroxybenzaldehyde

Reaction ID UCEXP185-2

203



tosylmethyl isocyanide

24528152

Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.409 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp185

+

methacrylic acid

+

benzylamine

+

4-(trifluoromethyl)benzaldehyde



t-butyl isocyanide

21111671

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCEXP187-2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.06 M Precipitate Yes Yield - % Comments Reference http://usefulchem.wikispaces.com/Exp187

+

methacrylic acid

+

benzylamine

+

4-(trifluoromethyl)benzaldehyde



t-butyl isocyanide

21111671

Reaction ID UCEXP188-2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.225 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp188

+

methacrylic acid

+

benzylamine

+

4-(trifluoromethyl)benzaldehyde



t-butyl isocyanide

21111671

Reaction ID UCEXP214C Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.404 M Precipitate Yes but the aldehyde alone is not soluble in methanol Yield - % Comments Reference http://usefulchem.wikispaces.com/Exp214

+

crotonic acid

+

benzylamine

+

phenanthrene-9-carboxaldehyde

Reaction ID UCEXP215B

204



t-butyl isocyanide

21105601

Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 0.678 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp215

+

crotonic acid

+

benzylamine

+

phenanthrene-9-carboxaldehyde



t-butyl isocyanide

21105601

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCEXP215F Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 0.661 M Precipitate Yes but not at room temperature Yield - % Comments Reference http://usefulchem.wikispaces.com/Exp215

+

4-chlorophenylacetic acid

+

benzylamine

+

phenanthrene-9-carboxaldehyde



n-butyl isocyanide

21106077

Reaction ID UCEXP217-1 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 0.384 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp217

+

4-chlorophenylacetic acid

+

benzylamine

+

phenanthrene-9-carboxaldehyde



n-butyl isocyanide

21106077

Reaction ID UCEXP217-2 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 0.383 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp217

+

crotonic acid

+

benzylamine

+

phenanthrene-9-carboxaldehyde

Reaction ID UCEXP231-1 Researcher

Khalid Mirza

205



t-butyl isocyanide

21105601

Reaction Type Ugi Solvent acetonitrile Limiting Reactant 1.538 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp231

+

formic acid

+

+

benzylamine

4-methylbenzaldehyde



tosylmethyl isocyanide

24528186

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCEXP231-2 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1 M Precipitate aldehyde insoluble at this concentration Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp231

+

crotonic acid

+

benzylamine

+

phenanthrene-9-carboxaldehyde



t-butyl isocyanide

21105601

Reaction ID UCEXP233-1 Researcher David Bulger Reaction Type Ugi Solvent methanol Limiting Reactant 0.921 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp233

+

1-aminocyclohexane-1carboxylic acid

+

benzylamine

+

3,5-dimethoxybenzaldehyde



t-butyl isocyanide

24534439

Reaction ID UCEXP233-10 Researcher David Bulger Reaction Type Ugi Solvent methanol Limiting Reactant 1.018 M Precipitate Yes Product Pending Comments Reference http://usefulchem.wikispaces.com/Exp233

+

phenylpropynoic acid

+

benzylamine

+

3,5-dimethoxybenzaldehyde

Reaction ID UCEXP233-11 Researcher

David Bulger

206



cyclohexylisocyanide

23078615

Reaction Type Ugi Solvent methanol Limiting Reactant 1.021 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp233

+

Boc-Pro-OH

+

benzylamine

+

3,5-dimethoxybenzaldehyde



t-butyl isocyanide

24528262

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCEXP233-12 Researcher David Bulger Reaction Type Ugi Solvent methanol Limiting Reactant 1.018 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp233

+

Boc-Pro-OH

+

benzylamine

+

3,5-dimethoxybenzaldehyde



cyclohexylisocyanide

24528263

Reaction ID UCEXP233-2 Researcher David Bulger Reaction Type Ugi Solvent methanol Limiting Reactant 0.92 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp233

+

1-aminocyclohexane-1carboxylic acid

+

benzylamine

+

3,5-dimethoxybenzaldehyde



cyclohexylisocyanide

24534440

Reaction ID UCEXP233-3 Researcher David Bulger Reaction Type Ugi Solvent methanol Limiting Reactant 0.918 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp233

+

phenylpropynoic acid

+

benzylamine

+

3,5-dimethoxybenzaldehyde

Reaction ID UCEXP233-4 Researcher Reaction Type

David Bulger Ugi

207



t-butyl isocyanide

24528265

Solvent methanol Limiting Reactant 0.917 M Precipitate Yes Product Pending Comments Reference http://usefulchem.wikispaces.com/Exp233

+

phenylpropynoic acid

+

benzylamine

+

3,5-dimethoxybenzaldehyde



cyclohexylisocyanide

23078615

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCEXP233-5 Researcher David Bulger Reaction Type Ugi Solvent methanol Limiting Reactant 0.919 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp233

+

Boc-Pro-OH

+

benzylamine

+

3,5-dimethoxybenzaldehyde



t-butyl isocyanide

24528262

Reaction ID UCEXP233-6 Researcher David Bulger Reaction Type Ugi Solvent methanol Limiting Reactant 0.917 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp233

+

Boc-Pro-OH

+

benzylamine

+

3,5-dimethoxybenzaldehyde



cyclohexylisocyanide

24528263

Reaction ID UCEXP233-7 Researcher David Bulger Reaction Type Ugi Solvent methanol Limiting Reactant 1.02 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp233

+

1-aminocyclohexane-1carboxylic acid

+

benzylamine

+

3,5-dimethoxybenzaldehyde

Reaction ID UCEXP233-8 Researcher Reaction Type

David Bulger Ugi

208



t-butyl isocyanide

24534439

Solvent methanol Limiting Reactant 1.018 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp233

+

1-aminocyclohexane-1carboxylic acid

+

benzylamine

+

3,5-dimethoxybenzaldehyde



cyclohexylisocyanide

24534440

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCEXP233-9 Researcher David Bulger Reaction Type Ugi Solvent methanol Limiting Reactant 1.021 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp233

+

phenylpropynoic acid

+

benzylamine

+

3,5-dimethoxybenzaldehyde



t-butyl isocyanide

24528265

Reaction ID UCEXP234-1 Researcher David Bulger Reaction Type Ugi Solvent methanol Limiting Reactant 1.004 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp234

+

phenylpropynoic acid

+

+

3,5Bis(trifluoromethyl)benzaldehyde

benzylamine



t-butyl isocyanide

24528266

Reaction ID UCEXP234-10 Researcher David Bulger Reaction Type Ugi Solvent methanol Limiting Reactant 0.916 M Precipitate Reactants insoluble Comments Reference http://usefulchem.wikispaces.com/Exp234

+

Boc-L-Serine

+

benzylamine

+

3,5-dimethoxybenzaldehyde

Reaction ID UCEXP234-2 Researcher Reaction Type

David Bulger Ugi

209



cyclohexylisocyanide

24528267

Solvent methanol Limiting Reactant 1.002 M Precipitate Yes Product Pending Comments Reference http://usefulchem.wikispaces.com/Exp234

+

phenylpropynoic acid

+

+

3,5Bis(trifluoromethyl)benzaldehyde

benzylamine



cyclohexylisocyanide

23078614

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCEXP234-3 Researcher David Bulger Reaction Type Ugi Solvent methanol Limiting Reactant 1.004 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp234

+

phenylpropynoic acid

+

+

3,5Bis(trifluoromethyl)benzaldehyde

benzylamine



t-butyl isocyanide

24528266

Reaction ID UCEXP234-4 Researcher David Bulger Reaction Type Ugi Solvent methanol Limiting Reactant 1.002 M Precipitate Yes Product Pending Comments Reference http://usefulchem.wikispaces.com/Exp234

+

phenylpropynoic acid

+

+

3,5Bis(trifluoromethyl)benzaldehyde

benzylamine



cyclohexylisocyanide

23078614

Reaction ID UCEXP234-5 Researcher David Bulger Reaction Type Ugi Solvent methanol Limiting Reactant 0.918 M Precipitate Reactants insoluble Comments Reference http://usefulchem.wikispaces.com/Exp234

+

Fmoc-Diglycine

+

benzylamine

Reaction ID UCEXP234-6

+

3,5-dimethoxybenzaldehyde

210



t-butyl isocyanide

24528270

Researcher David Bulger Reaction Type Ugi Solvent methanol Limiting Reactant 0.916 M Precipitate Reactants insoluble Comments Reference http://usefulchem.wikispaces.com/Exp234

+

Fmoc-Diglycine

+

benzylamine

+

3,5-dimethoxybenzaldehyde



cyclohexylisocyanide

24528271

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCEXP234-7 Researcher David Bulger Reaction Type Ugi Solvent methanol Limiting Reactant 0.918 M Precipitate Reactants insoluble Comments Reference http://usefulchem.wikispaces.com/Exp234

+

Boc-diglycine

+

benzylamine

+

3,5-dimethoxybenzaldehyde



t-butyl isocyanide

24528272

Reaction ID UCEXP234-8 Researcher David Bulger Reaction Type Ugi Solvent methanol Limiting Reactant 0.916 M Precipitate Reactants insoluble Comments Reference http://usefulchem.wikispaces.com/Exp234

+

Boc-diglycine

+

benzylamine

+

3,5-dimethoxybenzaldehyde



cyclohexylisocyanide

24528273

Reaction ID UCEXP234-9 Researcher David Bulger Reaction Type Ugi Solvent methanol Limiting Reactant 0.918 M Precipitate Reactants insoluble Comments Reference http://usefulchem.wikispaces.com/Exp234

+

Boc-L-Serine

+

benzylamine

+

3,5-dimethoxybenzaldehyde

Reaction ID UCExp236-03 Researcher Reaction Type

Khalid Mirza Ugi

211



t-butyl isocyanide

24528274

Solvent methanol Limiting Reactant 0.614 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp236

+

3,3'-dichloropivalic acid

+

benzylamine

+

4-(trifluoromethyl)benzaldehyde



n-butyl isocyanide

24528277

Reaction ID UCExp236-11

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.65 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp236

+

formic acid

+

benzylamine

+

4-(trifluoromethyl)benzaldehyde



t-butyl isocyanide

24528284

Reaction ID UCExp236-24 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.63 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp236

+

methacrylic acid

+

benzylamine

+

4-(trifluoromethyl)benzaldehyde



n-butyl isocyanide

24528297

Reaction ID UCExp236-26 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.612 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp236

+

3,3'-dichloropivalic acid

+

benzylamine

+

5-bromo-2thiophenecarboxaldehyde

Reaction ID UCExp238-04 Researcher Reaction Type Solvent

Khalid Mirza Ugi THF

212



t-butyl isocyanide

24528299

Limiting Reactant 1.866 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp238

+

crotonic acid

+

benzylamine

+

phenanthrene-9-carboxaldehyde



cyclohexylisocyanide

24528306

Reaction ID UCExp238-16

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.906 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp238

+

crotonic acid

+

benzylamine

+

phenanthrene-9-carboxaldehyde



t-butyl isocyanide

21105601

Reaction ID UCExp238-28 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.674 M Precipitate Yes Product Awaiting Characterization Comments Reference http://usefulchem.wikispaces.com/Exp238

+

Boc-Gly-OH

+

benzylamine

+

phenanthrene-9-carboxaldehyde



cyclohexylisocyanide

24528328

Reaction ID UCExp238-40 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.706 M Precipitate Yes Product Awaiting Characterization Comments Reference http://usefulchem.wikispaces.com/Exp238

+

Boc-Gly-OH

+

benzylamine

+

phenanthrene-9-carboxaldehyde

Reaction ID UCExp241-48 Researcher Reaction Type Solvent

Khalid Mirza Ugi methanol

213



t-butyl isocyanide

24528340

Limiting Reactant 0.734 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp241

+

3,4methylenedioxyphenylacetic acid

+

benzylamine

+

2,4-dimethylbenzaldehyde



t-butyl isocyanide

24528381

Boc-diglycine

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCEXP234-7 Researcher David Bulger Reaction Type Ugi Solvent methanol Limiting Reactant 0.918 M Precipitate Reactants insoluble Comments Reference http://usefulchem.wikispaces.com/Exp234

+

Boc-diglycine

+

benzylamine

+

3,5-dimethoxybenzaldehyde



t-butyl isocyanide

24528272

Reaction ID UCEXP234-8 Researcher David Bulger Reaction Type Ugi Solvent methanol Limiting Reactant 0.916 M Precipitate Reactants insoluble Comments Reference http://usefulchem.wikispaces.com/Exp234

+

Boc-diglycine

+

benzylamine

+

3,5-dimethoxybenzaldehyde



cyclohexylisocyanide

24528273

Boc-Gly-OH Reaction ID UCEXP052E Researcher Alicia Holsey Reaction Type Ugi Solvent methanol Limiting Reactant 0.223 M Precipitate Yes Yield 32 % Comments 1M solutions of the starting materials was made Reference http://usefulchem.wikispaces.com/Exp052

+

+

+

214



Boc-Gly-OH

5-methylfurfurylamine

piperonal

t-butyl isocyanide

10481872

Reaction ID UCEXP064C

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.393 M Precipitate Yes Yield 43.8 % Comments Solution was made up to 4 mL - methanol amount probably closer to 3 mL Reference http://usefulchem.wikispaces.com/Exp064

+

Boc-Gly-OH

+

5-methylfurfurylamine

+

veratraldehyde



benzyl isocyanide

10481870

Reaction ID UCEXP086B Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.402 M Precipitate Yes Yield 38 % Comments Solution was made up to 4 mL - methanol amount probably closer to 3 mL Reference http://usefulchem.wikispaces.com/Exp086

+

Boc-Gly-OH

+

5-methylfurfurylamine

+

benzaldehyde



t-butyl isocyanide

10481766

Reaction ID UCEXP099C Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.405 M Precipitate Yes Yield 47.2 % Comments Solution was made up to 4 mL - methanol amount probably closer to 3 mL Reference http://usefulchem.wikispaces.com/Exp099

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde

Reaction ID UCEXP104C Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.398 M

215



t-butyl isocyanide

21106059

Precipitate Yield Comments Reference

Yes 12 % Imine was preformed http://usefulchem.wikispaces.com/Exp104

+

Boc-Gly-OH

+

furfurylamine

+

veratraldehyde



t-butyl isocyanide

21106057

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCEXP108C Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.393 M Precipitate Yes Yield 20.4 % Comments Imine was preformed Reference http://usefulchem.wikispaces.com/Exp108

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde



benzyl isocyanide

21106009

Reaction ID UCEXP109C Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.222 M Precipitate Yes Product Pending Comments Imine was preformed Reference http://usefulchem.wikispaces.com/Exp109

+

+

5-(trifluoromethyl)-2furylmethylamine

Boc-Gly-OH

+

benzaldehyde



benzyl isocyanide

21105565

Reaction ID UCEXP201-01 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.039 M Precipitate Yes Yield 50.73 % Comments Automated liquid handling Reference http://usefulchem.wikispaces.com/Exp201

+

+

+

216



Boc-Gly-OH

furfurylamine

benzaldehyde

t-butyl isocyanide

21106059

Reaction ID UCEXP201-02 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.019 M Precipitate Yes Yield 59.07 % Comments Automated liquid handling Reference http://usefulchem.wikispaces.com/Exp201

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde



t-butyl isocyanide

21106059

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCEXP201-03 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.018 M Precipitate Yes Yield 61.55 % Comments Automated liquid handling Reference http://usefulchem.wikispaces.com/Exp201

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde



t-butyl isocyanide

21106059

Reaction ID UCEXP201-04 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.007 M Precipitate Yes Yield 60.31 % Comments Automated liquid handling Reference http://usefulchem.wikispaces.com/Exp201

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde



t-butyl isocyanide

21106059

Reaction ID UCEXP201-05 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.015 M Precipitate Yes Yield 60.2 % Comments Automated liquid handling Reference http://usefulchem.wikispaces.com/Exp201

+

+

+

217



Boc-Gly-OH

furfurylamine

benzaldehyde

t-butyl isocyanide

21106059

Reaction ID UCEXP201-06 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.998 M Precipitate Yes Yield 69.22 % Comments Automated liquid handling Reference http://usefulchem.wikispaces.com/Exp201

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde



t-butyl isocyanide

21106059

Reaction ID UCEXP201-07 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.289 M Precipitate Yes Yield 52.42 % Comments Automated liquid handling Reference http://usefulchem.wikispaces.com/Exp201

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde



t-butyl isocyanide

21106059

Reaction ID UCEXP201-08 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.287 M Precipitate Yes Yield 44.64 % Comments Automated liquid handling Reference http://usefulchem.wikispaces.com/Exp201

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde

Reaction ID UCEXP201-09 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.287 M Precipitate Yes Yield 50.28 %

218



t-butyl isocyanide

21106059

Comments Reference

Automated liquid handling http://usefulchem.wikispaces.com/Exp201

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde



t-butyl isocyanide

21106059

Reaction ID UCEXP201-10

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.286 M Precipitate Yes Yield 54.79 % Comments Automated liquid handling Reference http://usefulchem.wikispaces.com/Exp201

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde



t-butyl isocyanide

21106059

Reaction ID UCEXP201-11 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.287 M Precipitate Yes Yield 53.43 % Comments Automated liquid handling Reference http://usefulchem.wikispaces.com/Exp201

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde



t-butyl isocyanide

21106059

Reaction ID UCEXP201-12 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.286 M Precipitate Yes Yield 54.67 % Comments Automated liquid handling Reference http://usefulchem.wikispaces.com/Exp201

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde

Reaction ID UCEXP201-13 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.074 M

219



t-butyl isocyanide

21106059

Precipitate Yield Comments Reference

Yes 0.34 % Automated liquid handling http://usefulchem.wikispaces.com/Exp201

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde



t-butyl isocyanide

21106059

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCEXP201-14 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.074 M Precipitate Yes Yield 1.35 % Comments Automated liquid handling Reference http://usefulchem.wikispaces.com/Exp201

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde



t-butyl isocyanide

21106059

Reaction ID UCEXP201-15 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.074 M Precipitate Yes Yield 10.37 % Comments Automated liquid handling Reference http://usefulchem.wikispaces.com/Exp201

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde



t-butyl isocyanide

21106059

Reaction ID UCEXP201-16 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.074 M Precipitate Yes Yield 16.35 % Comments Automated liquid handling Reference http://usefulchem.wikispaces.com/Exp201

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde

220



t-butyl isocyanide

21106059

Reaction ID UCEXP201-17 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.074 M Precipitate Yes Yield 8.68 % Comments Automated liquid handling Reference http://usefulchem.wikispaces.com/Exp201

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde



t-butyl isocyanide

21106059

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCEXP201-18 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.074 M Precipitate Yes Yield 5.64 % Comments Automated liquid handling Reference http://usefulchem.wikispaces.com/Exp201

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde



t-butyl isocyanide

21106059

Reaction ID UCEXP201-19 Researcher Khalid Mirza Reaction Type Ugi Solvent ethanol Limiting Reactant 0.289 M Precipitate Yes Yield 51.52 % Comments Automated liquid handling Reference http://usefulchem.wikispaces.com/Exp201

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde



t-butyl isocyanide

21106059

Reaction ID UCEXP201-20 Researcher Khalid Mirza Reaction Type Ugi Solvent ethanol Limiting Reactant 0.287 M Precipitate Yes Yield 46.78 % Comments Automated liquid handling Reference http://usefulchem.wikispaces.com/Exp201

+

+

+

221



Boc-Gly-OH

furfurylamine

benzaldehyde

t-butyl isocyanide

21106059

Reaction ID UCEXP201-21 Researcher Khalid Mirza Reaction Type Ugi Solvent ethanol Limiting Reactant 0.287 M Precipitate Yes Yield 51.29 % Comments Automated liquid handling Reference http://usefulchem.wikispaces.com/Exp201

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde



t-butyl isocyanide

21106059

Reaction ID UCEXP201-22 Researcher Khalid Mirza Reaction Type Ugi Solvent ethanol Limiting Reactant 0.286 M Precipitate Yes Yield 54.11 % Comments Automated liquid handling Reference http://usefulchem.wikispaces.com/Exp201

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde



t-butyl isocyanide

21106059

Reaction ID UCEXP201-23 Researcher Khalid Mirza Reaction Type Ugi Solvent ethanol Limiting Reactant 0.287 M Precipitate Yes Yield 55.91 % Comments Automated liquid handling Reference http://usefulchem.wikispaces.com/Exp201

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde

Reaction ID UCEXP201-24 Researcher Khalid Mirza Reaction Type Ugi Solvent ethanol Limiting Reactant 0.286 M Precipitate Yes Yield 58.28 %

222



t-butyl isocyanide

21106059

Comments Reference

Automated liquid handling http://usefulchem.wikispaces.com/Exp201

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde



t-butyl isocyanide

21106059

Reaction ID UCEXP201-25

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Researcher Khalid Mirza Reaction Type Ugi Solvent ethanol Limiting Reactant 0.074 M Precipitate Yes Yield 1.24 % Comments Automated liquid handling Reference http://usefulchem.wikispaces.com/Exp201

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde



t-butyl isocyanide

21106059

Reaction ID UCEXP201-26 Researcher Khalid Mirza Reaction Type Ugi Solvent ethanol Limiting Reactant 0.074 M Precipitate Yes Yield 2.25 % Comments Automated liquid handling Reference http://usefulchem.wikispaces.com/Exp201

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde



t-butyl isocyanide

21106059

Reaction ID UCEXP201-27 Researcher Khalid Mirza Reaction Type Ugi Solvent ethanol Limiting Reactant 0.074 M Precipitate Yes Yield 7.78 % Comments Automated liquid handling Reference http://usefulchem.wikispaces.com/Exp201

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde

Reaction ID UCEXP201-28 Researcher Khalid Mirza Reaction Type Ugi Solvent ethanol Limiting Reactant 0.074 M

223



t-butyl isocyanide

21106059

Precipitate Yield Comments Reference

Yes 1.13 % Automated liquid handling http://usefulchem.wikispaces.com/Exp201

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde



t-butyl isocyanide

21106059

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCEXP201-29 Researcher Khalid Mirza Reaction Type Ugi Solvent ethanol Limiting Reactant 0.074 M Precipitate Yes Yield 0.79 % Comments Automated liquid handling Reference http://usefulchem.wikispaces.com/Exp201

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde



t-butyl isocyanide

21106059

Reaction ID UCEXP201-30 Researcher Khalid Mirza Reaction Type Ugi Solvent ethanol Limiting Reactant 0.074 M Precipitate Yes Yield 0.23 % Comments Automated liquid handling Reference http://usefulchem.wikispaces.com/Exp201

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde



t-butyl isocyanide

21106059

Reaction ID UCEXP201-31 Researcher Khalid Mirza Reaction Type Ugi Solvent acetonitrile Limiting Reactant 0.289 M Precipitate Yes Yield 39.23 % Comments Automated liquid handling Reference http://usefulchem.wikispaces.com/Exp201

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde

224



t-butyl isocyanide

21106059

Reaction ID UCEXP201-32 Researcher Khalid Mirza Reaction Type Ugi Solvent acetonitrile Limiting Reactant 0.287 M Precipitate Yes Yield 40.58 % Comments Automated liquid handling Reference http://usefulchem.wikispaces.com/Exp201

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde



t-butyl isocyanide

21106059

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCEXP201-33 Researcher Khalid Mirza Reaction Type Ugi Solvent acetonitrile Limiting Reactant 0.287 M Precipitate Yes Yield 43.85 % Comments Automated liquid handling Reference http://usefulchem.wikispaces.com/Exp201

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde



t-butyl isocyanide

21106059

Reaction ID UCEXP201-34 Researcher Khalid Mirza Reaction Type Ugi Solvent acetonitrile Limiting Reactant 0.286 M Precipitate Yes Yield 35.4 % Comments Automated liquid handling Reference http://usefulchem.wikispaces.com/Exp201

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde



t-butyl isocyanide

21106059

Reaction ID UCEXP201-35 Researcher Khalid Mirza Reaction Type Ugi Solvent acetonitrile Limiting Reactant 0.287 M Precipitate Yes Yield 41.37 % Comments Automated liquid handling Reference http://usefulchem.wikispaces.com/Exp201

+

+

+

225



Boc-Gly-OH

furfurylamine

benzaldehyde

t-butyl isocyanide

21106059

Reaction ID UCEXP201-36 Researcher Khalid Mirza Reaction Type Ugi Solvent acetonitrile Limiting Reactant 0.286 M Precipitate Yes Yield 39.23 % Comments Automated liquid handling Reference http://usefulchem.wikispaces.com/Exp201

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde



t-butyl isocyanide

21106059

Reaction ID UCEXP201-37 Researcher Khalid Mirza Reaction Type Ugi Solvent acetonitrile Limiting Reactant 0.074 M Precipitate Yes Yield 0.68 % Comments Automated liquid handling Reference http://usefulchem.wikispaces.com/Exp201

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde



t-butyl isocyanide

21106059

Reaction ID UCEXP201-38 Researcher Khalid Mirza Reaction Type Ugi Solvent acetonitrile Limiting Reactant 0.074 M Precipitate Yes Yield 1.8 % Comments Automated liquid handling Reference http://usefulchem.wikispaces.com/Exp201

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde

Reaction ID UCEXP201-39 Researcher Khalid Mirza Reaction Type Ugi Solvent acetonitrile Limiting Reactant 0.002 M Precipitate Yes Yield 1.01 %

226



t-butyl isocyanide

21106059

Comments Reference

Automated liquid handling http://usefulchem.wikispaces.com/Exp201

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde



t-butyl isocyanide

21106059

Reaction ID UCEXP201-40

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Researcher Khalid Mirza Reaction Type Ugi Solvent acetonitrile Limiting Reactant 0.074 M Precipitate Yes Yield 0.9 % Comments Automated liquid handling Reference http://usefulchem.wikispaces.com/Exp201

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde



t-butyl isocyanide

21106059

Reaction ID UCEXP201-41 Researcher Khalid Mirza Reaction Type Ugi Solvent acetonitrile Limiting Reactant 0.074 M Precipitate Yes Yield 1.01 % Comments Automated liquid handling Reference http://usefulchem.wikispaces.com/Exp201

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde



t-butyl isocyanide

21106059

Reaction ID UCEXP201-42 Researcher Khalid Mirza Reaction Type Ugi Solvent acetonitrile Limiting Reactant 0.074 M Precipitate Yes Yield 0.45 % Comments Automated liquid handling Reference http://usefulchem.wikispaces.com/Exp201

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde

Reaction ID UCEXP201-43 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 0.289 M

227



t-butyl isocyanide

21106059

Precipitate Yield Comments Reference

Yes 6.54 % Automated liquid handling http://usefulchem.wikispaces.com/Exp201

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde



t-butyl isocyanide

21106059

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCEXP201-44 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 0.287 M Precipitate Yes Yield 7.89 % Comments Automated liquid handling Reference http://usefulchem.wikispaces.com/Exp201

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde



t-butyl isocyanide

21106059

Reaction ID UCEXP201-45 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 0.287 M Precipitate Yes Yield 10.03 % Comments Automated liquid handling Reference http://usefulchem.wikispaces.com/Exp201

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde



t-butyl isocyanide

21106059

Reaction ID UCEXP201-46 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 0.286 M Precipitate Yes Yield 9.92 % Comments Automated liquid handling Reference http://usefulchem.wikispaces.com/Exp201

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde

228



t-butyl isocyanide

21106059

Reaction ID UCEXP201-47 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 0.287 M Precipitate Yes Yield 7.44 % Comments Automated liquid handling Reference http://usefulchem.wikispaces.com/Exp201

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde



t-butyl isocyanide

21106059

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCEXP201-48 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 0.286 M Precipitate Yes Yield 12.06 % Comments Automated liquid handling Reference http://usefulchem.wikispaces.com/Exp201

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde



t-butyl isocyanide

21106059

Reaction ID UCEXP217-3 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 0.383 M Precipitate Yes Product Pending Comments Reference http://usefulchem.wikispaces.com/Exp217

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde



t-butyl isocyanide

21106059

Reaction ID UCEXP217-4 Researcher Khalid Mirza Reaction Type Ugi Solvent DMSO Limiting Reactant 0.383 M Precipitate Yes Product Pending Comments Reference http://usefulchem.wikispaces.com/Exp217

+

+

+

229



Boc-Gly-OH

furfurylamine

benzaldehyde

t-butyl isocyanide

21106059

Reaction ID UCEXP217-5 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 0.384 M Precipitate Yes Product Pending Comments Reference http://usefulchem.wikispaces.com/Exp217

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

+

Boc-Gly-OH

+

furfurylamine

+

phenanthrene-9-carboxaldehyde



n-butyl isocyanide

21105594

Reaction ID UCEXP222-1 Researcher Khalid Mirza Reaction Type Ugi Solvent DMSO Limiting Reactant 0.898 M Precipitate Yes Yield - % Comments Reference http://usefulchem.wikispaces.com/Exp222

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde



t-butyl isocyanide

21106059

Reaction ID UCEXP222-2 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 0.898 M Precipitate Yes Yield - % Comments Reference http://usefulchem.wikispaces.com/Exp222

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde

Reaction ID UCEXP222-3 Researcher Khalid Mirza Reaction Type Ugi Solvent DMSO Limiting Reactant 0.473 M Precipitate No Comments -

230



t-butyl isocyanide

21106059

Reference

http://usefulchem.wikispaces.com/Exp222

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde



t-butyl isocyanide

21106059

Reaction ID UCEXP222-4

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 0.473 M Precipitate Yes Yield - % Comments Reference http://usefulchem.wikispaces.com/Exp222

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde



t-butyl isocyanide

21106059

Reaction ID UCEXP225-1 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.631 M Precipitate Yes Yield - % Comments 0.5 mmol of isocyanide was added to 500uL of a 2M solution of aldehyde; amine and acid Reference http://usefulchem.wikispaces.com/Exp225

+

Boc-Gly-OH

+

furfurylamine

+

piperonal



t-butyl isocyanide

24528157

Reaction ID UCEXP225-2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.905 M Precipitate Yes Product Pending Comments 0.5 mmol of isocyanide was added to 500uL of a 2M solution of aldehyde; amine and acid Reference http://usefulchem.wikispaces.com/Exp225

+

Boc-Gly-OH

+

furfurylamine

+

piperonal

Reaction ID UCEXP225-3 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.888 M Precipitate Yes

231



n-butyl isocyanide

24528158

Product Comments Reference

Pending 0.5 mmol of isocyanide was added to 500uL of a 2M solution of aldehyde; amine and acid http://usefulchem.wikispaces.com/Exp225

+

Boc-Gly-OH

+

furfurylamine

+

piperonal



1-pentyl isocyanide

24528159

Reaction ID UCEXP225-4

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.889 M Precipitate Yes Product Pending Comments 0.5 mmol of isocyanide was added to 500uL of a 2M solution of aldehyde; amine and acid Reference http://usefulchem.wikispaces.com/Exp225

+

Boc-Gly-OH

+

furfurylamine

+

piperonal



cyclohexylisocyanide

24528160

Reaction ID UCEXP225-5 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.891 M Precipitate Yes Product Pending Comments 0.5 mmol of isocyanide was added to 500uL of a 2M solution of aldehyde; amine and acid Reference http://usefulchem.wikispaces.com/Exp225

+

Boc-Gly-OH

+

furfurylamine

+

piperonal



benzyl isocyanide

24528161

Reaction ID UCEXP225-6 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.438 M Precipitate No Comments 0.5 mmol of isocyanide was added to 500uL of a 2M solution of aldehyde; amine and acid Reference http://usefulchem.wikispaces.com/Exp225

+

Boc-Gly-OH

+

furfurylamine

+

piperonal

Reaction ID UCEXP225-7 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.879 M

232



tosylmethyl isocyanide

24528162

Precipitate Comments Reference

No 0.5 mmol of isocyanide was added to 500uL of a 2M solution of aldehyde; amine and acid http://usefulchem.wikispaces.com/Exp225

+

Boc-Gly-OH

+

furfurylamine

+



2-morpholinoethyl isocyanide

piperonal

24528163

Reaction ID UCEXP225-8

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.868 M Precipitate No Comments 0.5 mmol of isocyanide was added to 500uL of a 2M solution of aldehyde; amine and acid Reference http://usefulchem.wikispaces.com/Exp225

+

Boc-Gly-OH

+

furfurylamine

+



2-chloro-6methylphenyl isocyanide

piperonal

24528164

Reaction ID UCEXP232-01 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.098 M Precipitate Yes Product Pending Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde



t-butyl isocyanide

21106059

Reaction ID UCEXP232-02 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.098 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde

Reaction ID UCEXP232-03 Researcher Reaction Type

Khalid Mirza Ugi

233



n-butyl isocyanide

24528189

Solvent methanol Limiting Reactant 1.099 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde



1-pentyl isocyanide

24528190

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCEXP232-04 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.098 M Precipitate Yes Product Pending Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde



cyclohexylisocyanide

24528191

Reaction ID UCEXP232-05 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.098 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+



1,1,3,3tetramethylbutyl isocyanide

benzaldehyde

24528192

Reaction ID UCEXP232-06 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.083 M Precipitate Yes Product Pending Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+

4-methylbenzaldehyde

Reaction ID UCEXP232-07

234



t-butyl isocyanide

24528193

Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.082 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+

4-methylbenzaldehyde



n-butyl isocyanide

24528194

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCEXP232-08 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.083 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+

4-methylbenzaldehyde



1-pentyl isocyanide

24528195

Reaction ID UCEXP232-09 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.083 M Precipitate Yes Product Pending Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+

4-methylbenzaldehyde



cyclohexylisocyanide

24528196

Reaction ID UCEXP232-10 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.083 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+

4-methylbenzaldehyde

235



1,1,3,3tetramethylbutyl isocyanide

24528197

Reaction ID UCEXP232-11 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.029 M Precipitate Yes Product Pending Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+

4-(trifluoromethyl)benzaldehyde



t-butyl isocyanide

24528198

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCEXP232-12 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.028 M Precipitate Yes Product Pending Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+

4-(trifluoromethyl)benzaldehyde



n-butyl isocyanide

24528199

Reaction ID UCEXP232-13 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.029 M Precipitate Yes Product Pending Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+

4-(trifluoromethyl)benzaldehyde



1-pentyl isocyanide

24528200

Reaction ID UCEXP232-14 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.028 M Precipitate Yes Product Pending Comments Reference http://usefulchem.wikispaces.com/Exp232

+

+

+

236



Boc-Gly-OH

furfurylamine

4-(trifluoromethyl)benzaldehyde

cyclohexylisocyanide

21782441

Reaction ID UCEXP232-15 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.028 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+



1,1,3,3tetramethylbutyl isocyanide

4-(trifluoromethyl)benzaldehyde

24528201

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCEXP232-16 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.366 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+

crotonaldehyde



t-butyl isocyanide

24528202

Reaction ID UCEXP232-17 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.365 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+

crotonaldehyde



n-butyl isocyanide

24528203

Reaction ID UCEXP232-18 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.367 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

+

+

+

237



Boc-Gly-OH

furfurylamine

crotonaldehyde

1-pentyl isocyanide

24528204

Reaction ID UCEXP232-19 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.366 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+

crotonaldehyde



cyclohexylisocyanide

24528205

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCEXP232-20 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.366 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+



1,1,3,3tetramethylbutyl isocyanide

crotonaldehyde

24528206

Reaction ID UCEXP232-21 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.008 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+

diphenylacetaldehyde



t-butyl isocyanide

24528207

Reaction ID UCEXP232-22 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.007 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

+

+

+

238



Boc-Gly-OH

furfurylamine

diphenylacetaldehyde

n-butyl isocyanide

24528208

Reaction ID UCEXP232-23 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.008 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+

diphenylacetaldehyde



1-pentyl isocyanide

24528209

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCEXP232-24 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.008 M Precipitate Yes Product Pending Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+

diphenylacetaldehyde



cyclohexylisocyanide

24528210

Reaction ID UCEXP232-25 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.008 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+



1,1,3,3tetramethylbutyl isocyanide

diphenylacetaldehyde

24528211

Reaction ID UCEXP232-26 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.092 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

+

+

+

239



Boc-Gly-OH

furfurylamine

cyclohexancarboxaldehyde

t-butyl isocyanide

24528212

Reaction ID UCEXP232-27 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.092 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

+

Boc-Gly-OH

+

furfurylamine

+

cyclohexancarboxaldehyde



n-butyl isocyanide

24528213

Reaction ID UCEXP232-28 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.093 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+

cyclohexancarboxaldehyde



1-pentyl isocyanide

24528214

Reaction ID UCEXP232-29 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.092 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+

cyclohexancarboxaldehyde

Reaction ID UCEXP232-30 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.092 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

240



cyclohexylisocyanide

24528215

+

Boc-Gly-OH

+

furfurylamine

+



1,1,3,3tetramethylbutyl isocyanide

cyclohexancarboxaldehyde

24528216

Reaction ID UCEXP232-31

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.11 M Precipitate Yes Product Pending Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+

2-furaldehyde



t-butyl isocyanide

24528217

Reaction ID UCEXP232-32 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.11 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+

2-furaldehyde



n-butyl isocyanide

24528218

Reaction ID UCEXP232-33 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.111 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+

2-furaldehyde

Reaction ID UCEXP232-34 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.11 M Precipitate No Comments -

241



1-pentyl isocyanide

24528219

Reference

http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

+

furfurylamine

2-furaldehyde



cyclohexylisocyanide

24528220

Reaction ID UCEXP232-35 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.11 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

+

Boc-Gly-OH

+

+

furfurylamine



1,1,3,3tetramethylbutyl isocyanide

2-furaldehyde

24528221

Reaction ID UCEXP232-36 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.081 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+

2-hydroxybenzaldehyde



t-butyl isocyanide

24528222

Reaction ID UCEXP232-37 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.081 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+

2-hydroxybenzaldehyde

Reaction ID UCEXP232-38 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.081 M Precipitate No Comments -

242



n-butyl isocyanide

24528223

Reference

http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+

2-hydroxybenzaldehyde



1-pentyl isocyanide

24528224

Reaction ID UCEXP232-39 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.081 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

+

Boc-Gly-OH

+

furfurylamine

+

2-hydroxybenzaldehyde



cyclohexylisocyanide

24528225

Reaction ID UCEXP232-40 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.081 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+



1,1,3,3tetramethylbutyl isocyanide

2-hydroxybenzaldehyde

24528226

Reaction ID UCEXP232-41 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.083 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+

o-tolualdehyde

Reaction ID UCEXP232-42 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.083 M Precipitate No Comments -

243



t-butyl isocyanide

24528227

Reference

http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+

o-tolualdehyde



n-butyl isocyanide

24528228

Reaction ID UCEXP232-43 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.083 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

+

Boc-Gly-OH

+

furfurylamine

+

o-tolualdehyde



1-pentyl isocyanide

24528229

Reaction ID UCEXP232-44 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.083 M Precipitate Yes Product Pending Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+

o-tolualdehyde



cyclohexylisocyanide

24528230

Reaction ID UCEXP232-45 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.083 M Precipitate Yes Product Pending Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+

o-tolualdehyde

Reaction ID UCEXP232-46 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.066 M

244



1,1,3,3tetramethylbutyl isocyanide

24528231

Precipitate Product Comments Reference

Yes Pending http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+

4-methoxybenzaldehyde



t-butyl isocyanide

24528232

Reaction ID UCEXP232-47

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.066 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+

4-methoxybenzaldehyde



n-butyl isocyanide

24528233

Reaction ID UCEXP232-48 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.067 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+

4-methoxybenzaldehyde



1-pentyl isocyanide

24528234

Reaction ID UCEXP232-49 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.066 M Precipitate Yes Product Pending Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+

4-methoxybenzaldehyde

Reaction ID UCEXP232-50 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.066 M

245



cyclohexylisocyanide

24528235

Precipitate Comments Reference

No http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+



1,1,3,3tetramethylbutyl isocyanide

4-methoxybenzaldehyde

24528236

Reaction ID UCEXP232-51

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.106 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+

hexanaldehyde



t-butyl isocyanide

24528237

Reaction ID UCEXP232-52 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.105 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+

hexanaldehyde



n-butyl isocyanide

24528238

Reaction ID UCEXP232-53 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.106 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+

hexanaldehyde

Reaction ID UCEXP232-54 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.106 M

246



1-pentyl isocyanide

24528239

Precipitate Comments Reference

No http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+

hexanaldehyde



cyclohexylisocyanide

24528240

Reaction ID UCEXP232-55

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.106 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+



1,1,3,3tetramethylbutyl isocyanide

hexanaldehyde

24528241

Reaction ID UCEXP232-56 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.109 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+

trans-2-hexenal



t-butyl isocyanide

24528242

Reaction ID UCEXP232-57 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.109 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+

trans-2-hexenal

Reaction ID UCEXP232-58 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.109 M

247



n-butyl isocyanide

24528243

Precipitate Comments Reference

No http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

+

furfurylamine

trans-2-hexenal



1-pentyl isocyanide

24528243

Reaction ID UCEXP232-59

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.109 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

+

furfurylamine

trans-2-hexenal



cyclohexylisocyanide

24528244

Reaction ID UCEXP232-60 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.109 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

+

furfurylamine



1,1,3,3tetramethylbutyl isocyanide

trans-2-hexenal

24528245

Reaction ID UCEXP232-61 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.069 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+

2-phenylpropionaldehyde

Reaction ID UCEXP232-62 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.069 M

248



t-butyl isocyanide

24534409

Precipitate Comments Reference

No http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+

2-phenylpropionaldehyde



n-butyl isocyanide

24534417

Reaction ID UCEXP232-63

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.07 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+

2-phenylpropionaldehyde



1-pentyl isocyanide

24534418

Reaction ID UCEXP232-64 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.069 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+

2-phenylpropionaldehyde



cyclohexylisocyanide

24534419

Reaction ID UCEXP232-65 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.069 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+

2-phenylpropionaldehyde

Reaction ID UCEXP232-66 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.067 M

249



1,1,3,3tetramethylbutyl isocyanide

24534420

Precipitate Product Comments Reference

Yes Pending http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+

m-anisaldehyde



t-butyl isocyanide

24528251

Reaction ID UCEXP232-67

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.068 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+

m-anisaldehyde



n-butyl isocyanide

24528252

Reaction ID UCEXP232-68 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.067 M Precipitate Yes Product Pending Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+

m-anisaldehyde



1-pentyl isocyanide

24528253

Reaction ID UCEXP232-69 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.067 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+

m-anisaldehyde

Reaction ID UCEXP232-70 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.067 M

250



cyclohexylisocyanide

24528254

Precipitate Comments Reference

No http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+



1,1,3,3tetramethylbutyl isocyanide

m-anisaldehyde

24528255

Reaction ID UCEXP232-71

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.106 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+

2-ethylbutyraldehyde



t-butyl isocyanide

24528256

Reaction ID UCEXP232-72 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.105 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+

2-ethylbutyraldehyde



n-butyl isocyanide

24528257

Reaction ID UCEXP232-73 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.106 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+

2-ethylbutyraldehyde

Reaction ID UCEXP232-74 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.105 M

251



1-pentyl isocyanide

24528258

Precipitate Comments Reference

No http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

+

furfurylamine

2-ethylbutyraldehyde



cyclohexylisocyanide

24528259

Reaction ID UCEXP232-75

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.105 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

+

furfurylamine



1,1,3,3tetramethylbutyl isocyanide

2-ethylbutyraldehyde

24528260

Reaction ID UCExp235-1 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1 M Precipitate Yes Product No Comments Reference http://usefulchem.wikispaces.com/Exp235

+

Boc-Gly-OH

+

furfurylamine

+

4-(trifluoromethyl)benzaldehyde



t-butyl isocyanide

24528198

Reaction ID UCExp235-2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1 M Precipitate Yes Product No Comments Reference http://usefulchem.wikispaces.com/Exp235

+

Boc-Gly-OH

+

furfurylamine

+

4-(trifluoromethyl)benzaldehyde

Reaction ID UCExp238-25 Researcher Reaction Type

Khalid Mirza Ugi

252



cyclohexylisocyanide

21782441

Solvent THF Limiting Reactant 1.686 M Precipitate Yes Product Awaiting Characterization Comments Reference http://usefulchem.wikispaces.com/Exp238

+

Boc-Gly-OH

+

2-chloroaniline

+

phenanthrene-9-carboxaldehyde



cyclohexylisocyanide

24528325

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCExp238-26 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.684 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp238

+

Boc-Gly-OH

+

3-chloroaniline

+

phenanthrene-9-carboxaldehyde



cyclohexylisocyanide

24528326

Reaction ID UCExp238-27 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.726 M Precipitate Yes Product Awaiting Characterization Comments Reference http://usefulchem.wikispaces.com/Exp238

+

+

Boc-Gly-OH

aniline

+

phenanthrene-9-carboxaldehyde



cyclohexylisocyanide

24528327

Reaction ID UCExp238-28 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.674 M Precipitate Yes Product Awaiting Characterization Comments Reference http://usefulchem.wikispaces.com/Exp238

+

Boc-Gly-OH

+

benzylamine

+

phenanthrene-9-carboxaldehyde

Reaction ID UCExp238-29 Researcher

Khalid Mirza

253



cyclohexylisocyanide

24528328

Reaction Type Ugi Solvent THF Limiting Reactant 1.704 M Precipitate Yes Product Awaiting Characterization Comments Reference http://usefulchem.wikispaces.com/Exp238

+

Boc-Gly-OH

+

butylamine

+

phenanthrene-9-carboxaldehyde



cyclohexylisocyanide

24528329

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCExp238-30 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.378 M Precipitate Yes but solvent evaporated Comments Reference http://usefulchem.wikispaces.com/Exp238

+

Boc-Gly-OH

+

cyclohexylamine

+

phenanthrene-9-carboxaldehyde



cyclohexylisocyanide

24528330

Reaction ID UCExp238-31 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.48 M Precipitate Yes but solvent evaporated Comments Reference http://usefulchem.wikispaces.com/Exp238

+

Boc-Gly-OH

+

furfurylamine

+

phenanthrene-9-carboxaldehyde



cyclohexylisocyanide

24528331

Reaction ID UCExp238-32 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.572 M Precipitate Yes Product Awaiting Characterization Comments Reference http://usefulchem.wikispaces.com/Exp238

+

Boc-Gly-OH

+

1-heptylamine

+

phenanthrene-9-carboxaldehyde

Reaction ID UCExp238-33 Researcher

Khalid Mirza

254



cyclohexylisocyanide

24528332

Reaction Type Ugi Solvent THF Limiting Reactant 1.616 M Precipitate Yes Product Awaiting Characterization Comments Reference http://usefulchem.wikispaces.com/Exp238

+

Boc-Gly-OH

+

1-hexylamine

+

phenanthrene-9-carboxaldehyde



cyclohexylisocyanide

24528333

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCExp238-34 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.648 M Precipitate Yes Product Awaiting Characterization Comments Reference http://usefulchem.wikispaces.com/Exp238

+

Boc-Gly-OH

+

methylamine

+

phenanthrene-9-carboxaldehyde



cyclohexylisocyanide

24528334

Reaction ID UCExp238-35 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.753 M Precipitate Yes Product Awaiting Characterization Comments Reference http://usefulchem.wikispaces.com/Exp238

+

Boc-Gly-OH

+

1-propylamine

+

phenanthrene-9-carboxaldehyde



cyclohexylisocyanide

24528335

Reaction ID UCExp238-36 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.686 M Precipitate Yes but solvent evaporated Comments Reference http://usefulchem.wikispaces.com/Exp238

+

Boc-Gly-OH

+

t-butylamine

+

phenanthrene-9-carboxaldehyde

Reaction ID UCExp238-37

255



cyclohexylisocyanide

24528336

Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.718 M Precipitate Yes but solvent evaporated Comments Reference http://usefulchem.wikispaces.com/Exp238

+

Boc-Gly-OH

+

2-chloroaniline

+

phenanthrene-9-carboxaldehyde



t-butyl isocyanide

24528337

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCExp238-38 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.716 M Precipitate Yes but solvent evaporated Comments Reference http://usefulchem.wikispaces.com/Exp238

+

Boc-Gly-OH

+

3-chloroaniline

+

phenanthrene-9-carboxaldehyde



t-butyl isocyanide

24528338

Reaction ID UCExp238-39 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.76 M Precipitate Yes Product Awaiting Characterization Comments Reference http://usefulchem.wikispaces.com/Exp238

+

+

Boc-Gly-OH

aniline

+

phenanthrene-9-carboxaldehyde



t-butyl isocyanide

24528339

Reaction ID UCExp238-40 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.706 M Precipitate Yes Product Awaiting Characterization Comments Reference http://usefulchem.wikispaces.com/Exp238

+

Boc-Gly-OH

+

benzylamine

+

phenanthrene-9-carboxaldehyde

Reaction ID UCExp238-41

256



t-butyl isocyanide

24528340

Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.737 M Precipitate Yes but solvent evaporated Comments Reference http://usefulchem.wikispaces.com/Exp238

+

Boc-Gly-OH

+

butylamine

+

phenanthrene-9-carboxaldehyde



t-butyl isocyanide

24528341

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCExp238-42 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.399 M Precipitate Yes but solvent evaporated Comments Reference http://usefulchem.wikispaces.com/Exp238

+

Boc-Gly-OH

+

cyclohexylamine

+

phenanthrene-9-carboxaldehyde



t-butyl isocyanide

24528342

Reaction ID UCExp238-43 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.505 M Precipitate Yes Product Awaiting Characterization Comments Reference http://usefulchem.wikispaces.com/Exp238

+

Boc-Gly-OH

+

furfurylamine

+

phenanthrene-9-carboxaldehyde



t-butyl isocyanide

24528343

Reaction ID UCExp238-44 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.6 M Precipitate Yes Product Awaiting Characterization Comments Reference http://usefulchem.wikispaces.com/Exp238

+

Boc-Gly-OH

+

1-heptylamine

+

phenanthrene-9-carboxaldehyde

257



t-butyl isocyanide

24528344

Boc-L-Serine Reaction ID UCEXP234-10 Researcher David Bulger Reaction Type Ugi Solvent methanol Limiting Reactant 0.916 M Precipitate Reactants insoluble Comments Reference http://usefulchem.wikispaces.com/Exp234

+

Boc-L-Serine

+

benzylamine

+

3,5-dimethoxybenzaldehyde



cyclohexylisocyanide

24528267

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCEXP234-9 Researcher David Bulger Reaction Type Ugi Solvent methanol Limiting Reactant 0.918 M Precipitate Reactants insoluble Comments Reference http://usefulchem.wikispaces.com/Exp234

+

Boc-L-Serine

+

benzylamine

+

3,5-dimethoxybenzaldehyde



t-butyl isocyanide

24528274

Boc-L-Threonine Reaction ID UCEXP234-11 Researcher David Bulger Reaction Type Ugi Solvent methanol Limiting Reactant 0.893 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp234

+

+

glycine methyl ester hydrochloride

Boc-L-Threonine

+

3,5-dimethoxybenzaldehyde



t-butyl isocyanide

24528268

Reaction ID UCEXP234-12 Researcher David Bulger Reaction Type Ugi Solvent methanol Limiting Reactant 0.891 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp234

+

+

+

258



glycine methyl ester hydrochloride

Boc-L-Threonine

3,5-dimethoxybenzaldehyde

cyclohexylisocyanide

24528269

Boc-Pro-OH Reaction ID UCEXP233-11

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Researcher David Bulger Reaction Type Ugi Solvent methanol Limiting Reactant 1.021 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp233

+

Boc-Pro-OH

+

benzylamine

+

3,5-dimethoxybenzaldehyde



t-butyl isocyanide

24528262

Reaction ID UCEXP233-12 Researcher David Bulger Reaction Type Ugi Solvent methanol Limiting Reactant 1.018 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp233

+

Boc-Pro-OH

+

benzylamine

+

3,5-dimethoxybenzaldehyde



cyclohexylisocyanide

24528263

Reaction ID UCEXP233-5 Researcher David Bulger Reaction Type Ugi Solvent methanol Limiting Reactant 0.919 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp233

+

Boc-Pro-OH

+

benzylamine

+

3,5-dimethoxybenzaldehyde

Reaction ID UCEXP233-6 Researcher David Bulger Reaction Type Ugi Solvent methanol Limiting Reactant 0.917 M Precipitate No

259



t-butyl isocyanide

24528262

Comments Reference

http://usefulchem.wikispaces.com/Exp233

+

+

Boc-Pro-OH

benzylamine

+

3,5-dimethoxybenzaldehyde



cyclohexylisocyanide

24528263

Boc-Trp-OH Reaction ID UCEXP131-1

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Researcher Rikesh Parikh Reaction Type Ugi Solvent methanol Limiting Reactant 0.608 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp131

+

+

Boc-Trp-OH

furfurylamine

+

veratraldehyde



n-butyl isocyanide

21106067

Reaction ID UCEXP131-2 Researcher Rikesh Parikh Reaction Type Ugi Solvent methanol Limiting Reactant 0.623 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp131

+

+

Boc-Trp-OH

furfurylamine

+

veratraldehyde



1-pentyl isocyanide

21106068

Reaction ID UCEXP131-3 Researcher Rikesh Parikh Reaction Type Ugi Solvent methanol Limiting Reactant 0.614 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp131

+

Boc-Trp-OH

+

5-methylfurfurylamine

+

veratraldehyde

Reaction ID UCEXP131-4 Researcher Rikesh Parikh Reaction Type Ugi Solvent methanol Limiting Reactant 0.612 M

260



1-pentyl isocyanide

21106069

Precipitate Comments Reference

No Protocol from Explan005 followed http://usefulchem.wikispaces.com/Exp131

+

Boc-Trp-OH

+

1-heptylamine

+

o-vanillin



benzyl isocyanide

21106061

Reaction ID UCEXP131-5

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Researcher Rikesh Parikh Reaction Type Ugi Solvent methanol Limiting Reactant 0.605 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp131

+

Boc-Trp-OH

+

1-octylamine

+

o-vanillin



benzyl isocyanide

21106062

Reaction ID UCEXP131-6 Researcher Rikesh Parikh Reaction Type Ugi Solvent methanol Limiting Reactant 0.625 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp131

+

Boc-Trp-OH

+

1-hexylamine

+

o-vanillin



n-butyl isocyanide

21106063

Reaction ID UCEXP131-7 Researcher Rikesh Parikh Reaction Type Ugi Solvent methanol Limiting Reactant 0.617 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp131

+

Boc-Trp-OH

+

1-hexylamine

+

o-vanillin

Reaction ID UCEXP131-8 Researcher Rikesh Parikh Reaction Type Ugi Solvent methanol Limiting Reactant 0.618 M Precipitate No Comments Protocol from Explan005 followed

261



1-pentyl isocyanide

21106064

Reference

http://usefulchem.wikispaces.com/Exp131

+

Boc-Trp-OH

+

1-heptylamine

+

o-vanillin



n-butyl isocyanide

21106065

Reaction ID UCEXP131-9 Researcher Rikesh Parikh Reaction Type Ugi Solvent methanol Limiting Reactant 0.61 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp131

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

+

Boc-Trp-OH

+

1-heptylamine

+

o-vanillin



1-pentyl isocyanide

21106066

Reaction ID UCEXP134-1 Researcher Rikesh Parikh Reaction Type Ugi Solvent methanol Limiting Reactant 0.645 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp134

+

Boc-Trp-OH

+

1-propylamine

+

o-vanillin



n-butyl isocyanide

21106070

Reaction ID UCEXP134-2 Researcher Rikesh Parikh Reaction Type Ugi Solvent methanol Limiting Reactant 0.636 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp134

+

Boc-Trp-OH

+

1-propylamine

+

o-vanillin

Reaction ID UCEXP134-3 Researcher Rikesh Parikh Reaction Type Ugi Solvent methanol Limiting Reactant 0.612 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp134

262



1-pentyl isocyanide

21106071

+

Boc-Trp-OH

+

+

1-octylamine

o-vanillin



n-butyl isocyanide

21106072

Reaction ID UCEXP134-4 Researcher Rikesh Parikh Reaction Type Ugi Solvent methanol Limiting Reactant 0.604 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp134

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

+

Boc-Trp-OH

+

+

1-octylamine

o-vanillin



1-pentyl isocyanide

21106073

Reaction ID UCEXP173E/V2B17 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.223 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp173

+

Boc-Trp-OH

+

methylamine

+

3,4-dihydroxybenzaldehyde



t-butyl isocyanide

21106045

Reaction ID UCEXP174E/V2B36 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.223 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp174

+

Boc-Trp-OH

+

methylamine

+

2-hydroxybenzaldehyde

Reaction ID UCEXP174N/V2B46 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.223 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp174

263



n-butyl isocyanide

21106201

+

Boc-Trp-OH

+

methylamine

+

3-hydroxybenzaldehyde



n-butyl isocyanide

21106193

Reaction ID UCEXP181-073V2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.222 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

+

Boc-Trp-OH

+

+

methylamine

benzaldehyde



t-butyl isocyanide

24528109

Reaction ID UCEXP228-1 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.253 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp228

+

Boc-Trp-OH

+

octadecylamine

+

4,7-dimethoxy-1-naphthaldehyde



tosylmethyl isocyanide

24528181

Reaction ID UCEXP228-2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.265 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp228

+

Boc-Trp-OH

+

octadecylamine

+

3-hydroxybenzaldehyde

Reaction ID UCEXP228-3 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.551 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp228

264



n-butyl isocyanide

24528182

+

Boc-Trp-OH

+

octadecylamine

+

2,4-dimethylbenzaldehyde



n-butyl isocyanide

24534188

Reaction ID UCEXP228-4 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.634 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp228

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

+

Boc-Trp-OH

+

+

octadecylamine

benzaldehyde



n-butyl isocyanide

24534192

Reaction ID UCEXP228-5 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.372 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp228

+

Boc-Trp-OH

+

5-methylfurfurylamine

+

4-(dimethylamino)benzaldehyde



tosylmethyl isocyanide

24534191

Reaction ID UCEXP228-6 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.627 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp228

+

Boc-Trp-OH

+

5-methylfurfurylamine

+

4-(trifluoromethyl)benzaldehyde

Reaction ID UCEXP229-1 Researcher David Bulger Reaction Type Ugi Solvent methanol Limiting Reactant 0.667 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp229

265



n-butyl isocyanide

24534190

+

Boc-Trp-OH

+

+

octadecylamine

4-methylbenzaldehyde



t-butyl isocyanide

24534189

Reaction ID UCEXP229-2 Researcher David Bulger Reaction Type Ugi Solvent methanol Limiting Reactant 0.667 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp229

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

+

Boc-Trp-OH

+

+

1-hexylamine

benzaldehyde



n-butyl isocyanide

24528183

butylamine Reaction ID UCExp236-04 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.844 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp236

+

methacrylic acid

+

butylamine

+

4-(trifluoromethyl)benzaldehyde



t-butyl isocyanide

24528278

Reaction ID UCExp236-16 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.872 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp236

+

formic acid

+

butylamine

+

4-(trifluoromethyl)benzaldehyde

Reaction ID UCExp238-05 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.903 M Precipitate No Comments -

266



t-butyl isocyanide

24528289

Reference

http://usefulchem.wikispaces.com/Exp238

+

crotonic acid

+

butylamine

+

phenanthrene-9-carboxaldehyde



cyclohexylisocyanide

24528307

Reaction ID UCExp238-17 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.945 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp238

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

+

crotonic acid

+

butylamine

+

phenanthrene-9-carboxaldehyde



t-butyl isocyanide

24528318

Reaction ID UCExp238-29 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.704 M Precipitate Yes Product Awaiting Characterization Comments Reference http://usefulchem.wikispaces.com/Exp238

+

Boc-Gly-OH

+

butylamine

+

phenanthrene-9-carboxaldehyde



cyclohexylisocyanide

24528329

Reaction ID UCExp238-41 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.737 M Precipitate Yes but solvent evaporated Comments Reference http://usefulchem.wikispaces.com/Exp238

+

Boc-Gly-OH

+

butylamine

+

phenanthrene-9-carboxaldehyde

Reaction ID UCExp241-30 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.717 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp241

267



t-butyl isocyanide

24528341

+

3,4methylenedioxyphenylacetic acid

+

+

5-bromo-2thiophenecarboxaldehyde

butylamine



t-butyl isocyanide

24528367

butyric acid Reaction ID UCEXP174Q/V2B50

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.222 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp174

+

butyric acid

+

3-chloroaniline

+

2-hydroxybenzaldehyde



tosylmethyl isocyanide

21106191

cbz-proline Reaction ID UCExp245-17 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.502 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp245

+

cbz-proline

+

furfurylamine

+

piperonal



n-butyl isocyanide

24528399

Reaction ID UCExp245-18 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.12 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp245

+

cbz-proline

+

furfurylamine

+

piperonal

Reaction ID UCExp245-19 Researcher

Khalid Mirza

268



n-butyl isocyanide

24528399

Reaction Type Ugi Solvent methanol Limiting Reactant 0.496 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp245

+

cbz-proline

+

5-methylfurfurylamine

+

piperonal



n-butyl isocyanide

24528400

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCExp245-20 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.092 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp245

+

cbz-proline

+

5-methylfurfurylamine

+

piperonal



n-butyl isocyanide

24528400

Reaction ID UCExp245-21 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.5 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp245

+

cbz-proline

+

furfurylamine

+

piperonal



t-butyl isocyanide

24528401

Reaction ID UCExp245-22 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.109 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp245

+

cbz-proline

+

furfurylamine

+

piperonal

Reaction ID UCExp245-23 Researcher Reaction Type Solvent

Khalid Mirza Ugi methanol

269



t-butyl isocyanide

24528401

Limiting Reactant 0.497 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp245

+

cbz-proline

+

furfurylamine

+

piperonal



cyclohexylisocyanide

24528402

Reaction ID UCExp245-24

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.096 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp245

+

cbz-proline

+

furfurylamine

+

piperonal



cyclohexylisocyanide

24528402

Reaction ID UCExp245-25 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.509 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp245

+

cbz-proline

+

furfurylamine

+



1,1,3,3tetramethylbutyl isocyanide

piperonal

24528403

Reaction ID UCExp245-26 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.038 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp245

+

cbz-proline

+

furfurylamine

+

piperonal

Reaction ID UCExp245-27 Researcher Reaction Type

Khalid Mirza Ugi

270



1,1,3,3tetramethylbutyl isocyanide

24528403

Solvent methanol Limiting Reactant 0.494 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp245

+

cbz-proline

+

5-methylfurfurylamine

+

piperonal



t-butyl isocyanide

24528404

Reaction ID UCExp245-28

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.082 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp245

+

cbz-proline

+

5-methylfurfurylamine

+

piperonal



t-butyl isocyanide

24528404

Reaction ID UCExp245-29 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.503 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp245

+

cbz-proline

+

5-methylfurfurylamine

+



1,1,3,3tetramethylbutyl isocyanide

piperonal

24528405

Reaction ID UCExp245-30 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.013 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp245

+

cbz-proline

+

5-methylfurfurylamine

+

piperonal

Reaction ID UCExp245-31 Researcher

Khalid Mirza

271



1,1,3,3tetramethylbutyl isocyanide

24528405

Reaction Type Ugi Solvent methanol Limiting Reactant 0.504 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp245

+

cbz-proline

+

+

5-methylfurfurylamine

piperonal



cyclohexylisocyanide

24528406

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCExp245-32 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.002 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp245

+

cbz-proline

+

+

5-methylfurfurylamine

piperonal



cyclohexylisocyanide

24528406

chloroacetic acid Reaction ID UCEXP215G Researcher Khalid Mirza Reaction Type Ugi Solvent THF + methanol Limiting Reactant 0.291 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp215

+

chloroacetic acid

+

+

5-bromo-2thiophenecarboxaldehyde

3-chloroaniline



benzyl isocyanide

24528156

crotonaldehyde Reaction ID UCEXP232-16 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.366 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

+

+

+

272



Boc-Gly-OH

furfurylamine

crotonaldehyde

t-butyl isocyanide

24528202

Reaction ID UCEXP232-17 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.365 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

+

Boc-Gly-OH

+

furfurylamine

+

crotonaldehyde



n-butyl isocyanide

24528203

Reaction ID UCEXP232-18 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.367 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+

crotonaldehyde



1-pentyl isocyanide

24528204

Reaction ID UCEXP232-19 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.366 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+

crotonaldehyde

Reaction ID UCEXP232-20 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.366 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

273



cyclohexylisocyanide

24528205

+

Boc-Gly-OH

+

+

furfurylamine



1,1,3,3tetramethylbutyl isocyanide

crotonaldehyde

24528206

crotonic acid

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCEXP148A-V1B153 Researcher Khalid Mirza/ Emily Messner Reaction Type Ugi Solvent methanol Limiting Reactant 0.398 M Precipitate Yes but the aldehyde alone is not soluble in methanol Yield 50.1 % Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp148

+

crotonic acid

+

1-heptylamine

+

phenanthrene-9-carboxaldehyde



t-butyl isocyanide

21106058

Reaction ID UCEXP150D-V1B155 Researcher Khalid Mirza/ Emily Messner Reaction Type Ugi Solvent methanol Limiting Reactant 0.404 M Precipitate Yes but the aldehyde alone is not soluble in methanol Yield 59 % Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp150

+

crotonic acid

+

benzylamine

+

phenanthrene-9-carboxaldehyde



t-butyl isocyanide

21105601

Reaction ID UCEXP156B-V1B155 Researcher Emily Messner Reaction Type Ugi Solvent methanol Limiting Reactant 0.678 M Precipitate Yes but reactants initially insoluble Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp156

+

crotonic acid

+

benzylamine

+

phenanthrene-9-carboxaldehyde

Reaction ID UCEXP214C Researcher Reaction Type

Khalid Mirza Ugi

274



t-butyl isocyanide

21106075

Solvent methanol Limiting Reactant 0.404 M Precipitate Yes but the aldehyde alone is not soluble in methanol Yield - % Comments Reference http://usefulchem.wikispaces.com/Exp214

+

+

crotonic acid

benzylamine

+

phenanthrene-9-carboxaldehyde



t-butyl isocyanide

21105601

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCEXP215A Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 0.661 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp215

+

crotonic acid

+

1-heptylamine

+

phenanthrene-9-carboxaldehyde



t-butyl isocyanide

21106058

Reaction ID UCEXP215B Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 0.678 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp215

+

crotonic acid

+

benzylamine

+

phenanthrene-9-carboxaldehyde



t-butyl isocyanide

21105601

Reaction ID UCEXP217-2 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 0.383 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp217

+

crotonic acid

+

benzylamine

+

phenanthrene-9-carboxaldehyde

Reaction ID UCEXP231-2 Researcher

Khalid Mirza

275



t-butyl isocyanide

21105601

Reaction Type Ugi Solvent THF Limiting Reactant 1 M Precipitate aldehyde insoluble at this concentration Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp231

+

crotonic acid

+

benzylamine

+

phenanthrene-9-carboxaldehyde



t-butyl isocyanide

21105601

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCExp238-01 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.881 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp238

+

crotonic acid

+

2-chloroaniline

+

phenanthrene-9-carboxaldehyde



cyclohexylisocyanide

24528303

Reaction ID UCExp238-02 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.879 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp238

+

crotonic acid

+

3-chloroaniline

+

phenanthrene-9-carboxaldehyde



cyclohexylisocyanide

24528304

Reaction ID UCExp238-03 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.931 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp238

+

crotonic acid

+

aniline

+

phenanthrene-9-carboxaldehyde

Reaction ID UCExp238-04 Researcher Reaction Type Solvent

Khalid Mirza Ugi THF

276



cyclohexylisocyanide

24528305

Limiting Reactant 1.866 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp238

+

crotonic acid

+

benzylamine

+

phenanthrene-9-carboxaldehyde



cyclohexylisocyanide

24528306

Reaction ID UCExp238-05

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.903 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp238

+

crotonic acid

+

butylamine

+

phenanthrene-9-carboxaldehyde



cyclohexylisocyanide

24528307

Reaction ID UCExp238-06 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.849 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp238

+

crotonic acid

+

cyclohexylamine

+

phenanthrene-9-carboxaldehyde



cyclohexylisocyanide

24528308

Reaction ID UCExp238-07 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.628 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp238

+

crotonic acid

+

furfurylamine

+

phenanthrene-9-carboxaldehyde

Reaction ID UCExp238-08 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.74 M Precipitate No

277



cyclohexylisocyanide

24528309

Comments Reference

http://usefulchem.wikispaces.com/Exp238

+

crotonic acid

+

1-heptylamine

+

phenanthrene-9-carboxaldehyde



cyclohexylisocyanide

24528310

Reaction ID UCExp238-09

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.794 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp238

+

crotonic acid

+

1-hexylamine

+

phenanthrene-9-carboxaldehyde



cyclohexylisocyanide

24528311

Reaction ID UCExp238-10 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.825 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp238

+

crotonic acid

+

methylamine

+

phenanthrene-9-carboxaldehyde



cyclohexylisocyanide

24528312

Reaction ID UCExp238-11 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.965 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp238

+

crotonic acid

+

1-propylamine

+

phenanthrene-9-carboxaldehyde

Reaction ID UCExp238-12 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.881 M Precipitate Yes but solvent evaporated Comments Reference http://usefulchem.wikispaces.com/Exp238

278



cyclohexylisocyanide

24528313

+

crotonic acid

+

t-butylamine

+

phenanthrene-9-carboxaldehyde



cyclohexylisocyanide

24528314

Reaction ID UCExp238-13 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.921 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp238

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

+

crotonic acid

+

2-chloroaniline

+

phenanthrene-9-carboxaldehyde



t-butyl isocyanide

24528315

Reaction ID UCExp238-14 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.919 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp238

+

crotonic acid

+

3-chloroaniline

+

phenanthrene-9-carboxaldehyde



t-butyl isocyanide

24528316

Reaction ID UCExp238-15 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.974 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp238

+

crotonic acid

+

aniline

+

phenanthrene-9-carboxaldehyde

Reaction ID UCExp238-16 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.906 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp238

279



t-butyl isocyanide

24528317

+

crotonic acid

+

benzylamine

+

phenanthrene-9-carboxaldehyde



t-butyl isocyanide

21105601

Reaction ID UCExp238-17 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.945 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp238

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

+

crotonic acid

+

butylamine

+

phenanthrene-9-carboxaldehyde



t-butyl isocyanide

24528318

Reaction ID UCExp238-18 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.888 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp238

+

crotonic acid

+

cyclohexylamine

+

phenanthrene-9-carboxaldehyde



t-butyl isocyanide

24528319

Reaction ID UCExp238-19 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.658 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp238

+

crotonic acid

+

furfurylamine

+

phenanthrene-9-carboxaldehyde

Reaction ID UCExp238-20 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.775 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp238

280



t-butyl isocyanide

24528320

+

crotonic acid

+

1-heptylamine

+

phenanthrene-9-carboxaldehyde



t-butyl isocyanide

21106058

Reaction ID UCExp238-21 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.831 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp238

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

+

crotonic acid

+

1-hexylamine

+

phenanthrene-9-carboxaldehyde



t-butyl isocyanide

24528321

Reaction ID UCExp238-22 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.867 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp238

+

crotonic acid

+

methylamine

+

phenanthrene-9-carboxaldehyde



t-butyl isocyanide

24528322

Reaction ID UCExp238-23 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 2.009 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp238

+

crotonic acid

+

1-propylamine

+

phenanthrene-9-carboxaldehyde

Reaction ID UCExp238-24 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.921 M Precipitate Yes but solvent evaporated Comments Reference http://usefulchem.wikispaces.com/Exp238

281



t-butyl isocyanide

24528323

+

crotonic acid

+

t-butylamine

+

phenanthrene-9-carboxaldehyde



t-butyl isocyanide

24528324

cyclohexancarboxaldehyde Reaction ID UCEXP232-26

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.092 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+

cyclohexancarboxaldehyde



t-butyl isocyanide

24528212

Reaction ID UCEXP232-27 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.092 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+

cyclohexancarboxaldehyde



n-butyl isocyanide

24528213

Reaction ID UCEXP232-28 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.093 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+

cyclohexancarboxaldehyde

Reaction ID UCEXP232-29 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.092 M Precipitate No Comments -

282



1-pentyl isocyanide

24528214

Reference

http://usefulchem.wikispaces.com/Exp232

+

+

Boc-Gly-OH

furfurylamine

+

cyclohexancarboxaldehyde



cyclohexylisocyanide

24528215

Reaction ID UCEXP232-30 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.092 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

+

+

Boc-Gly-OH

furfurylamine

+



1,1,3,3tetramethylbutyl isocyanide

cyclohexancarboxaldehyde

24528216

cyclohexylamine Reaction ID UCEXP162 Researcher Shannon Oseback Reaction Type Ugi Solvent methanol Limiting Reactant 0.285 M Precipitate Reactants Insoluble Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp162

+

phenylacetic acid

+

cyclohexylamine

+

phenanthrene-9-carboxaldehyde



t-butyl isocyanide

21105590

Reaction ID UCEXP183-049V1 Researcher Emily Messner Reaction Type Ugi Solvent methanol Limiting Reactant 0.398 M Precipitate Reactants Insoluble Comments Reference http://usefulchem.wikispaces.com/Exp183

+

mandelic acid

+

cyclohexylamine

+

phenanthrene-9-carboxaldehyde

Reaction ID UCEXP184-1/49 Researcher Reaction Type Solvent

Emily Messner Ugi ethanol

283



t-butyl isocyanide

24528153

Limiting Reactant 0.398 M Precipitate Reactants insoluble Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp184

+

mandelic acid

+

cyclohexylamine

+

phenanthrene-9-carboxaldehyde



t-butyl isocyanide

24528154

Reaction ID UCEXP184-2/49

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Researcher Emily Messner Reaction Type Ugi Solvent acetonitrile Limiting Reactant 0.398 M Precipitate Reactants insoluble Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp184

+

mandelic acid

+

cyclohexylamine

+

phenanthrene-9-carboxaldehyde



t-butyl isocyanide

24528154

Reaction ID UCEXP184-3/49 Researcher Emily Messner Reaction Type Ugi Solvent dichloromethane Limiting Reactant 0.398 M Precipitate Reactants insoluble Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp184

+

mandelic acid

+

cyclohexylamine

+

phenanthrene-9-carboxaldehyde



t-butyl isocyanide

24528154

Reaction ID UCExp236-29 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.614 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp236

+

3,3'-dichloropivalic acid

+

cyclohexylamine

+

4-(trifluoromethyl)benzaldehyde

Reaction ID UCExp238-06 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.849 M Precipitate No

284



t-butyl isocyanide

24528302

Comments Reference

http://usefulchem.wikispaces.com/Exp238

+

crotonic acid

+

cyclohexylamine

+

phenanthrene-9-carboxaldehyde



cyclohexylisocyanide

24528308

Reaction ID UCExp238-18

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.888 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp238

+

crotonic acid

+

cyclohexylamine

+

phenanthrene-9-carboxaldehyde



t-butyl isocyanide

24528319

Reaction ID UCExp238-30 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.378 M Precipitate Yes but solvent evaporated Comments Reference http://usefulchem.wikispaces.com/Exp238

+

Boc-Gly-OH

+

cyclohexylamine

+

phenanthrene-9-carboxaldehyde



cyclohexylisocyanide

24528330

Reaction ID UCExp238-42 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.399 M Precipitate Yes but solvent evaporated Comments Reference http://usefulchem.wikispaces.com/Exp238

+

Boc-Gly-OH

+

cyclohexylamine

+

phenanthrene-9-carboxaldehyde

Reaction ID UCExp241-37 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.733 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp241

285



t-butyl isocyanide

24528342

+

+

3,4methylenedioxyphenylacetic acid

cyclohexylamine

+

4-(trifluoromethyl)benzaldehyde



t-butyl isocyanide

24528373

cyclohexylisocyanide

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCEXP225-4 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.889 M Precipitate Yes Product Pending Comments 0.5 mmol of isocyanide was added to 500uL of a 2M solution of aldehyde; amine and acid Reference http://usefulchem.wikispaces.com/Exp225

+

+

Boc-Gly-OH

furfurylamine

+

piperonal



cyclohexylisocyanide

24528160

Reaction ID UCEXP226-4 Researcher David Bulger Reaction Type Ugi Solvent THF Limiting Reactant 0.52 M Precipitate No Comments 0.5 mmol of isocyanide was added to 900uL of a 0.55M solution of aldehyde; amine and acid Reference http://usefulchem.wikispaces.com/Exp226

+

1-pyrenebutyric acid

+

5-methylfurfurylamine

+

benzaldehyde



cyclohexylisocyanide

24528168

Reaction ID UCEXP227-4 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 0.445 M Precipitate No Comments 0.5 mmol of isocyanide was added to 500uL of a 0.5M solution of aldehyde; amine and acid Reference http://usefulchem.wikispaces.com/Exp227

+

1-pyrenebutyric acid

+

furfurylamine

+

piperonal

Reaction ID UCEXP232-04 Researcher Reaction Type Solvent

Khalid Mirza Ugi methanol

286



cyclohexylisocyanide

24528176

Limiting Reactant 1.098 M Precipitate Yes Product Pending Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

+

furfurylamine

benzaldehyde



cyclohexylisocyanide

24528191

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCEXP232-09 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.083 M Precipitate Yes Product Pending Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

+

furfurylamine

4-methylbenzaldehyde



cyclohexylisocyanide

24528196

Reaction ID UCEXP232-14 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.028 M Precipitate Yes Product Pending Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+

4-(trifluoromethyl)benzaldehyde



cyclohexylisocyanide

21782441

Reaction ID UCEXP232-19 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.366 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+

crotonaldehyde

Reaction ID UCEXP232-24 Researcher Reaction Type

Khalid Mirza Ugi

287



cyclohexylisocyanide

24528205

Solvent methanol Limiting Reactant 1.008 M Precipitate Yes Product Pending Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

+

furfurylamine

diphenylacetaldehyde



cyclohexylisocyanide

24528210

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCEXP232-29 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.092 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+

cyclohexancarboxaldehyde



cyclohexylisocyanide

24528215

Reaction ID UCEXP232-34 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.11 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

+

furfurylamine

2-furaldehyde



cyclohexylisocyanide

24528220

Reaction ID UCEXP232-39 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.081 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+

2-hydroxybenzaldehyde

Reaction ID UCEXP232-44 Researcher Reaction Type Solvent

Khalid Mirza Ugi methanol

288



cyclohexylisocyanide

24528225

Limiting Reactant 1.083 M Precipitate Yes Product Pending Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

+

furfurylamine

o-tolualdehyde



cyclohexylisocyanide

24528230

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCEXP232-49 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.066 M Precipitate Yes Product Pending Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+

4-methoxybenzaldehyde



cyclohexylisocyanide

24528235

Reaction ID UCEXP232-54 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.106 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+

hexanaldehyde



cyclohexylisocyanide

24528240

Reaction ID UCEXP232-59 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.109 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+

trans-2-hexenal

Reaction ID UCEXP232-64 Researcher Reaction Type Solvent

Khalid Mirza Ugi methanol

289



cyclohexylisocyanide

24528244

Limiting Reactant 1.069 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+

2-phenylpropionaldehyde



cyclohexylisocyanide

24534419

Reaction ID UCEXP232-69

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.067 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

+

furfurylamine

m-anisaldehyde



cyclohexylisocyanide

24528254

Reaction ID UCEXP232-74 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.105 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

+

furfurylamine

2-ethylbutyraldehyde



cyclohexylisocyanide

24528259

Reaction ID UCEXP233-10 Researcher David Bulger Reaction Type Ugi Solvent methanol Limiting Reactant 1.018 M Precipitate Yes Product Pending Comments Reference http://usefulchem.wikispaces.com/Exp233

+

phenylpropynoic acid

+

benzylamine

+

3,5-dimethoxybenzaldehyde

Reaction ID UCEXP233-12 Researcher David Bulger Reaction Type Ugi Solvent methanol Limiting Reactant 1.018 M

290



cyclohexylisocyanide

23078615

Precipitate Comments Reference

No http://usefulchem.wikispaces.com/Exp233

+

Boc-Pro-OH

+

benzylamine

+

3,5-dimethoxybenzaldehyde



cyclohexylisocyanide

24528263

Reaction ID UCEXP233-2

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Researcher David Bulger Reaction Type Ugi Solvent methanol Limiting Reactant 0.92 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp233

+

1-aminocyclohexane-1carboxylic acid

+

benzylamine

+

3,5-dimethoxybenzaldehyde



cyclohexylisocyanide

24534440

Reaction ID UCEXP233-4 Researcher David Bulger Reaction Type Ugi Solvent methanol Limiting Reactant 0.917 M Precipitate Yes Product Pending Comments Reference http://usefulchem.wikispaces.com/Exp233

+

phenylpropynoic acid

+

benzylamine

+

3,5-dimethoxybenzaldehyde



cyclohexylisocyanide

23078615

Reaction ID UCEXP233-6 Researcher David Bulger Reaction Type Ugi Solvent methanol Limiting Reactant 0.917 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp233

+

Boc-Pro-OH

+

benzylamine

+

3,5-dimethoxybenzaldehyde

Reaction ID UCEXP233-8 Researcher David Bulger Reaction Type Ugi Solvent methanol Limiting Reactant 1.018 M

291



cyclohexylisocyanide

24528263

Precipitate Comments Reference

No http://usefulchem.wikispaces.com/Exp233

+

+

1-aminocyclohexane-1carboxylic acid

benzylamine

+

3,5-dimethoxybenzaldehyde



cyclohexylisocyanide

24534440

Reaction ID UCEXP234-10

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Researcher David Bulger Reaction Type Ugi Solvent methanol Limiting Reactant 0.916 M Precipitate Reactants insoluble Comments Reference http://usefulchem.wikispaces.com/Exp234

+

+

Boc-L-Serine

benzylamine

+

3,5-dimethoxybenzaldehyde



cyclohexylisocyanide

24528267

Reaction ID UCEXP234-12 Researcher David Bulger Reaction Type Ugi Solvent methanol Limiting Reactant 0.891 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp234

+

+

glycine methyl ester hydrochloride

Boc-L-Threonine

+

3,5-dimethoxybenzaldehyde



cyclohexylisocyanide

24528269

Reaction ID UCEXP234-2 Researcher David Bulger Reaction Type Ugi Solvent methanol Limiting Reactant 1.002 M Precipitate Yes Product Pending Comments Reference http://usefulchem.wikispaces.com/Exp234

+

phenylpropynoic acid

+

benzylamine

+

3,5Bis(trifluoromethyl)benzaldehyde

Reaction ID UCEXP234-4 Researcher Reaction Type

David Bulger Ugi

292



cyclohexylisocyanide

23078614

Solvent methanol Limiting Reactant 1.002 M Precipitate Yes Product Pending Comments Reference http://usefulchem.wikispaces.com/Exp234

+

+

phenylpropynoic acid

+

3,5Bis(trifluoromethyl)benzaldehyde

benzylamine



cyclohexylisocyanide

23078614

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCEXP234-6 Researcher David Bulger Reaction Type Ugi Solvent methanol Limiting Reactant 0.916 M Precipitate Reactants insoluble Comments Reference http://usefulchem.wikispaces.com/Exp234

+

+

Fmoc-Diglycine

benzylamine

+

3,5-dimethoxybenzaldehyde



cyclohexylisocyanide

24528271

Reaction ID UCEXP234-8 Researcher David Bulger Reaction Type Ugi Solvent methanol Limiting Reactant 0.916 M Precipitate Reactants insoluble Comments Reference http://usefulchem.wikispaces.com/Exp234

+

+

Boc-diglycine

benzylamine

+

3,5-dimethoxybenzaldehyde



cyclohexylisocyanide

24528273

Reaction ID UCExp235-2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1 M Precipitate Yes Product No Comments Reference http://usefulchem.wikispaces.com/Exp235

+

Boc-Gly-OH

+

furfurylamine

+

4-(trifluoromethyl)benzaldehyde

Reaction ID UCExp238-01 Researcher

Khalid Mirza

293



cyclohexylisocyanide

21782441

Reaction Type Ugi Solvent THF Limiting Reactant 1.881 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp238

+

crotonic acid

+

2-chloroaniline

+

phenanthrene-9-carboxaldehyde



cyclohexylisocyanide

24528303

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCExp238-02 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.879 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp238

+

crotonic acid

+

3-chloroaniline

+

phenanthrene-9-carboxaldehyde



cyclohexylisocyanide

24528304

Reaction ID UCExp238-03 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.931 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp238

+

+

crotonic acid

aniline

+

phenanthrene-9-carboxaldehyde



cyclohexylisocyanide

24528305

Reaction ID UCExp238-04 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.866 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp238

+

crotonic acid

+

benzylamine

+

phenanthrene-9-carboxaldehyde

Reaction ID UCExp238-05 Researcher Reaction Type Solvent

Khalid Mirza Ugi THF

294



cyclohexylisocyanide

24528306

Limiting Reactant 1.903 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp238

+

crotonic acid

+

butylamine

+

phenanthrene-9-carboxaldehyde



cyclohexylisocyanide

24528307

Reaction ID UCExp238-06

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.849 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp238

+

crotonic acid

+

cyclohexylamine

+

phenanthrene-9-carboxaldehyde



cyclohexylisocyanide

24528308

Reaction ID UCExp238-07 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.628 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp238

+

crotonic acid

+

furfurylamine

+

phenanthrene-9-carboxaldehyde



cyclohexylisocyanide

24528309

Reaction ID UCExp238-08 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.74 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp238

+

crotonic acid

+

1-heptylamine

+

phenanthrene-9-carboxaldehyde

Reaction ID UCExp238-09 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.794 M Precipitate No

295



cyclohexylisocyanide

24528310

Comments Reference

http://usefulchem.wikispaces.com/Exp238

+

crotonic acid

+

1-hexylamine

+

phenanthrene-9-carboxaldehyde



cyclohexylisocyanide

24528311

Reaction ID UCExp238-10

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.825 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp238

+

crotonic acid

+

methylamine

+

phenanthrene-9-carboxaldehyde



cyclohexylisocyanide

24528312

Reaction ID UCExp238-11 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.965 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp238

+

crotonic acid

+

1-propylamine

+

phenanthrene-9-carboxaldehyde



cyclohexylisocyanide

24528313

Reaction ID UCExp238-12 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.881 M Precipitate Yes but solvent evaporated Comments Reference http://usefulchem.wikispaces.com/Exp238

+

crotonic acid

+

t-butylamine

+

phenanthrene-9-carboxaldehyde

Reaction ID UCExp238-25 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.686 M Precipitate Yes Product Awaiting Characterization Comments -

296



cyclohexylisocyanide

24528314

Reference

http://usefulchem.wikispaces.com/Exp238

+

Boc-Gly-OH

+

2-chloroaniline

+

phenanthrene-9-carboxaldehyde



cyclohexylisocyanide

24528325

Reaction ID UCExp238-26 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.684 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp238

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

+

Boc-Gly-OH

+

3-chloroaniline

+

phenanthrene-9-carboxaldehyde



cyclohexylisocyanide

24528326

Reaction ID UCExp238-27 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.726 M Precipitate Yes Product Awaiting Characterization Comments Reference http://usefulchem.wikispaces.com/Exp238

+

+

Boc-Gly-OH

aniline

+

phenanthrene-9-carboxaldehyde



cyclohexylisocyanide

24528327

Reaction ID UCExp238-28 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.674 M Precipitate Yes Product Awaiting Characterization Comments Reference http://usefulchem.wikispaces.com/Exp238

+

Boc-Gly-OH

+

benzylamine

+

phenanthrene-9-carboxaldehyde

Reaction ID UCExp238-29 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.704 M Precipitate Yes Product Awaiting Characterization

297



cyclohexylisocyanide

24528328

Comments Reference

http://usefulchem.wikispaces.com/Exp238

+

Boc-Gly-OH

+

butylamine

+

phenanthrene-9-carboxaldehyde



cyclohexylisocyanide

24528329

Reaction ID UCExp238-30

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.378 M Precipitate Yes but solvent evaporated Comments Reference http://usefulchem.wikispaces.com/Exp238

+

Boc-Gly-OH

+

cyclohexylamine

+

phenanthrene-9-carboxaldehyde



cyclohexylisocyanide

24528330

Reaction ID UCExp238-31 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.48 M Precipitate Yes but solvent evaporated Comments Reference http://usefulchem.wikispaces.com/Exp238

+

Boc-Gly-OH

+

furfurylamine

+

phenanthrene-9-carboxaldehyde



cyclohexylisocyanide

24528331

Reaction ID UCExp238-32 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.572 M Precipitate Yes Product Awaiting Characterization Comments Reference http://usefulchem.wikispaces.com/Exp238

+

Boc-Gly-OH

+

1-heptylamine

+

phenanthrene-9-carboxaldehyde

Reaction ID UCExp238-33 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.616 M Precipitate Yes Product Awaiting Characterization

298



cyclohexylisocyanide

24528332

Comments Reference

http://usefulchem.wikispaces.com/Exp238

+

Boc-Gly-OH

+

1-hexylamine

+

phenanthrene-9-carboxaldehyde



cyclohexylisocyanide

24528333

Reaction ID UCExp238-34

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.648 M Precipitate Yes Product Awaiting Characterization Comments Reference http://usefulchem.wikispaces.com/Exp238

+

Boc-Gly-OH

+

methylamine

+

phenanthrene-9-carboxaldehyde



cyclohexylisocyanide

24528334

Reaction ID UCExp238-35 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.753 M Precipitate Yes Product Awaiting Characterization Comments Reference http://usefulchem.wikispaces.com/Exp238

+

Boc-Gly-OH

+

1-propylamine

+

phenanthrene-9-carboxaldehyde



cyclohexylisocyanide

24528335

Reaction ID UCExp238-36 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.686 M Precipitate Yes but solvent evaporated Comments Reference http://usefulchem.wikispaces.com/Exp238

+

Boc-Gly-OH

+

t-butylamine

+

phenanthrene-9-carboxaldehyde

Reaction ID UCExp240-03 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.562 M Precipitate No

299



cyclohexylisocyanide

24528336

Comments Reference

http://usefulchem.wikispaces.com/Exp240

+

phenylacetic acid

+

furfurylamine

+

phenanthrene-9-carboxaldehyde



cyclohexylisocyanide

24528345

Reaction ID UCExp240-09

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.78 M Precipitate Yes Yield - % Comments Reference http://usefulchem.wikispaces.com/Exp240

+

phenylacetic acid

+

5-methylfurfurylamine

+

phenanthrene-9-carboxaldehyde



cyclohexylisocyanide

21782450

Reaction ID UCExp241-08 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.52 M Precipitate YES Yield - % Comments Reference http://usefulchem.wikispaces.com/Exp241

+

3,4methylenedioxyphenylacetic acid

+

methylamine

+

veratraldehyde



cyclohexylisocyanide

21782465

Reaction ID UCExp241-09 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.564 M Precipitate YES Yield - % Comments Reference http://usefulchem.wikispaces.com/Exp241

+

3,4methylenedioxyphenylacetic acid

+

methylamine

+

veratraldehyde

Reaction ID UCExp242-3 Researcher

Marshall Moritz

300



cyclohexylisocyanide

21782465

Reaction Type Ugi Solvent benzene Limiting Reactant 0.432 M Precipitate Yes Product No Comments Reference http://usefulchem.wikispaces.com/Exp242

+

phenylacetic acid

+

furfurylamine

+

phenanthrene-9-carboxaldehyde



cyclohexylisocyanide

24528384

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCExp242-8 Researcher Marshall Moritz Reaction Type Ugi Solvent benzene Limiting Reactant 0.424 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp242

+

phenylacetic acid

+

5-methylfurfurylamine

+

phenanthrene-9-carboxaldehyde



cyclohexylisocyanide

24528389

Reaction ID UCExp245-07 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.504 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp245

+

3,4methylenedioxyphenylacetic acid

+

furfurylamine

+

piperonal



cyclohexylisocyanide

24528394

Reaction ID UCExp245-08 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.708 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp245

+

3,4methylenedioxyphenylacetic acid

+

furfurylamine

+

piperonal

301



cyclohexylisocyanide

24528394

Reaction ID UCExp245-13 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.499 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp245

+

3,4methylenedioxyphenylacetic acid

+

5-methylfurfurylamine

+

piperonal



cyclohexylisocyanide

24528397

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCExp245-14 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.696 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp245

+

3,4methylenedioxyphenylacetic acid

+

5-methylfurfurylamine

+

piperonal



cyclohexylisocyanide

24528397

Reaction ID UCExp245-23 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.497 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp245

+

cbz-proline

+

furfurylamine

+

piperonal



cyclohexylisocyanide

24528402

Reaction ID UCExp245-24 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.096 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp245

+

cbz-proline

+

furfurylamine

+

piperonal

302



cyclohexylisocyanide

24528402

Reaction ID UCExp245-31 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.504 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp245

+

cbz-proline

+

+

5-methylfurfurylamine

piperonal



cyclohexylisocyanide

24528406

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCExp245-32 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.002 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp245

+

cbz-proline

+

+

5-methylfurfurylamine

piperonal



cyclohexylisocyanide

24528406

D-(−)-Quinic acid Reaction ID UCEXP174O/V2B47 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.223 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp174

+

D-(−)-Quinic acid

+

5-methylfurfurylamine

+

3,5-dimethoxybenzaldehyde



t-butyl isocyanide

21106186

Reaction ID UCEXP181-065V2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.223 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

+

+

+

303



D-(−)-Quinic acid

benzylamine

3,5-dimethoxybenzaldehyde

t-butyl isocyanide

24528104

Reaction ID UCEXP181-100V2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.225 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

+

D-(−)-Quinic acid

+

+

methylamine

4-chlorobenzaldehyde



tosylmethyl isocyanide

24528131

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCEXP181-104V2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.223 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

+

D-(−)-Quinic acid

+

methylamine

+

4-(dimethylamino)benzaldehyde



tosylmethyl isocyanide

24528134

Reaction ID UCEXP181-108V2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.223 M Precipitate Yes Product No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

+

D-(−)-Quinic acid

+

methylamine

+

2-naphthaldehyde



tosylmethyl isocyanide

24528138

decanoic acid Reaction ID UCEXP173N/V2B26 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.217 M Precipitate Reactants Insoluble Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp173

+

+

+

304



decanoic acid

2-chloroaniline

o-vanillin

tosylmethyl isocyanide

21105847

Reaction ID UCEXP181-092V2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.217 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

+

decanoic acid

+

2-chloroaniline

+

3-methoxybenzaldehyde



tosylmethyl isocyanide

24528124

diphenylacetaldehyde Reaction ID UCEXP232-21 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.008 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+

diphenylacetaldehyde



t-butyl isocyanide

24528207

Reaction ID UCEXP232-22 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.007 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+

diphenylacetaldehyde

Reaction ID UCEXP232-23 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.008 M Precipitate No Comments -

305



n-butyl isocyanide

24528208

Reference

http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

+

furfurylamine

diphenylacetaldehyde



1-pentyl isocyanide

24528209

Reaction ID UCEXP232-24

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.008 M Precipitate Yes Product Pending Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

+

furfurylamine

diphenylacetaldehyde



cyclohexylisocyanide

24528210

Reaction ID UCEXP232-25 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.008 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

+

furfurylamine



1,1,3,3tetramethylbutyl isocyanide

diphenylacetaldehyde

24528211

diphenylacetic acid Reaction ID UCEXP181-076V2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.224 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

+

diphenylacetic acid

+

1-propylamine

+

3,4-dihydroxybenzaldehyde

Reaction ID UCEXP181-088V2 Researcher Reaction Type

Khalid Mirza Ugi

306



n-butyl isocyanide

24528112

Solvent methanol Limiting Reactant 0.222 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

+

diphenylacetic acid

+

5-methylfurfurylamine

+

3,4-dihydroxybenzaldehyde



n-butyl isocyanide

24528532

Reaction ID UCEXP181-119V2

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.226 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

+

diphenylacetic acid

+

methylamine

+

3,4-dihydroxybenzaldehyde



n-butyl isocyanide

24528148

Fmoc-Diglycine Reaction ID UCEXP234-5 Researcher David Bulger Reaction Type Ugi Solvent methanol Limiting Reactant 0.918 M Precipitate Reactants insoluble Comments Reference http://usefulchem.wikispaces.com/Exp234

+

Fmoc-Diglycine

+

benzylamine

+

3,5-dimethoxybenzaldehyde



t-butyl isocyanide

24528270

Reaction ID UCEXP234-6 Researcher David Bulger Reaction Type Ugi Solvent methanol Limiting Reactant 0.916 M Precipitate Reactants insoluble Comments Reference http://usefulchem.wikispaces.com/Exp234

+

Fmoc-Diglycine

+

benzylamine

+

3,5-dimethoxybenzaldehyde

307



cyclohexylisocyanide

24528271

formic acid Reaction ID UCEXP130-1 Researcher Rikesh Parikh Reaction Type Ugi Solvent methanol Limiting Reactant 0.751 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp130

+

formic acid

+

5-methylfurfurylamine

+

2-naphthaldehyde



n-butyl isocyanide

21106081

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCEXP130-2 Researcher Rikesh Parikh Reaction Type Ugi Solvent methanol Limiting Reactant 0.728 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp130

+

formic acid

+

1-hexylamine

+

2-naphthaldehyde



1-pentyl isocyanide

21106078

Reaction ID UCEXP130-3 Researcher Rikesh Parikh Reaction Type Ugi Solvent methanol Limiting Reactant 0.429 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp130

+

formic acid

+

5-methylfurfurylamine

+

benzaldehyde



tosylmethyl isocyanide

21106060

Reaction ID UCEXP130-4 Researcher Rikesh Parikh Reaction Type Ugi Solvent methanol Limiting Reactant 0.725 M Precipitate Yes Product Not Determined Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp130

+

formic acid

+

furfurylamine

+

2-naphthaldehyde

308



benzyl isocyanide

21106080

Reaction ID UCEXP130-5 Researcher Rikesh Parikh Reaction Type Ugi Solvent methanol Limiting Reactant 0.734 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp130

+

formic acid

+

+

furfurylamine

2-naphthaldehyde



n-butyl isocyanide

21106079

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCEXP231-1 Researcher Khalid Mirza Reaction Type Ugi Solvent acetonitrile Limiting Reactant 1.538 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp231

+

formic acid

+

+

benzylamine

4-methylbenzaldehyde



tosylmethyl isocyanide

24528186

Reaction ID UCExp236-05 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.65 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp236

+

formic acid

+

t-butylamine

+

4-(trifluoromethyl)benzaldehyde



t-butyl isocyanide

24528279

Reaction ID UCExp236-08 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.65 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp236

+

formic acid

+

3-chloroaniline

+

4-(trifluoromethyl)benzaldehyde

Reaction ID UCExp236-11

309



t-butyl isocyanide

24528281

Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.65 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp236

+

formic acid

+

benzylamine

+

4-(trifluoromethyl)benzaldehyde



t-butyl isocyanide

24528284

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCExp236-16 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.872 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp236

+

formic acid

+

butylamine

+

4-(trifluoromethyl)benzaldehyde



t-butyl isocyanide

24528289

Reaction ID UCExp236-19 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.927 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp236

+

formic acid

+

methylamine

+

4-(trifluoromethyl)benzaldehyde



n-butyl isocyanide

24528292

Reaction ID UCExp236-21 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.65 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp236

+

formic acid

+

aniline

+

4-(trifluoromethyl)benzaldehyde

furfurylamine 310



t-butyl isocyanide

24528294

Reaction ID UCEXP099C Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.405 M Precipitate Yes Yield 47.2 % Comments Solution was made up to 4 mL - methanol amount probably closer to 3 mL Reference http://usefulchem.wikispaces.com/Exp099

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde



t-butyl isocyanide

21106059

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCEXP104C Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.398 M Precipitate Yes Yield 12 % Comments Imine was preformed Reference http://usefulchem.wikispaces.com/Exp104

+

Boc-Gly-OH

+

furfurylamine

+

veratraldehyde



t-butyl isocyanide

21106057

Reaction ID UCEXP108C Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.393 M Precipitate Yes Yield 20.4 % Comments Imine was preformed Reference http://usefulchem.wikispaces.com/Exp108

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde



benzyl isocyanide

21106009

Reaction ID UCEXP130-4 Researcher Rikesh Parikh Reaction Type Ugi Solvent methanol Limiting Reactant 0.725 M Precipitate Yes Product Not Determined Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp130

+

+

+

311



formic acid

furfurylamine

2-naphthaldehyde

benzyl isocyanide

21106080

Reaction ID UCEXP130-5 Researcher Rikesh Parikh Reaction Type Ugi Solvent methanol Limiting Reactant 0.734 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp130

+

formic acid

+

+

furfurylamine

2-naphthaldehyde



n-butyl isocyanide

21106079

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCEXP131-1 Researcher Rikesh Parikh Reaction Type Ugi Solvent methanol Limiting Reactant 0.608 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp131

+

Boc-Trp-OH

+

+

furfurylamine

veratraldehyde



n-butyl isocyanide

21106067

Reaction ID UCEXP131-2 Researcher Rikesh Parikh Reaction Type Ugi Solvent methanol Limiting Reactant 0.623 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp131

+

Boc-Trp-OH

+

+

furfurylamine

veratraldehyde



1-pentyl isocyanide

21106068

Reaction ID UCEXP160C-V1B19 Researcher Emily Messner Reaction Type Ugi Solvent methanol Limiting Reactant 0.388 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp160

+

3,4-dihydroxyphenylacetic acid

+

furfurylamine

+

phenanthrene-9-carboxaldehyde

312



n-butyl isocyanide

21105579

Reaction ID UCEXP163A-V1B14 Researcher Tim Bohinsky Reaction Type Ugi Solvent methanol Limiting Reactant 0.387 M Precipitate no and aldehyde alone not solube Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp163

+

mandelic acid

+

furfurylamine

+

phenanthrene-9-carboxaldehyde



t-butyl isocyanide

21105596

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCEXP171GV2B7 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.218 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp171

+

3,4-dihydroxyphenylacetic acid

+

+

furfurylamine

2-naphthaldehyde



tosylmethyl isocyanide

21106054

Reaction ID UCEXP173F/V2B18 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.219 M Precipitate no and aldehyde alone not solube Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp173

+

2,3-dihydroxybenzoic acid

+

furfurylamine

+

phenanthrene-9-carboxaldehyde



t-butyl isocyanide

21106041

Reaction ID UCEXP173L/V2B24 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.221 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp173

+

3,4-dihydroxyphenylacetic acid

+

furfurylamine

+

3-hydroxybenzaldehyde

313



tosylmethyl isocyanide

21106051

Reaction ID UCEXP173M/V2B25 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.22 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp173

+

3,4-dihydroxyphenylacetic acid

+

furfurylamine

+

4-chlorobenzaldehyde



tosylmethyl isocyanide

21106043

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCEXP173O/V2B27 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.222 M Precipitate Yes Product pending Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp173

+

3,4-dihydroxyphenylacetic acid

+

furfurylamine

+

benzaldehyde



tosylmethyl isocyanide

21105843

Reaction ID UCEXP173Q/V2B29 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.22 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp173

+

3,4-dihydroxyphenylacetic acid

+

furfurylamine

+

4-methylbenzaldehyde



tosylmethyl isocyanide

21106042

Reaction ID UCEXP174B/V2B33 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.22 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp174

+

+

+

314



3,4-dihydroxyphenylacetic acid

furfurylamine

3-methoxybenzaldehyde

tosylmethyl isocyanide

21106204

Reaction ID UCEXP174D/V2B35 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.221 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp174

+

benzoic acid

+

furfurylamine

+

2-hydroxybenzaldehyde



tosylmethyl isocyanide

21106202

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCEXP174U/V2B54 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.22 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp174

+

3,4-dihydroxyphenylacetic acid

+

furfurylamine

+

4-methoxybenzaldehyde



tosylmethyl isocyanide

21106187

Reaction ID UCEXP176C Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant - M Precipitate Yes Yield 62 % Comments aldehyde not soluble until all reactants added Reference http://usefulchem.wikispaces.com/Exp176

+

phenylacetic acid

+

furfurylamine

+

phenanthrene-9-carboxaldehyde



n-butyl isocyanide

21105594

Reaction ID UCEXP178 Researcher Shannon Oseback Reaction Type Ugi Solvent methanol Limiting Reactant 0.388 M Precipitate Yes but the aldehyde alone is not soluble in methanol Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp178

+

+

+

315



phenylacetic acid

furfurylamine

phenanthrene-9-carboxaldehyde

n-butyl isocyanide

21105594

Reaction ID UCEXP181-056V2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.219 M Precipitate Reactants Insoluble Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

+

2,4,6-trihydroxybenzoic acid

+

furfurylamine

+

phenanthrene-9-carboxaldehyde



n-butyl isocyanide

24528097

Reaction ID UCEXP181-060V2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.221 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

+

phenylpropynoic acid

+

furfurylamine

+

2-hydroxybenzaldehyde



tosylmethyl isocyanide

24528100

Reaction ID UCEXP181-067V2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.221 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

+

3,4-dihydroxyphenylacetic acid

+

furfurylamine

+

4-hydroxybenzaldehyde

Reaction ID UCEXP181-075V2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.218 M Precipitate no and aldehyde alone not solube Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

316



tosylmethyl isocyanide

24528106

+

mandelic acid

+

furfurylamine

+

phenanthrene-9-carboxaldehyde



n-butyl isocyanide

24528111

Reaction ID UCEXP181-079V2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.218 M Precipitate Reactants Insoluble Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

+

2,4,6-trihydroxybenzoic acid

+

furfurylamine

+

phenanthrene-9-carboxaldehyde



t-butyl isocyanide

24528115

Reaction ID UCEXP181-082V2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.221 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

+

3,4-dihydroxyphenylacetic acid

+

furfurylamine

+

3,4-dihydroxybenzaldehyde



tosylmethyl isocyanide

24528118

Reaction ID UCEXP181-094V2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.217 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

+

3,4-dihydroxyphenylacetic acid

+

furfurylamine

+

3,5-dimethoxybenzaldehyde

Reaction ID UCEXP181-097V2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.221 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

317



tosylmethyl isocyanide

24528126

+

3,4-dihydroxyphenylacetic acid

+

furfurylamine

+

2-hydroxybenzaldehyde



tosylmethyl isocyanide

24528128

Reaction ID UCEXP181-117V2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.22 M Precipitate Reactants Insoluble Comments Protocol from Explan005 followed; hydrate of acid used Reference http://usefulchem.wikispaces.com/Exp181

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

+

2,4,6-trihydroxybenzoic acid

+

+

furfurylamine

veratraldehyde



tosylmethyl isocyanide

24534442

Reaction ID UCEXP181-123V2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.214 M Precipitate no and aldehyde alone not solube Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

+

3,4-dihydroxyphenylacetic acid

+

furfurylamine

+

phenanthrene-9-carboxaldehyde



tosylmethyl isocyanide

24528151

Reaction ID UCEXP201-01 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.039 M Precipitate Yes Yield 50.73 % Comments Automated liquid handling Reference http://usefulchem.wikispaces.com/Exp201

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde

Reaction ID UCEXP201-02 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.019 M Precipitate Yes

318



t-butyl isocyanide

21106059

Yield Comments Reference

59.07 % Automated liquid handling http://usefulchem.wikispaces.com/Exp201

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde



t-butyl isocyanide

21106059

Reaction ID UCEXP201-03

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.018 M Precipitate Yes Yield 61.55 % Comments Automated liquid handling Reference http://usefulchem.wikispaces.com/Exp201

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde



t-butyl isocyanide

21106059

Reaction ID UCEXP201-04 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.007 M Precipitate Yes Yield 60.31 % Comments Automated liquid handling Reference http://usefulchem.wikispaces.com/Exp201

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde



t-butyl isocyanide

21106059

Reaction ID UCEXP201-05 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.015 M Precipitate Yes Yield 60.2 % Comments Automated liquid handling Reference http://usefulchem.wikispaces.com/Exp201

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde

Reaction ID UCEXP201-06 Researcher Reaction Type Solvent

Khalid Mirza Ugi methanol

319



t-butyl isocyanide

21106059

Limiting Reactant 0.998 M Precipitate Yes Yield 69.22 % Comments Automated liquid handling Reference http://usefulchem.wikispaces.com/Exp201

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde



t-butyl isocyanide

21106059

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCEXP201-07 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.289 M Precipitate Yes Yield 52.42 % Comments Automated liquid handling Reference http://usefulchem.wikispaces.com/Exp201

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde



t-butyl isocyanide

21106059

Reaction ID UCEXP201-08 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.287 M Precipitate Yes Yield 44.64 % Comments Automated liquid handling Reference http://usefulchem.wikispaces.com/Exp201

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde



t-butyl isocyanide

21106059

Reaction ID UCEXP201-09 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.287 M Precipitate Yes Yield 50.28 % Comments Automated liquid handling Reference http://usefulchem.wikispaces.com/Exp201

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde

320



t-butyl isocyanide

21106059

Reaction ID UCEXP201-10 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.286 M Precipitate Yes Yield 54.79 % Comments Automated liquid handling Reference http://usefulchem.wikispaces.com/Exp201

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde



t-butyl isocyanide

21106059

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCEXP201-11 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.287 M Precipitate Yes Yield 53.43 % Comments Automated liquid handling Reference http://usefulchem.wikispaces.com/Exp201

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde



t-butyl isocyanide

21106059

Reaction ID UCEXP201-12 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.286 M Precipitate Yes Yield 54.67 % Comments Automated liquid handling Reference http://usefulchem.wikispaces.com/Exp201

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde



t-butyl isocyanide

21106059

Reaction ID UCEXP201-13 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.074 M Precipitate Yes Yield 0.34 % Comments Automated liquid handling Reference http://usefulchem.wikispaces.com/Exp201

+

+

+

321



Boc-Gly-OH

furfurylamine

benzaldehyde

t-butyl isocyanide

21106059

Reaction ID UCEXP201-14 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.074 M Precipitate Yes Yield 1.35 % Comments Automated liquid handling Reference http://usefulchem.wikispaces.com/Exp201

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde



t-butyl isocyanide

21106059

Reaction ID UCEXP201-15 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.074 M Precipitate Yes Yield 10.37 % Comments Automated liquid handling Reference http://usefulchem.wikispaces.com/Exp201

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde



t-butyl isocyanide

21106059

Reaction ID UCEXP201-16 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.074 M Precipitate Yes Yield 16.35 % Comments Automated liquid handling Reference http://usefulchem.wikispaces.com/Exp201

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde

Reaction ID UCEXP201-17 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.074 M Precipitate Yes Yield 8.68 %

322



t-butyl isocyanide

21106059

Comments Reference

Automated liquid handling http://usefulchem.wikispaces.com/Exp201

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde



t-butyl isocyanide

21106059

Reaction ID UCEXP201-18

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.074 M Precipitate Yes Yield 5.64 % Comments Automated liquid handling Reference http://usefulchem.wikispaces.com/Exp201

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde



t-butyl isocyanide

21106059

Reaction ID UCEXP201-19 Researcher Khalid Mirza Reaction Type Ugi Solvent ethanol Limiting Reactant 0.289 M Precipitate Yes Yield 51.52 % Comments Automated liquid handling Reference http://usefulchem.wikispaces.com/Exp201

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde



t-butyl isocyanide

21106059

Reaction ID UCEXP201-20 Researcher Khalid Mirza Reaction Type Ugi Solvent ethanol Limiting Reactant 0.287 M Precipitate Yes Yield 46.78 % Comments Automated liquid handling Reference http://usefulchem.wikispaces.com/Exp201

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde

Reaction ID UCEXP201-21 Researcher Khalid Mirza Reaction Type Ugi Solvent ethanol Limiting Reactant 0.287 M

323



t-butyl isocyanide

21106059

Precipitate Yield Comments Reference

Yes 51.29 % Automated liquid handling http://usefulchem.wikispaces.com/Exp201

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde



t-butyl isocyanide

21106059

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCEXP201-22 Researcher Khalid Mirza Reaction Type Ugi Solvent ethanol Limiting Reactant 0.286 M Precipitate Yes Yield 54.11 % Comments Automated liquid handling Reference http://usefulchem.wikispaces.com/Exp201

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde



t-butyl isocyanide

21106059

Reaction ID UCEXP201-23 Researcher Khalid Mirza Reaction Type Ugi Solvent ethanol Limiting Reactant 0.287 M Precipitate Yes Yield 55.91 % Comments Automated liquid handling Reference http://usefulchem.wikispaces.com/Exp201

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde



t-butyl isocyanide

21106059

Reaction ID UCEXP201-24 Researcher Khalid Mirza Reaction Type Ugi Solvent ethanol Limiting Reactant 0.286 M Precipitate Yes Yield 58.28 % Comments Automated liquid handling Reference http://usefulchem.wikispaces.com/Exp201

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde

324



t-butyl isocyanide

21106059

Reaction ID UCEXP201-25 Researcher Khalid Mirza Reaction Type Ugi Solvent ethanol Limiting Reactant 0.074 M Precipitate Yes Yield 1.24 % Comments Automated liquid handling Reference http://usefulchem.wikispaces.com/Exp201

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde



t-butyl isocyanide

21106059

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCEXP201-26 Researcher Khalid Mirza Reaction Type Ugi Solvent ethanol Limiting Reactant 0.074 M Precipitate Yes Yield 2.25 % Comments Automated liquid handling Reference http://usefulchem.wikispaces.com/Exp201

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde



t-butyl isocyanide

21106059

Reaction ID UCEXP201-27 Researcher Khalid Mirza Reaction Type Ugi Solvent ethanol Limiting Reactant 0.074 M Precipitate Yes Yield 7.78 % Comments Automated liquid handling Reference http://usefulchem.wikispaces.com/Exp201

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde



t-butyl isocyanide

21106059

Reaction ID UCEXP201-28 Researcher Khalid Mirza Reaction Type Ugi Solvent ethanol Limiting Reactant 0.074 M Precipitate Yes Yield 1.13 % Comments Automated liquid handling Reference http://usefulchem.wikispaces.com/Exp201

+

+

+

325



Boc-Gly-OH

furfurylamine

benzaldehyde

t-butyl isocyanide

21106059

Reaction ID UCEXP201-29 Researcher Khalid Mirza Reaction Type Ugi Solvent ethanol Limiting Reactant 0.074 M Precipitate Yes Yield 0.79 % Comments Automated liquid handling Reference http://usefulchem.wikispaces.com/Exp201

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde



t-butyl isocyanide

21106059

Reaction ID UCEXP201-30 Researcher Khalid Mirza Reaction Type Ugi Solvent ethanol Limiting Reactant 0.074 M Precipitate Yes Yield 0.23 % Comments Automated liquid handling Reference http://usefulchem.wikispaces.com/Exp201

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde



t-butyl isocyanide

21106059

Reaction ID UCEXP201-31 Researcher Khalid Mirza Reaction Type Ugi Solvent acetonitrile Limiting Reactant 0.289 M Precipitate Yes Yield 39.23 % Comments Automated liquid handling Reference http://usefulchem.wikispaces.com/Exp201

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde

Reaction ID UCEXP201-32 Researcher Khalid Mirza Reaction Type Ugi Solvent acetonitrile Limiting Reactant 0.287 M Precipitate Yes Yield 40.58 %

326



t-butyl isocyanide

21106059

Comments Reference

Automated liquid handling http://usefulchem.wikispaces.com/Exp201

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde



t-butyl isocyanide

21106059

Reaction ID UCEXP201-33

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Researcher Khalid Mirza Reaction Type Ugi Solvent acetonitrile Limiting Reactant 0.287 M Precipitate Yes Yield 43.85 % Comments Automated liquid handling Reference http://usefulchem.wikispaces.com/Exp201

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde



t-butyl isocyanide

21106059

Reaction ID UCEXP201-34 Researcher Khalid Mirza Reaction Type Ugi Solvent acetonitrile Limiting Reactant 0.286 M Precipitate Yes Yield 35.4 % Comments Automated liquid handling Reference http://usefulchem.wikispaces.com/Exp201

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde



t-butyl isocyanide

21106059

Reaction ID UCEXP201-35 Researcher Khalid Mirza Reaction Type Ugi Solvent acetonitrile Limiting Reactant 0.287 M Precipitate Yes Yield 41.37 % Comments Automated liquid handling Reference http://usefulchem.wikispaces.com/Exp201

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde

Reaction ID UCEXP201-36 Researcher Khalid Mirza Reaction Type Ugi Solvent acetonitrile Limiting Reactant 0.286 M

327



t-butyl isocyanide

21106059

Precipitate Yield Comments Reference

Yes 39.23 % Automated liquid handling http://usefulchem.wikispaces.com/Exp201

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde



t-butyl isocyanide

21106059

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCEXP201-37 Researcher Khalid Mirza Reaction Type Ugi Solvent acetonitrile Limiting Reactant 0.074 M Precipitate Yes Yield 0.68 % Comments Automated liquid handling Reference http://usefulchem.wikispaces.com/Exp201

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde



t-butyl isocyanide

21106059

Reaction ID UCEXP201-38 Researcher Khalid Mirza Reaction Type Ugi Solvent acetonitrile Limiting Reactant 0.074 M Precipitate Yes Yield 1.8 % Comments Automated liquid handling Reference http://usefulchem.wikispaces.com/Exp201

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde



t-butyl isocyanide

21106059

Reaction ID UCEXP201-39 Researcher Khalid Mirza Reaction Type Ugi Solvent acetonitrile Limiting Reactant 0.002 M Precipitate Yes Yield 1.01 % Comments Automated liquid handling Reference http://usefulchem.wikispaces.com/Exp201

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde

328



t-butyl isocyanide

21106059

Reaction ID UCEXP201-40 Researcher Khalid Mirza Reaction Type Ugi Solvent acetonitrile Limiting Reactant 0.074 M Precipitate Yes Yield 0.9 % Comments Automated liquid handling Reference http://usefulchem.wikispaces.com/Exp201

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde



t-butyl isocyanide

21106059

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCEXP201-41 Researcher Khalid Mirza Reaction Type Ugi Solvent acetonitrile Limiting Reactant 0.074 M Precipitate Yes Yield 1.01 % Comments Automated liquid handling Reference http://usefulchem.wikispaces.com/Exp201

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde



t-butyl isocyanide

21106059

Reaction ID UCEXP201-42 Researcher Khalid Mirza Reaction Type Ugi Solvent acetonitrile Limiting Reactant 0.074 M Precipitate Yes Yield 0.45 % Comments Automated liquid handling Reference http://usefulchem.wikispaces.com/Exp201

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde



t-butyl isocyanide

21106059

Reaction ID UCEXP201-43 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 0.289 M Precipitate Yes Yield 6.54 % Comments Automated liquid handling Reference http://usefulchem.wikispaces.com/Exp201

+

+

+

329



Boc-Gly-OH

furfurylamine

benzaldehyde

t-butyl isocyanide

21106059

Reaction ID UCEXP201-44 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 0.287 M Precipitate Yes Yield 7.89 % Comments Automated liquid handling Reference http://usefulchem.wikispaces.com/Exp201

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde



t-butyl isocyanide

21106059

Reaction ID UCEXP201-45 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 0.287 M Precipitate Yes Yield 10.03 % Comments Automated liquid handling Reference http://usefulchem.wikispaces.com/Exp201

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde



t-butyl isocyanide

21106059

Reaction ID UCEXP201-46 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 0.286 M Precipitate Yes Yield 9.92 % Comments Automated liquid handling Reference http://usefulchem.wikispaces.com/Exp201

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde

Reaction ID UCEXP201-47 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 0.287 M Precipitate Yes Yield 7.44 %

330



t-butyl isocyanide

21106059

Comments Reference

Automated liquid handling http://usefulchem.wikispaces.com/Exp201

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde



t-butyl isocyanide

21106059

Reaction ID UCEXP201-48

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 0.286 M Precipitate Yes Yield 12.06 % Comments Automated liquid handling Reference http://usefulchem.wikispaces.com/Exp201

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde



t-butyl isocyanide

21106059

Reaction ID UCEXP217-3 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 0.383 M Precipitate Yes Product Pending Comments Reference http://usefulchem.wikispaces.com/Exp217

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde



t-butyl isocyanide

21106059

Reaction ID UCEXP217-4 Researcher Khalid Mirza Reaction Type Ugi Solvent DMSO Limiting Reactant 0.383 M Precipitate Yes Product Pending Comments Reference http://usefulchem.wikispaces.com/Exp217

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde

Reaction ID UCEXP217-5 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 0.384 M

331



t-butyl isocyanide

21106059

Precipitate Product Comments Reference

Yes Pending http://usefulchem.wikispaces.com/Exp217

+

Boc-Gly-OH

+

furfurylamine

+

phenanthrene-9-carboxaldehyde



n-butyl isocyanide

21105594

Reaction ID UCEXP222-1

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Researcher Khalid Mirza Reaction Type Ugi Solvent DMSO Limiting Reactant 0.898 M Precipitate Yes Yield - % Comments Reference http://usefulchem.wikispaces.com/Exp222

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde



t-butyl isocyanide

21106059

Reaction ID UCEXP222-2 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 0.898 M Precipitate Yes Yield - % Comments Reference http://usefulchem.wikispaces.com/Exp222

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde



t-butyl isocyanide

21106059

Reaction ID UCEXP222-3 Researcher Khalid Mirza Reaction Type Ugi Solvent DMSO Limiting Reactant 0.473 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp222

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde

Reaction ID UCEXP222-4 Researcher Reaction Type Solvent

Khalid Mirza Ugi THF

332



t-butyl isocyanide

21106059

Limiting Reactant 0.473 M Precipitate Yes Yield - % Comments Reference http://usefulchem.wikispaces.com/Exp222

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde



t-butyl isocyanide

21106059

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCEXP225-1 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.631 M Precipitate Yes Yield - % Comments 0.5 mmol of isocyanide was added to 500uL of a 2M solution of aldehyde; amine and acid Reference http://usefulchem.wikispaces.com/Exp225

+

Boc-Gly-OH

+

furfurylamine

+

piperonal



t-butyl isocyanide

24528157

Reaction ID UCEXP225-2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.905 M Precipitate Yes Product Pending Comments 0.5 mmol of isocyanide was added to 500uL of a 2M solution of aldehyde; amine and acid Reference http://usefulchem.wikispaces.com/Exp225

+

Boc-Gly-OH

+

furfurylamine

+

piperonal



n-butyl isocyanide

24528158

Reaction ID UCEXP225-3 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.888 M Precipitate Yes Product Pending Comments 0.5 mmol of isocyanide was added to 500uL of a 2M solution of aldehyde; amine and acid Reference http://usefulchem.wikispaces.com/Exp225

+

Boc-Gly-OH

+

furfurylamine

+

piperonal

333



1-pentyl isocyanide

24528159

Reaction ID UCEXP225-4 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.889 M Precipitate Yes Product Pending Comments 0.5 mmol of isocyanide was added to 500uL of a 2M solution of aldehyde; amine and acid Reference http://usefulchem.wikispaces.com/Exp225

+

Boc-Gly-OH

+

furfurylamine

+

piperonal



cyclohexylisocyanide

24528160

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCEXP225-5 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.891 M Precipitate Yes Product Pending Comments 0.5 mmol of isocyanide was added to 500uL of a 2M solution of aldehyde; amine and acid Reference http://usefulchem.wikispaces.com/Exp225

+

Boc-Gly-OH

+

furfurylamine

+

piperonal



benzyl isocyanide

24528161

Reaction ID UCEXP225-6 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.438 M Precipitate No Comments 0.5 mmol of isocyanide was added to 500uL of a 2M solution of aldehyde; amine and acid Reference http://usefulchem.wikispaces.com/Exp225

+

Boc-Gly-OH

+

furfurylamine

+

piperonal



tosylmethyl isocyanide

24528162

Reaction ID UCEXP225-7 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.879 M Precipitate No Comments 0.5 mmol of isocyanide was added to 500uL of a 2M solution of aldehyde; amine and acid Reference http://usefulchem.wikispaces.com/Exp225

+

Boc-Gly-OH

+

furfurylamine

+

piperonal

334



2-morpholinoethyl isocyanide

24528163

Reaction ID UCEXP225-8 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.868 M Precipitate No Comments 0.5 mmol of isocyanide was added to 500uL of a 2M solution of aldehyde; amine and acid Reference http://usefulchem.wikispaces.com/Exp225

+

Boc-Gly-OH

+

furfurylamine

+



2-chloro-6methylphenyl isocyanide

piperonal

24528164

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCEXP227-1 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 0.261 M Precipitate No Comments 0.5 mmol of isocyanide was added to 500uL of a 0.5M solution of aldehyde; amine and acid Reference http://usefulchem.wikispaces.com/Exp227

+

1-pyrenebutyric acid

+

furfurylamine

+

piperonal



t-butyl isocyanide

24528173

Reaction ID UCEXP227-2 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 0.453 M Precipitate No Comments 0.5 mmol of isocyanide was added to 500uL of a 0.5M solution of aldehyde; amine and acid Reference http://usefulchem.wikispaces.com/Exp227

+

1-pyrenebutyric acid

+

furfurylamine

+

piperonal



n-butyl isocyanide

24528174

Reaction ID UCEXP227-3 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 0.444 M Precipitate No Comments 0.5 mmol of isocyanide was added to 500uL of a 0.5M solution of aldehyde; amine and acid Reference http://usefulchem.wikispaces.com/Exp227

+

1-pyrenebutyric acid

+

furfurylamine

+

piperonal

335



1-pentyl isocyanide

24528175

Reaction ID UCEXP227-4 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 0.445 M Precipitate No Comments 0.5 mmol of isocyanide was added to 500uL of a 0.5M solution of aldehyde; amine and acid Reference http://usefulchem.wikispaces.com/Exp227

+

1-pyrenebutyric acid

+

furfurylamine

+

piperonal



cyclohexylisocyanide

24528176

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCEXP227-5 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 0.446 M Precipitate No Comments 0.5 mmol of isocyanide was added to 500uL of a 0.5M solution of aldehyde; amine and acid Reference http://usefulchem.wikispaces.com/Exp227

+

1-pyrenebutyric acid

+

furfurylamine

+

piperonal



benzyl isocyanide

24528177

Reaction ID UCEXP227-6 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 0.251 M Precipitate No Comments 0.5 mmol of isocyanide was added to 500uL of a 0.5M solution of aldehyde; amine and acid Reference http://usefulchem.wikispaces.com/Exp227

+

1-pyrenebutyric acid

+

furfurylamine

+

piperonal



tosylmethyl isocyanide

24528178

Reaction ID UCEXP227-7 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 0.439 M Precipitate No Comments 0.5 mmol of isocyanide was added to 500uL of a 0.5M solution of aldehyde; amine and acid Reference http://usefulchem.wikispaces.com/Exp227

+

1-pyrenebutyric acid

+

furfurylamine

+

piperonal

336



2-morpholinoethyl isocyanide

24528179

Reaction ID UCEXP227-8 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 0.434 M Precipitate No Comments 0.5 mmol of isocyanide was added to 500uL of a 0.5M solution of aldehyde; amine and acid Reference http://usefulchem.wikispaces.com/Exp227

+

1-pyrenebutyric acid

+

furfurylamine

+



2-chloro-6methylphenyl isocyanide

piperonal

24528180

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCEXP231-7 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 0.667 M Precipitate Yes Product Pending Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp231

+

1-pyrenebutyric acid

+

furfurylamine

+

2-furaldehyde



n-butyl isocyanide

24528187

Reaction ID UCEXP232-01 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.098 M Precipitate Yes Product Pending Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde



t-butyl isocyanide

21106059

Reaction ID UCEXP232-02 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.098 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

+

+

+

337



Boc-Gly-OH

furfurylamine

benzaldehyde

n-butyl isocyanide

24528189

Reaction ID UCEXP232-03 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.099 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde



1-pentyl isocyanide

24528190

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCEXP232-04 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.098 M Precipitate Yes Product Pending Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde



cyclohexylisocyanide

24528191

Reaction ID UCEXP232-05 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.098 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+



1,1,3,3tetramethylbutyl isocyanide

benzaldehyde

24528192

Reaction ID UCEXP232-06 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.083 M Precipitate Yes Product Pending Comments Reference http://usefulchem.wikispaces.com/Exp232

+

+

+

338



Boc-Gly-OH

furfurylamine

4-methylbenzaldehyde

t-butyl isocyanide

24528193

Reaction ID UCEXP232-07 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.082 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

+

Boc-Gly-OH

+

furfurylamine

+

4-methylbenzaldehyde



n-butyl isocyanide

24528194

Reaction ID UCEXP232-08 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.083 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+

4-methylbenzaldehyde



1-pentyl isocyanide

24528195

Reaction ID UCEXP232-09 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.083 M Precipitate Yes Product Pending Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+

4-methylbenzaldehyde

Reaction ID UCEXP232-10 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.083 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

339



cyclohexylisocyanide

24528196

+

Boc-Gly-OH

+

+

furfurylamine



1,1,3,3tetramethylbutyl isocyanide

4-methylbenzaldehyde

24528197

Reaction ID UCEXP232-11

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.029 M Precipitate Yes Product Pending Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+

4-(trifluoromethyl)benzaldehyde



t-butyl isocyanide

24528198

Reaction ID UCEXP232-12 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.028 M Precipitate Yes Product Pending Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+

4-(trifluoromethyl)benzaldehyde



n-butyl isocyanide

24528199

Reaction ID UCEXP232-13 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.029 M Precipitate Yes Product Pending Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+

4-(trifluoromethyl)benzaldehyde

Reaction ID UCEXP232-14 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.028 M

340



1-pentyl isocyanide

24528200

Precipitate Product Comments Reference

Yes Pending http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+

4-(trifluoromethyl)benzaldehyde



cyclohexylisocyanide

21782441

Reaction ID UCEXP232-15

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.028 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+



1,1,3,3tetramethylbutyl isocyanide

4-(trifluoromethyl)benzaldehyde

24528201

Reaction ID UCEXP232-16 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.366 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+

crotonaldehyde



t-butyl isocyanide

24528202

Reaction ID UCEXP232-17 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.365 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+

crotonaldehyde

Reaction ID UCEXP232-18 Researcher Reaction Type Solvent

Khalid Mirza Ugi methanol

341



n-butyl isocyanide

24528203

Limiting Reactant 1.367 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+

crotonaldehyde



1-pentyl isocyanide

24528204

Reaction ID UCEXP232-19

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.366 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+

crotonaldehyde



cyclohexylisocyanide

24528205

Reaction ID UCEXP232-20 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.366 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+



1,1,3,3tetramethylbutyl isocyanide

crotonaldehyde

24528206

Reaction ID UCEXP232-21 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.008 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+

diphenylacetaldehyde

Reaction ID UCEXP232-22 Researcher Reaction Type Solvent

Khalid Mirza Ugi methanol

342



t-butyl isocyanide

24528207

Limiting Reactant 1.007 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+

diphenylacetaldehyde



n-butyl isocyanide

24528208

Reaction ID UCEXP232-23

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.008 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+

diphenylacetaldehyde



1-pentyl isocyanide

24528209

Reaction ID UCEXP232-24 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.008 M Precipitate Yes Product Pending Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+

diphenylacetaldehyde



cyclohexylisocyanide

24528210

Reaction ID UCEXP232-25 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.008 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+

diphenylacetaldehyde

Reaction ID UCEXP232-26 Researcher Reaction Type

Khalid Mirza Ugi

343



1,1,3,3tetramethylbutyl isocyanide

24528211

Solvent methanol Limiting Reactant 1.092 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+

cyclohexancarboxaldehyde



t-butyl isocyanide

24528212

Reaction ID UCEXP232-27

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.092 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+

cyclohexancarboxaldehyde



n-butyl isocyanide

24528213

Reaction ID UCEXP232-28 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.093 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+

cyclohexancarboxaldehyde



1-pentyl isocyanide

24528214

Reaction ID UCEXP232-29 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.092 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+

cyclohexancarboxaldehyde

Reaction ID UCEXP232-30 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.092 M

344



cyclohexylisocyanide

24528215

Precipitate Comments Reference

No http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+



1,1,3,3tetramethylbutyl isocyanide

cyclohexancarboxaldehyde

24528216

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCEXP232-31 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.11 M Precipitate Yes Product Pending Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+

2-furaldehyde



t-butyl isocyanide

24528217

Reaction ID UCEXP232-32 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.11 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+

2-furaldehyde



n-butyl isocyanide

24528218

Reaction ID UCEXP232-33 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.111 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+

2-furaldehyde

Reaction ID UCEXP232-34 Researcher Reaction Type Solvent

Khalid Mirza Ugi methanol

345



1-pentyl isocyanide

24528219

Limiting Reactant 1.11 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

+

furfurylamine

2-furaldehyde



cyclohexylisocyanide

24528220

Reaction ID UCEXP232-35

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.11 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

+

furfurylamine



1,1,3,3tetramethylbutyl isocyanide

2-furaldehyde

24528221

Reaction ID UCEXP232-36 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.081 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+

2-hydroxybenzaldehyde



t-butyl isocyanide

24528222

Reaction ID UCEXP232-37 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.081 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+

2-hydroxybenzaldehyde

Reaction ID UCEXP232-38 Researcher Reaction Type Solvent

Khalid Mirza Ugi methanol

346



n-butyl isocyanide

24528223

Limiting Reactant 1.081 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+

2-hydroxybenzaldehyde



1-pentyl isocyanide

24528224

Reaction ID UCEXP232-39

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.081 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+

2-hydroxybenzaldehyde



cyclohexylisocyanide

24528225

Reaction ID UCEXP232-40 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.081 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+



1,1,3,3tetramethylbutyl isocyanide

2-hydroxybenzaldehyde

24528226

Reaction ID UCEXP232-41 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.083 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+

o-tolualdehyde

Reaction ID UCEXP232-42 Researcher Reaction Type Solvent

Khalid Mirza Ugi methanol

347



t-butyl isocyanide

24528227

Limiting Reactant 1.083 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+

o-tolualdehyde



n-butyl isocyanide

24528228

Reaction ID UCEXP232-43

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.083 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+

o-tolualdehyde



1-pentyl isocyanide

24528229

Reaction ID UCEXP232-44 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.083 M Precipitate Yes Product Pending Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+

o-tolualdehyde



cyclohexylisocyanide

24528230

Reaction ID UCEXP232-45 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.083 M Precipitate Yes Product Pending Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+

o-tolualdehyde

Reaction ID UCEXP232-46 Researcher

Khalid Mirza

348



1,1,3,3tetramethylbutyl isocyanide

24528231

Reaction Type Ugi Solvent methanol Limiting Reactant 1.066 M Precipitate Yes Product Pending Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+

4-methoxybenzaldehyde



t-butyl isocyanide

24528232

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCEXP232-47 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.066 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+

4-methoxybenzaldehyde



n-butyl isocyanide

24528233

Reaction ID UCEXP232-48 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.067 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+

4-methoxybenzaldehyde



1-pentyl isocyanide

24528234

Reaction ID UCEXP232-49 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.066 M Precipitate Yes Product Pending Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+

4-methoxybenzaldehyde

Reaction ID UCEXP232-50 Researcher

Khalid Mirza

349



cyclohexylisocyanide

24528235

Reaction Type Ugi Solvent methanol Limiting Reactant 1.066 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+



1,1,3,3tetramethylbutyl isocyanide

4-methoxybenzaldehyde

24528236

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCEXP232-51 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.106 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+

hexanaldehyde



t-butyl isocyanide

24528237

Reaction ID UCEXP232-52 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.105 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+

hexanaldehyde



n-butyl isocyanide

24528238

Reaction ID UCEXP232-53 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.106 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+

hexanaldehyde

Reaction ID UCEXP232-54 Researcher

Khalid Mirza

350



1-pentyl isocyanide

24528239

Reaction Type Ugi Solvent methanol Limiting Reactant 1.106 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+

hexanaldehyde



cyclohexylisocyanide

24528240

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCEXP232-55 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.106 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+



1,1,3,3tetramethylbutyl isocyanide

hexanaldehyde

24528241

Reaction ID UCEXP232-56 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.109 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+

trans-2-hexenal



t-butyl isocyanide

24528242

Reaction ID UCEXP232-57 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.109 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+

trans-2-hexenal

Reaction ID UCEXP232-58 Researcher

Khalid Mirza

351



n-butyl isocyanide

24528243

Reaction Type Ugi Solvent methanol Limiting Reactant 1.109 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

+

furfurylamine

trans-2-hexenal



1-pentyl isocyanide

24528243

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCEXP232-59 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.109 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

+

furfurylamine

trans-2-hexenal



cyclohexylisocyanide

24528244

Reaction ID UCEXP232-60 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.109 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

+

furfurylamine



1,1,3,3tetramethylbutyl isocyanide

trans-2-hexenal

24528245

Reaction ID UCEXP232-61 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.069 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+

2-phenylpropionaldehyde

Reaction ID UCEXP232-62 Researcher

Khalid Mirza

352



t-butyl isocyanide

24534409

Reaction Type Ugi Solvent methanol Limiting Reactant 1.069 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+

2-phenylpropionaldehyde



n-butyl isocyanide

24534417

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCEXP232-63 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.07 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+

2-phenylpropionaldehyde



1-pentyl isocyanide

24534418

Reaction ID UCEXP232-64 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.069 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+

2-phenylpropionaldehyde



cyclohexylisocyanide

24534419

Reaction ID UCEXP232-65 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.069 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+

2-phenylpropionaldehyde

Reaction ID UCEXP232-66 Researcher

Khalid Mirza

353



1,1,3,3tetramethylbutyl isocyanide

24534420

Reaction Type Ugi Solvent methanol Limiting Reactant 1.067 M Precipitate Yes Product Pending Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+

m-anisaldehyde



t-butyl isocyanide

24528251

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCEXP232-67 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.068 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+

m-anisaldehyde



n-butyl isocyanide

24528252

Reaction ID UCEXP232-68 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.067 M Precipitate Yes Product Pending Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+

m-anisaldehyde



1-pentyl isocyanide

24528253

Reaction ID UCEXP232-69 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.067 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+

m-anisaldehyde

Reaction ID UCEXP232-70 Researcher

Khalid Mirza

354



cyclohexylisocyanide

24528254

Reaction Type Ugi Solvent methanol Limiting Reactant 1.067 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+



1,1,3,3tetramethylbutyl isocyanide

m-anisaldehyde

24528255

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCEXP232-71 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.106 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+

2-ethylbutyraldehyde



t-butyl isocyanide

24528256

Reaction ID UCEXP232-72 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.105 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+

2-ethylbutyraldehyde



n-butyl isocyanide

24528257

Reaction ID UCEXP232-73 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.106 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+

2-ethylbutyraldehyde

Reaction ID UCEXP232-74 Researcher

Khalid Mirza

355



1-pentyl isocyanide

24528258

Reaction Type Ugi Solvent methanol Limiting Reactant 1.105 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

+

furfurylamine

2-ethylbutyraldehyde



cyclohexylisocyanide

24528259

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCEXP232-75 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.105 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

+

furfurylamine



1,1,3,3tetramethylbutyl isocyanide

2-ethylbutyraldehyde

24528260

Reaction ID UCExp235-1 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1 M Precipitate Yes Product No Comments Reference http://usefulchem.wikispaces.com/Exp235

+

Boc-Gly-OH

+

furfurylamine

+

4-(trifluoromethyl)benzaldehyde



t-butyl isocyanide

24528198

Reaction ID UCExp235-2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1 M Precipitate Yes Product No Comments Reference http://usefulchem.wikispaces.com/Exp235

+

Boc-Gly-OH

+

furfurylamine

+

4-(trifluoromethyl)benzaldehyde

356



cyclohexylisocyanide

21782441

Reaction ID UCExp237-01 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.778 M Precipitate Yes Product Awaiting Characterization Comments Reference http://usefulchem.wikispaces.com/Exp237

+

phenylacetic acid

+

furfurylamine

+

phenanthrene-9-carboxaldehyde



n-butyl isocyanide

21105594

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCExp237-02 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 0.746 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp237

+

phenylacetic acid

+

furfurylamine

+

phenanthrene-9-carboxaldehyde



n-butyl isocyanide

21105594

Reaction ID UCExp238-07 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.628 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp238

+

crotonic acid

+

furfurylamine

+

phenanthrene-9-carboxaldehyde



cyclohexylisocyanide

24528309

Reaction ID UCExp238-19 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.658 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp238

+

crotonic acid

+

furfurylamine

Reaction ID UCExp238-31

+

phenanthrene-9-carboxaldehyde

357



t-butyl isocyanide

24528320

Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.48 M Precipitate Yes but solvent evaporated Comments Reference http://usefulchem.wikispaces.com/Exp238

+

Boc-Gly-OH

+

furfurylamine

+

phenanthrene-9-carboxaldehyde



cyclohexylisocyanide

24528331

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCExp238-43 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.505 M Precipitate Yes Product Awaiting Characterization Comments Reference http://usefulchem.wikispaces.com/Exp238

+

Boc-Gly-OH

+

furfurylamine

+

phenanthrene-9-carboxaldehyde



t-butyl isocyanide

24528343

Reaction ID UCExp240-01 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.607 M Precipitate Yes but after 48h Comments Reference http://usefulchem.wikispaces.com/Exp240

+

phenylacetic acid

+

furfurylamine

+

phenanthrene-9-carboxaldehyde



n-butyl isocyanide

21105594

Reaction ID UCExp240-02 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.587 M Precipitate Yes Yield - % Comments Reference http://usefulchem.wikispaces.com/Exp240

+

phenylacetic acid

+

furfurylamine

+

phenanthrene-9-carboxaldehyde

Reaction ID UCExp240-03

358



t-butyl isocyanide

21791788

Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.562 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp240

+

phenylacetic acid

+

furfurylamine

+

phenanthrene-9-carboxaldehyde



cyclohexylisocyanide

24528345

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCExp240-04 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.458 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp240

+

phenylacetic acid

+

furfurylamine

+



1,1,3,3tetramethylbutyl isocyanide

phenanthrene-9-carboxaldehyde

21782583

Reaction ID UCExp240-05 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.568 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp240

+

phenylacetic acid

+

furfurylamine

+

phenanthrene-9-carboxaldehyde



benzyl isocyanide

24528346

Reaction ID UCExp240-06 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.559 M Precipitate Yes Yield - % Comments Reference http://usefulchem.wikispaces.com/Exp240

+

phenylacetic acid

+

furfurylamine

+

phenanthrene-9-carboxaldehyde

359



1-pentyl isocyanide

24528347

Reaction ID UCExp241-43 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.71 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp241

+

3,4methylenedioxyphenylacetic acid

+

furfurylamine

+

4-(trifluoromethyl)benzaldehyde



t-butyl isocyanide

24528376

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCExp242-1 Researcher Marshall Moritz Reaction Type Ugi Solvent benzene Limiting Reactant 0.435 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp242

+

phenylacetic acid

+

furfurylamine

+

phenanthrene-9-carboxaldehyde



n-butyl isocyanide

21105594

Reaction ID UCExp242-2 Researcher Marshall Moritz Reaction Type Ugi Solvent benzene Limiting Reactant 0.436 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp242

+

phenylacetic acid

+

furfurylamine

+

phenanthrene-9-carboxaldehyde



t-butyl isocyanide

24528383

Reaction ID UCExp242-3 Researcher Marshall Moritz Reaction Type Ugi Solvent benzene Limiting Reactant 0.432 M Precipitate Yes Product No Comments Reference http://usefulchem.wikispaces.com/Exp242

+

phenylacetic acid

+

furfurylamine

+

phenanthrene-9-carboxaldehyde

360



cyclohexylisocyanide

24528384

Reaction ID UCExp242-4 Researcher Marshall Moritz Reaction Type Ugi Solvent benzene Limiting Reactant 0.414 M Precipitate Yes Product No Comments Reference http://usefulchem.wikispaces.com/Exp242

+

phenylacetic acid

+

furfurylamine

+



1,1,3,3tetramethylbutyl isocyanide

phenanthrene-9-carboxaldehyde

24528385

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCExp242-5 Researcher Marshall Moritz Reaction Type Ugi Solvent benzene Limiting Reactant 0.432 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp242

+

phenylacetic acid

+

furfurylamine

+

phenanthrene-9-carboxaldehyde



1-pentyl isocyanide

24528386

Reaction ID UCExp245-01 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.509 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp245

+

3,4methylenedioxyphenylacetic acid

+

furfurylamine

+

piperonal



n-butyl isocyanide

24528391

Reaction ID UCExp245-02 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.718 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp245

+

+

+

361



3,4methylenedioxyphenylacetic acid

furfurylamine

piperonal

n-butyl isocyanide

24528391

Reaction ID UCExp245-05

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.507 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp245

+

3,4methylenedioxyphenylacetic acid

+

furfurylamine

+

piperonal



t-butyl isocyanide

24528393

Reaction ID UCExp245-06 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.714 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp245

+

3,4methylenedioxyphenylacetic acid

+

furfurylamine

+

piperonal



t-butyl isocyanide

24528393

Reaction ID UCExp245-07 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.504 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp245

+

3,4methylenedioxyphenylacetic acid

+

furfurylamine

+

piperonal

Reaction ID UCExp245-08 Researcher Reaction Type

Khalid Mirza Ugi

362



cyclohexylisocyanide

24528394

Solvent methanol Limiting Reactant 0.708 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp245

+

3,4methylenedioxyphenylacetic acid

+

furfurylamine

+

piperonal



cyclohexylisocyanide

24528394

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCExp245-09 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.492 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp245

+

3,4methylenedioxyphenylacetic acid

+

furfurylamine

+



1,1,3,3tetramethylbutyl isocyanide

piperonal

24528395

Reaction ID UCExp245-10 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.683 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp245

+

3,4methylenedioxyphenylacetic acid

+

furfurylamine

+



1,1,3,3tetramethylbutyl isocyanide

piperonal

24528395

Reaction ID UCExp245-17 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.502 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp245

+

cbz-proline

+

furfurylamine

+

piperonal

363



n-butyl isocyanide

24528399

Reaction ID UCExp245-18 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.12 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp245

+

cbz-proline

+

furfurylamine

+

piperonal



n-butyl isocyanide

24528399

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCExp245-21 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.5 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp245

+

cbz-proline

+

furfurylamine

+

piperonal



t-butyl isocyanide

24528401

Reaction ID UCExp245-22 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.109 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp245

+

cbz-proline

+

furfurylamine

+

piperonal



t-butyl isocyanide

24528401

Reaction ID UCExp245-23 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.497 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp245

+

cbz-proline

+

furfurylamine

+

piperonal

Reaction ID UCExp245-24

364



cyclohexylisocyanide

24528402

Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.096 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp245

+

cbz-proline

+

furfurylamine

+

piperonal



cyclohexylisocyanide

24528402

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCExp245-25 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.509 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp245

+

cbz-proline

+

furfurylamine

+



1,1,3,3tetramethylbutyl isocyanide

piperonal

24528403

Reaction ID UCExp245-26 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.038 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp245

+

cbz-proline

+

furfurylamine

+



1,1,3,3tetramethylbutyl isocyanide

piperonal

24528403

Reaction ID UCExp245-33 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.507 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp245

+

3,4methylenedioxyphenylacetic acid

+

furfurylamine

+

piperonal

365



t-butyl isocyanide

24528407

Reaction ID UCExp245-34 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.714 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp245

+

3,4methylenedioxyphenylacetic acid

+

furfurylamine

+

piperonal



t-butyl isocyanide

24528407

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCExp245-35 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.492 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp245

+

3,4methylenedioxyphenylacetic acid

+

furfurylamine

+



1,1,3,3tetramethylbutyl isocyanide

piperonal

24528408

Reaction ID UCExp245-36 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.683 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp245

+

3,4methylenedioxyphenylacetic acid

+

furfurylamine

+



1,1,3,3tetramethylbutyl isocyanide

piperonal

24528408

Reaction ID UCExp245-37 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.509 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp245

+

+

+

366



3,4methylenedioxyphenylacetic acid

furfurylamine

piperonal

n-butyl isocyanide

24528409

Reaction ID UCExp245-38

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.718 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp245

+

3,4methylenedioxyphenylacetic acid

+

+

furfurylamine

piperonal



n-butyl isocyanide

24528409

Reaction ID UCExp252-01 Researcher Khalid Mirza Reaction Type Ugi Solvent benzene Limiting Reactant 0.403 M Precipitate Yes Yield - % Comments Reference http://usefulchem.wikispaces.com/Exp252

+

phenylacetic acid

+

furfurylamine

+

phenanthrene-9-carboxaldehyde



n-butyl isocyanide

21105594

Reaction ID UCExp253-01 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.53 M Precipitate Yes Yield 42.6 % Comments Reference http://usefulchem.wikispaces.com/Exp253

+

phenylacetic acid

+

furfurylamine

+

phenanthrene-9-carboxaldehyde

Reaction ID UCExp254-01 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.08 M

367



n-butyl isocyanide

21105594

Precipitate Yield Comments Reference

Yes - % http://usefulchem.wikispaces.com/Exp254

+

phenylacetic acid

+

furfurylamine

+

phenanthrene-9-carboxaldehyde



n-butyl isocyanide

21105594

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCExp255-01 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.4 M Precipitate Yes Yield 65.8 % Comments Reference http://usefulchem.wikispaces.com/Exp255

+

phenylacetic acid

+

furfurylamine

+

phenanthrene-9-carboxaldehyde



n-butyl isocyanide

21105594

Reaction ID UCExp255-02 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.4 M Precipitate Yes Yield 65.1 % Comments Reference http://usefulchem.wikispaces.com/Exp255

+

phenylacetic acid

+

furfurylamine

+

phenanthrene-9-carboxaldehyde



n-butyl isocyanide

21105594

Reaction ID UCExp255-03 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.4 M Precipitate Yes Yield 66.4 % Comments Reference http://usefulchem.wikispaces.com/Exp255

+

phenylacetic acid

+

furfurylamine

+

phenanthrene-9-carboxaldehyde

368



n-butyl isocyanide

21105594

Reaction ID UCExp255-04 Researcher Khalid Mirza Reaction Type Ugi Solvent benzene Limiting Reactant 0.4 M Precipitate Yes Yield 29.7 % Comments Reference http://usefulchem.wikispaces.com/Exp255

+

phenylacetic acid

+

furfurylamine

+

phenanthrene-9-carboxaldehyde



n-butyl isocyanide

21105594

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCExp255-05 Researcher Khalid Mirza Reaction Type Ugi Solvent benzene Limiting Reactant 0.4 M Precipitate Yes Yield 30.5 % Comments Reference http://usefulchem.wikispaces.com/Exp255

+

phenylacetic acid

+

furfurylamine

+

phenanthrene-9-carboxaldehyde



n-butyl isocyanide

21105594

Reaction ID UCExp255-06 Researcher Khalid Mirza Reaction Type Ugi Solvent benzene Limiting Reactant 0.4 M Precipitate Yes Yield 28.9 % Comments Reference http://usefulchem.wikispaces.com/Exp255

+

phenylacetic acid

+

furfurylamine

+

phenanthrene-9-carboxaldehyde



n-butyl isocyanide

21105594

Reaction ID UCExp256-01 Researcher Khalid Mirza Reaction Type Ugi Solvent benzene Limiting Reactant 0.4 M Precipitate Yes Yield 17 % Comments Reference http://usefulchem.wikispaces.com/Exp256

+

+

+

369



phenylacetic acid

furfurylamine

phenanthrene-9-carboxaldehyde

n-butyl isocyanide

21105594

Reaction ID UCExp257-01 Researcher Khalid Mirza Reaction Type Ugi Solvent ethyl acetate Limiting Reactant 0.37 M Precipitate Yes Yield 24 % Comments Reference http://usefulchem.wikispaces.com/Exp257

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

+

+

phenylacetic acid

furfurylamine

+

phenanthrene-9-carboxaldehyde



n-butyl isocyanide

21105594

furoic acid Reaction ID UCEXP182 Researcher Emily Messner Reaction Type Ugi Solvent methanol Limiting Reactant 0.398 M Precipitate Reactants Insoluble Comments Reference http://usefulchem.wikispaces.com/Exp182

+

+

furoic acid

1-heptylamine

+

phenanthrene-9-carboxaldehyde



n-butyl isocyanide

21168529

glycine methyl ester hydrochloride Reaction ID UCEXP234-11 Researcher David Bulger Reaction Type Ugi Solvent methanol Limiting Reactant 0.893 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp234

+

Boc-L-Threonine

+

glycine methyl ester hydrochloride

+

3,5-dimethoxybenzaldehyde

Reaction ID UCEXP234-12 Researcher

David Bulger

370



t-butyl isocyanide

24528268

Reaction Type Ugi Solvent methanol Limiting Reactant 0.891 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp234

+

+

glycine methyl ester hydrochloride

Boc-L-Threonine

+

3,5-dimethoxybenzaldehyde



cyclohexylisocyanide

24528269

glycolic acid

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCEXP231-8 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 0.833 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp231

+

glycolic acid

+

1-heptylamine

+

2-methoxy-1-naphthaldehyde



tosylmethyl isocyanide

24528188

hexanaldehyde Reaction ID UCEXP232-51 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.106 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+

hexanaldehyde



t-butyl isocyanide

24528237

Reaction ID UCEXP232-52 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.105 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

+

+

+

371



Boc-Gly-OH

furfurylamine

hexanaldehyde

n-butyl isocyanide

24528238

Reaction ID UCEXP232-53 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.106 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

+

Boc-Gly-OH

+

furfurylamine

+

hexanaldehyde



1-pentyl isocyanide

24528239

Reaction ID UCEXP232-54 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.106 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+

hexanaldehyde



cyclohexylisocyanide

24528240

Reaction ID UCEXP232-55 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.106 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+

hexanaldehyde

hexanoic acid Reaction ID UCEXP181-089V2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.221 M

372



1,1,3,3tetramethylbutyl isocyanide

24528241

Precipitate Comments Reference

Reactants Insoluble Protocol from Explan005 followed http://usefulchem.wikispaces.com/Exp181

+

hexanoic acid

+

3-chloroaniline

+

2-hydroxybenzaldehyde



tosylmethyl isocyanide

24528122

Reaction ID UCEXP181-093V2

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.221 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

+

+

hexanoic acid

aniline

+

2-hydroxybenzaldehyde



tosylmethyl isocyanide

24528125

m-anisaldehyde Reaction ID UCEXP232-66 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.067 M Precipitate Yes Product Pending Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+

m-anisaldehyde



t-butyl isocyanide

24528251

Reaction ID UCEXP232-67 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.068 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+

m-anisaldehyde

Reaction ID UCEXP232-68 Researcher Reaction Type

Khalid Mirza Ugi

373



n-butyl isocyanide

24528252

Solvent methanol Limiting Reactant 1.067 M Precipitate Yes Product Pending Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+

m-anisaldehyde



1-pentyl isocyanide

24528253

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCEXP232-69 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.067 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+

m-anisaldehyde



cyclohexylisocyanide

24528254

Reaction ID UCEXP232-70 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.067 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+



1,1,3,3tetramethylbutyl isocyanide

m-anisaldehyde

24528255

Reaction ID UCExp241-02 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.502 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp241

+

3,4methylenedioxyphenylacetic acid

+

methylamine

+

m-anisaldehyde

374



benzyl isocyanide

24534408

mandelic acid Reaction ID UCEXP163A-V1B14 Researcher Tim Bohinsky Reaction Type Ugi Solvent methanol Limiting Reactant 0.387 M Precipitate no and aldehyde alone not solube Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp163

+

mandelic acid

+

furfurylamine

+

phenanthrene-9-carboxaldehyde



t-butyl isocyanide

21105596

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCEXP174R/V2B51 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.221 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp174

+

mandelic acid

+

3-chloroaniline

+

2-hydroxybenzaldehyde



tosylmethyl isocyanide

21106190

Reaction ID UCEXP181-071V2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.221 M Precipitate Yes Product No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

+

mandelic acid

+

benzylamine

+

benzaldehyde



tosylmethyl isocyanide

24528531

Reaction ID UCEXP181-075V2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.218 M Precipitate no and aldehyde alone not solube Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

+

+

+

375



mandelic acid

furfurylamine

phenanthrene-9-carboxaldehyde

n-butyl isocyanide

24528111

Reaction ID UCEXP181-084V2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.225 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

+

mandelic acid

+

benzylamine

+

3-methoxybenzaldehyde



n-butyl isocyanide

24528119

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCEXP181-103V2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.226 M Precipitate no and aldehyde alone not solube Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

+

mandelic acid

+

methylamine

+

phenanthrene-9-carboxaldehyde



n-butyl isocyanide

24528133

Reaction ID UCEXP183-049V1 Researcher Emily Messner Reaction Type Ugi Solvent methanol Limiting Reactant 0.398 M Precipitate Reactants Insoluble Comments Reference http://usefulchem.wikispaces.com/Exp183

+

mandelic acid

+

cyclohexylamine

+

phenanthrene-9-carboxaldehyde



t-butyl isocyanide

24528153

Reaction ID UCEXP184-1/49 Researcher Emily Messner Reaction Type Ugi Solvent ethanol Limiting Reactant 0.398 M Precipitate Reactants insoluble Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp184

+

mandelic acid

+

cyclohexylamine

+

phenanthrene-9-carboxaldehyde

376



t-butyl isocyanide

24528154

Reaction ID UCEXP184-2/49 Researcher Emily Messner Reaction Type Ugi Solvent acetonitrile Limiting Reactant 0.398 M Precipitate Reactants insoluble Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp184

+

mandelic acid

+

cyclohexylamine

+

phenanthrene-9-carboxaldehyde



t-butyl isocyanide

24528154

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCEXP184-3/49 Researcher Emily Messner Reaction Type Ugi Solvent dichloromethane Limiting Reactant 0.398 M Precipitate Reactants insoluble Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp184

+

mandelic acid

+

cyclohexylamine

+

phenanthrene-9-carboxaldehyde



t-butyl isocyanide

24528154

methacrylic acid Reaction ID UCEXP174I/V2B41 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.224 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp174

+

+

methacrylic acid

aniline

+

3,4-dihydroxybenzaldehyde



tosylmethyl isocyanide

21106198

Reaction ID UCEXP185-1 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.409 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp185

+

methacrylic acid

+

5-methylfurfurylamine

+

4-(trifluoromethyl)benzaldehyde

377



t-butyl isocyanide

21111670

Reaction ID UCEXP185-2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.409 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp185

+

methacrylic acid

+

benzylamine

+

4-(trifluoromethyl)benzaldehyde



t-butyl isocyanide

21111671

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCEXP187-1 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.057 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp187

+

methacrylic acid

+

5-methylfurfurylamine

+

4-(trifluoromethyl)benzaldehyde



t-butyl isocyanide

21111670

Reaction ID UCEXP187-2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.06 M Precipitate Yes Yield - % Comments Reference http://usefulchem.wikispaces.com/Exp187

+

methacrylic acid

+

benzylamine

+

4-(trifluoromethyl)benzaldehyde



t-butyl isocyanide

21111671

Reaction ID UCEXP187-3 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.064 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp187

+

methacrylic acid

+

t-butylamine

+

4-(trifluoromethyl)benzaldehyde

378



t-butyl isocyanide

21143155

Reaction ID UCEXP188-1 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.225 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp188

+

methacrylic acid

+

5-methylfurfurylamine

+

4-(trifluoromethyl)benzaldehyde



t-butyl isocyanide

21111670

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCEXP188-2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.225 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp188

+

methacrylic acid

+

benzylamine

+

4-(trifluoromethyl)benzaldehyde



t-butyl isocyanide

21111671

Reaction ID UCEXP188-3 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.225 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp188

+

methacrylic acid

+

t-butylamine

+

4-(trifluoromethyl)benzaldehyde



t-butyl isocyanide

21143155

Reaction ID UCExp236-04 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.844 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp236

+

methacrylic acid

+

butylamine

+

4-(trifluoromethyl)benzaldehyde

Reaction ID UCExp236-10

379



t-butyl isocyanide

24528278

Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.888 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp236

+

methacrylic acid

+

methylamine

+

4-(trifluoromethyl)benzaldehyde



n-butyl isocyanide

24528283

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCExp236-12 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.636 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp236

+

+

methacrylic acid

aniline

+

4-(trifluoromethyl)benzaldehyde



t-butyl isocyanide

24528285

Reaction ID UCExp236-20 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.631 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp236

+

methacrylic acid

+

t-butylamine

+

4-(trifluoromethyl)benzaldehyde



n-butyl isocyanide

24528293

Reaction ID UCExp236-23 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.631 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp236

+

methacrylic acid

+

3-chloroaniline

+

4-(trifluoromethyl)benzaldehyde

Reaction ID UCExp236-24 Researcher Reaction Type

Khalid Mirza Ugi

380



n-butyl isocyanide

24528296

Solvent methanol Limiting Reactant 0.63 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp236

+

+

methacrylic acid

benzylamine

+

4-(trifluoromethyl)benzaldehyde



n-butyl isocyanide

24528297

Reaction ID UCExp236-28

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.631 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp236

+

+

methacrylic acid

1-hexylamine

+

4-(trifluoromethyl)benzaldehyde



t-butyl isocyanide

24528301

methoxy acetic ac id Reaction ID UCEXP231-4 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 2 M Precipitate Yes Product Pending Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp231

+

methoxy acetic ac id

+

5-methylfurfurylamine

+

4-(trifluoromethyl)benzaldehyde



n-butyl isocyanide

21486238

methylamine Reaction ID UCEXP147-1V2B1 Researcher Mitesh Shah Reaction Type Ugi Solvent methanol Limiting Reactant 0.659 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp147

+

+

+

381



2,3-dihydroxybenzoic acid

methylamine

4,7-dimethoxy-1-naphthaldehyde

tosylmethyl isocyanide

21105839

Reaction ID UCEXP147-3V2B6 Researcher Mitesh Shah Reaction Type Ugi Solvent methanol Limiting Reactant 0.662 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp+147

+

1-pyrenebutyric acid

+

+

methylamine

2-naphthaldehyde



t-butyl isocyanide

21105841

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCEXP151-1V2B10 Researcher Mitesh Shah Reaction Type Ugi Solvent methanol Limiting Reactant 0.694 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp151

+

2,4,6-trihydroxybenzoic acid

+

methylamine

+

3,4-dihydroxybenzaldehyde



tosylmethyl isocyanide

21106049

Reaction ID UCEXP171A/V2B1 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.221 M Precipitate Yes Product Impurities found Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp171

+

2,3-dihydroxybenzoic acid

+

methylamine

+

4,7-dimethoxy-1-naphthaldehyde



tosylmethyl isocyanide

21105839

Reaction ID UCEXP171C/V2B3 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.222 M Precipitate Reactants Insoluble Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp171

+

+

+

382



2,4,6-trihydroxybenzoic acid

methylamine

phenanthrene-9-carboxaldehyde

tosylmethyl isocyanide

21106040

Reaction ID UCEXP171FV2B6 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.222 M Precipitate Yes but reactants initially insoluble Yield - % Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp171

+

1-pyrenebutyric acid

+

+

methylamine

2-naphthaldehyde



t-butyl isocyanide

21105841

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCEXP171HV2B8 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.223 M Precipitate Yes Product No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp171

+

2,4,6-trihydroxybenzoic acid

+

methylamine

+

3,5-dimethoxybenzaldehyde



tosylmethyl isocyanide

21105832

Reaction ID UCEXP171JV2B10 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.225 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp171

+

2,4,6-trihydroxybenzoic acid

+

methylamine

+

3,4-dihydroxybenzaldehyde

Reaction ID UCEXP171KV2B11 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.222 M Precipitate Yes Yield - % Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp171

383



tosylmethyl isocyanide

21106049

+

1-pyrenebutyric acid

+

methylamine

+

4-(dimethylamino)benzaldehyde



t-butyl isocyanide

21105842

Reaction ID UCEXP171LV2B-12 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.22 M Precipitate Reactants Insoluble Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp171

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

+

1-pyrenebutyric acid

+

methylamine

+

phenanthrene-9-carboxaldehyde



t-butyl isocyanide

21106039

Reaction ID UCEXP173B/V2B14 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.223 M Precipitate Yes but reactants initially insoluble Yield - % Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp173

+

1-pyrenebutyric acid

+

+

methylamine

4-methylbenzaldehyde



t-butyl isocyanide

21105844

Reaction ID UCEXP173C/V2B15 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.222 M Precipitate Reactants Insoluble Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp173

+

1-pyrenebutyric acid

+

methylamine

+

4-(trifluoromethyl)benzaldehyde

Reaction ID UCEXP173D/V2B16 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.224 M Precipitate Reactants Insoluble Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp173

384



t-butyl isocyanide

21106044

+

1-pyrenebutyric acid

+

methylamine

+

2-hydroxybenzaldehyde



n-butyl isocyanide

21106048

Reaction ID UCEXP173E/V2B17 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.223 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp173

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

+

Boc-Trp-OH

+

methylamine

+

3,4-dihydroxybenzaldehyde



t-butyl isocyanide

21106045

Reaction ID UCEXP173I/V3B21 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.225 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp173

+

3,4-dihydroxyphenylacetic acid

+

methylamine

+

3-hydroxybenzaldehyde



tosylmethyl isocyanide

21106052

Reaction ID UCEXP173J/V2B22 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.224 M Precipitate Reactants Insoluble Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp173

+

1-pyrenebutyric acid

+

methylamine

+

3,4-dihydroxybenzaldehyde

Reaction ID UCEXP173P/V2B28 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.222 M Precipitate Reactants Insoluble Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp173

385



t-butyl isocyanide

21106038

+

1-pyrenebutyric acid

+

methylamine

+

3-methoxybenzaldehyde



t-butyl isocyanide

21106050

Reaction ID UCEXP174C/V2B34 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.226 M Precipitate Yes but the aldehyde alone is not soluble in methanol Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp174

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

+

5-nitrosalicylic acid

+

methylamine

+

phenanthrene-9-carboxaldehyde



n-butyl isocyanide

21106205

Reaction ID UCEXP174E/V2B36 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.223 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp174

+

Boc-Trp-OH

+

methylamine

+

2-hydroxybenzaldehyde



n-butyl isocyanide

21106201

Reaction ID UCEXP174F/V2B38 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.222 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp174

+

3,4-dihydroxyphenylacetic acid

+

methylamine

+

veratraldehyde

Reaction ID UCEXP174H/V2B40 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.223 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp174

386



tosylmethyl isocyanide

21106200

+

2,4,6-trihydroxybenzoic acid

+

+

methylamine

2-naphthaldehyde



tosylmethyl isocyanide

21106188

Reaction ID UCEXP174L/V2B44 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.224 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp174

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

+

2,4,6-trihydroxybenzoic acid

+

methylamine

+

4-methoxybenzaldehyde



tosylmethyl isocyanide

21106195

Reaction ID UCEXP174N/V2B46 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.223 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp174

+

Boc-Trp-OH

+

methylamine

+

3-hydroxybenzaldehyde



n-butyl isocyanide

21106193

Reaction ID UCEXP174S/V2B52 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.225 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp174

+

5-nitrosalicylic acid

+

methylamine

+

4,7-dimethoxy-1-naphthaldehyde

Reaction ID UCEXP181-057V2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.224 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

387



n-butyl isocyanide

21106203

+

phenylpropynoic acid

+

methylamine

+

2-hydroxybenzaldehyde



tosylmethyl isocyanide

24528098

Reaction ID UCEXP181-059V2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.225 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

+

4-hydroxybenzoic acid

+

+

methylamine

2-methylbenzaldehyde



tosylmethyl isocyanide

24528099

Reaction ID UCEXP181-062V2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.223 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

+

4-hydroxybenzoic acid

+

methylamine

+

3,5-dimethoxybenzaldehyde



tosylmethyl isocyanide

24528101

Reaction ID UCEXP181-066V2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.225 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

+

2,4,6-trihydroxybenzoic acid

+

methylamine

+

3-hydroxybenzaldehyde

Reaction ID UCEXP181-068V2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.224 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

388



tosylmethyl isocyanide

24528105

+

3,4-dihydroxyphenylacetic acid

+

+

methylamine

o-vanillin



tosylmethyl isocyanide

24528107

Reaction ID UCEXP181-072V2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.224 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

+

2,6-dihydroxybenzoic acid

+

methylamine

+

4-(trifluoromethyl)benzaldehyde



tosylmethyl isocyanide

21106207

Reaction ID UCEXP181-073V2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.222 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

+

Boc-Trp-OH

+

+

methylamine

benzaldehyde



t-butyl isocyanide

24528109

Reaction ID UCEXP181-086V2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.225 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

+

4-hydroxybenzoic acid

+

methylamine

+

3-hydroxybenzaldehyde

Reaction ID UCEXP181-087V2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.222 M Precipitate Reactants Insoluble Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

389



tosylmethyl isocyanide

24528121

+

1-pyrenebutyric acid

+

methylamine

+

2,4-dimethylbenzaldehyde



t-butyl isocyanide

21106206

Reaction ID UCEXP181-090V2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.226 M Precipitate Reactants Insoluble Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

+

4-nitrobenzoic acid

+

methylamine

+

3,4-dihydroxybenzaldehyde



tosylmethyl isocyanide

24528123

Reaction ID UCEXP181-096V2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.224 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

+

4-hydroxybenzoic acid

+

methylamine

+

3-methoxybenzaldehyde



tosylmethyl isocyanide

24528127

Reaction ID UCEXP181-098V2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.226 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

+

2,3-dihydroxybenzoic acid

+

methylamine

+

4-hydroxybenzaldehyde

Reaction ID UCEXP181-100V2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.225 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

390



tosylmethyl isocyanide

24528129

+

D-(−)-Quinic acid

+

+

methylamine

4-chlorobenzaldehyde



tosylmethyl isocyanide

24528131

Reaction ID UCEXP181-101V2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.221 M Precipitate Reactants Insoluble Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

+

2,4,6-trihydroxybenzoic acid

+

methylamine

+

4,7-dimethoxy-1-naphthaldehyde



tosylmethyl isocyanide

24528132

Reaction ID UCEXP181-103V2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.226 M Precipitate no and aldehyde alone not solube Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

+

mandelic acid

+

methylamine

+

phenanthrene-9-carboxaldehyde



n-butyl isocyanide

24528133

Reaction ID UCEXP181-104V2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.223 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

+

D-(−)-Quinic acid

+

methylamine

+

4-(dimethylamino)benzaldehyde

Reaction ID UCEXP181-106V2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.224 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

391



tosylmethyl isocyanide

24528134

+

4-hydroxybenzoic acid

+

+

methylamine

2-naphthaldehyde



tosylmethyl isocyanide

24528136

Reaction ID UCEXP181-108V2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.223 M Precipitate Yes Product No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

+

D-(−)-Quinic acid

+

+

methylamine

2-naphthaldehyde



tosylmethyl isocyanide

24528138

Reaction ID UCEXP181-111V2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.226 M Precipitate Reactants Insoluble Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

+

2,4,6-trihydroxybenzoic acid

+

methylamine

+

phenanthrene-9-carboxaldehyde



t-butyl isocyanide

24528534

Reaction ID UCEXP181-112V2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.224 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

+

2,3-dihydroxybenzoic acid

+

methylamine

+

4-methoxybenzaldehyde

Reaction ID UCEXP181-116V2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.225 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

392



tosylmethyl isocyanide

24528141

+

2,3-dihydroxybenzoic acid

+

+

methylamine

4-chlorobenzaldehyde



tosylmethyl isocyanide

24528145

Reaction ID UCEXP181-118V2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.224 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

+

3,4-dihydroxyphenylacetic acid

+

+

5-bromo-2thiophenecarboxaldehyde

methylamine



tosylmethyl isocyanide

24528147

Reaction ID UCEXP181-119V2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.226 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

+

diphenylacetic acid

+

methylamine

+

3,4-dihydroxybenzaldehyde



n-butyl isocyanide

24528148

Reaction ID UCEXP181-120V2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.222 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

+

2,4,6-trihydroxybenzoic acid

+

methylamine

+

3,5Bis(trifluoromethyl)benzaldehyde

Reaction ID UCEXP215C Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 0.662 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp215

393



tosylmethyl isocyanide

24528149

+

1-pyrenebutyric acid

+

+

methylamine

2-naphthaldehyde



t-butyl isocyanide

21105841

Reaction ID UCEXP215D Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 0.66 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp215

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

+

1-pyrenebutyric acid

+

methylamine

+

4-(dimethylamino)benzaldehyde



t-butyl isocyanide

21105842

Reaction ID UCEXP215E Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 0.715 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp215

+

4-chlorophenylacetic acid

+

+

methylamine

4-methylbenzaldehyde



t-butyl isocyanide

24528155

Reaction ID UCEXP222-5 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 0.898 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp222

+

1-pyrenebutyric acid

+

methylamine

+

4-(dimethylamino)benzaldehyde

Reaction ID UCEXP222-6 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 0.898 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp222

394



t-butyl isocyanide

21105842

+

1-pyrenebutyric acid

+

+

methylamine

4-methylbenzaldehyde



t-butyl isocyanide

21105844

Reaction ID UCEXP228-7 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 0.67 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp228

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

+

1-pyrenebutyric acid

+

+

methylamine

4-methylbenzaldehyde



t-butyl isocyanide

21105844

Reaction ID UCEXP231-3 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 0.75 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp231

+

1-pyrenebutyric acid

+

+

methylamine

2-naphthaldehyde



t-butyl isocyanide

21105841

Reaction ID UCExp236-10 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.888 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp236

+

methacrylic acid

+

methylamine

+

4-(trifluoromethyl)benzaldehyde

Reaction ID UCExp236-14 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.856 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp236

395



n-butyl isocyanide

24528283

+

3,3'-dichloropivalic acid

+

+

5-bromo-2thiophenecarboxaldehyde

methylamine



t-butyl isocyanide

24528287

Reaction ID UCExp236-18 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.858 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp236

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

+

3,3'-dichloropivalic acid

+

methylamine

+

2,4-dimethylbenzaldehyde



t-butyl isocyanide

24528291

Reaction ID UCExp236-19 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.927 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp236

+

formic acid

+

methylamine

+

4-(trifluoromethyl)benzaldehyde



n-butyl isocyanide

24528292

Reaction ID UCExp238-10 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.825 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp238

+

crotonic acid

+

methylamine

+

phenanthrene-9-carboxaldehyde

Reaction ID UCExp238-22 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.867 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp238

396



cyclohexylisocyanide

24528312

+

crotonic acid

+

methylamine

+

phenanthrene-9-carboxaldehyde



t-butyl isocyanide

24528322

Reaction ID UCExp238-34 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.648 M Precipitate Yes Product Awaiting Characterization Comments Reference http://usefulchem.wikispaces.com/Exp238

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

+

Boc-Gly-OH

+

methylamine

+

phenanthrene-9-carboxaldehyde



cyclohexylisocyanide

24528334

Reaction ID UCExp241-01 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.502 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp241

+

3,4methylenedioxyphenylacetic acid

+

methylamine

+

4-methoxybenzaldehyde



benzyl isocyanide

24534407

Reaction ID UCExp241-02 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.502 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp241

+

3,4methylenedioxyphenylacetic acid

+

methylamine

+

m-anisaldehyde

Reaction ID UCExp241-03 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.512 M Precipitate No

397



benzyl isocyanide

24534408

Comments Reference

http://usefulchem.wikispaces.com/Exp241

+

3,4methylenedioxyphenylacetic acid

+

methylamine

+

2-furaldehyde



benzyl isocyanide

24534403

Reaction ID UCExp241-04

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.525 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp241

+

3,4methylenedioxyphenylacetic acid

+

methylamine

+

veratraldehyde



n-butyl isocyanide

24528355

Reaction ID UCExp241-05 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.525 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp241

+

3,4methylenedioxyphenylacetic acid

+

methylamine

+

veratraldehyde



n-butyl isocyanide

24528355

Reaction ID UCExp241-06 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.523 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp241

+

3,4methylenedioxyphenylacetic acid

+

methylamine

+

veratraldehyde

Reaction ID UCExp241-07

398



t-butyl isocyanide

24528356

Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.523 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp241

+

3,4methylenedioxyphenylacetic acid

+

methylamine

+

veratraldehyde



t-butyl isocyanide

24528356

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCExp241-08 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.52 M Precipitate YES Yield - % Comments Reference http://usefulchem.wikispaces.com/Exp241

+

3,4methylenedioxyphenylacetic acid

+

methylamine

+

veratraldehyde



cyclohexylisocyanide

21782465

Reaction ID UCExp241-09 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.564 M Precipitate YES Yield - % Comments Reference http://usefulchem.wikispaces.com/Exp241

+

3,4methylenedioxyphenylacetic acid

+

methylamine

+

veratraldehyde



cyclohexylisocyanide

21782465

Reaction ID UCExp241-10 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.548 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp241

+

+

+

399



3,4methylenedioxyphenylacetic acid

methylamine

1,1,3,3tetramethylbutyl isocyanide

veratraldehyde

24528357

Reaction ID UCExp241-11

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.548 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp241

+

3,4methylenedioxyphenylacetic acid

+

methylamine

+



1,1,3,3tetramethylbutyl isocyanide

veratraldehyde

24528357

Reaction ID UCExp241-12 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.563 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp241

+

3,4methylenedioxyphenylacetic acid

+

methylamine

+

veratraldehyde



1-pentyl isocyanide

24528358

Reaction ID UCExp241-13 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.563 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp241

+

3,4methylenedioxyphenylacetic acid

+

methylamine

+

veratraldehyde

Reaction ID UCExp241-14 Researcher Reaction Type

Khalid Mirza Ugi

400



1-pentyl isocyanide

24528358

Solvent methanol Limiting Reactant 0.565 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp241

+

3,4methylenedioxyphenylacetic acid

+

+

methylamine

veratraldehyde



benzyl isocyanide

24528359

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCExp241-15 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.565 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp241

+

3,4methylenedioxyphenylacetic acid

+

+

methylamine

veratraldehyde



benzyl isocyanide

24528359

Reaction ID UCExp241-16 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.565 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp241

+

3,4methylenedioxyphenylacetic acid

+

+

methylamine

veratraldehyde



benzyl isocyanide

24528359

Reaction ID UCExp241-17 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.577 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp241

+

3,4methylenedioxyphenylacetic acid

+

methylamine

+

5-bromo-2thiophenecarboxaldehyde

401



t-butyl isocyanide

24528360

Reaction ID UCExp241-18 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.571 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp241

+

3,4methylenedioxyphenylacetic acid

+

methylamine

+

2,4-dimethylbenzaldehyde



t-butyl isocyanide

24528361

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCExp241-21 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.576 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp241

+

3,4methylenedioxyphenylacetic acid

+

methylamine

+

4-methylbenzaldehyde



t-butyl isocyanide

24528362

Reaction ID UCExp241-22 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.578 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp241

+

3,4methylenedioxyphenylacetic acid

+

methylamine

+

o-tolualdehyde



t-butyl isocyanide

24528363

Reaction ID UCExp241-23 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.559 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp241

+

+

+

402



3,4methylenedioxyphenylacetic acid

5-bromo-2thiophenecarboxaldehyde

methylamine

n-butyl isocyanide

24528364

Reaction ID UCExp241-26

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.573 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp241

+

+

3,4methylenedioxyphenylacetic acid

methylamine

+

2,4-dimethylbenzaldehyde



n-butyl isocyanide

24528365

n-butyl isocyanide Reaction ID UCEXP130-1 Researcher Rikesh Parikh Reaction Type Ugi Solvent methanol Limiting Reactant 0.751 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp130

+

formic acid

+

5-methylfurfurylamine

+

2-naphthaldehyde



n-butyl isocyanide

21106081

Reaction ID UCEXP130-5 Researcher Rikesh Parikh Reaction Type Ugi Solvent methanol Limiting Reactant 0.734 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp130

+

formic acid

+

furfurylamine

+

2-naphthaldehyde

Reaction ID UCEXP131-1 Researcher Reaction Type Solvent

Rikesh Parikh Ugi methanol

403



n-butyl isocyanide

21106079

Limiting Reactant 0.608 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp131

+

Boc-Trp-OH

+

furfurylamine

+

veratraldehyde



n-butyl isocyanide

21106067

Reaction ID UCEXP131-6

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Researcher Rikesh Parikh Reaction Type Ugi Solvent methanol Limiting Reactant 0.625 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp131

+

Boc-Trp-OH

+

1-hexylamine

+

o-vanillin



n-butyl isocyanide

21106063

Reaction ID UCEXP131-8 Researcher Rikesh Parikh Reaction Type Ugi Solvent methanol Limiting Reactant 0.618 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp131

+

Boc-Trp-OH

+

1-heptylamine

+

o-vanillin



n-butyl isocyanide

21106065

Reaction ID UCEXP134-1 Researcher Rikesh Parikh Reaction Type Ugi Solvent methanol Limiting Reactant 0.645 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp134

+

Boc-Trp-OH

+

1-propylamine

+

o-vanillin

Reaction ID UCEXP134-3 Researcher Rikesh Parikh Reaction Type Ugi Solvent methanol Limiting Reactant 0.612 M Precipitate No

404



n-butyl isocyanide

21106070

Comments Reference

Protocol from Explan005 followed http://usefulchem.wikispaces.com/Exp134

+

Boc-Trp-OH

+

+

1-octylamine

o-vanillin



n-butyl isocyanide

21106072

Reaction ID UCEXP159C-V1B18

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Researcher Emily Messner Reaction Type Ugi Solvent methanol Limiting Reactant 0.661 M Precipitate Yes but the aldehyde alone is not soluble in methanol Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp159

+

4-chlorophenylacetic acid

+

benzylamine

+

phenanthrene-9-carboxaldehyde



n-butyl isocyanide

21106077

Reaction ID UCEXP160C-V1B19 Researcher Emily Messner Reaction Type Ugi Solvent methanol Limiting Reactant 0.388 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp160

+

3,4-dihydroxyphenylacetic acid

+

furfurylamine

+

phenanthrene-9-carboxaldehyde



n-butyl isocyanide

21105579

Reaction ID UCEXP164 Researcher Emily Messner/Shannon Oseback Reaction Type Ugi Solvent methanol Limiting Reactant 0.287 M Precipitate Reactants Insoluble Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp164

+

phenylacetic acid

+

aniline

+

phenanthrene-9-carboxaldehyde

Reaction ID UCEXP167A-V1B12 Researcher Tim Bohinsky Reaction Type Ugi Solvent methanol Limiting Reactant 0.403 M Precipitate Reactants Insoluble Comments Protocol from Explan005 followed

405



n-butyl isocyanide

21106183

Reference

http://usefulchem.wikispaces.com/Exp167

+

3,4methylenedioxyphenylacetic acid

+

1-propylamine

+

phenanthrene-9-carboxaldehyde



n-butyl isocyanide

21105597

Reaction ID UCEXP173D/V2B16

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.224 M Precipitate Reactants Insoluble Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp173

+

1-pyrenebutyric acid

+

methylamine

+

2-hydroxybenzaldehyde



n-butyl isocyanide

21106048

Reaction ID UCEXP173G/V2B19 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.223 M Precipitate Yes Yield - % Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp173

+

phenylpropynoic acid

+

benzylamine

+

3,5-dimethoxybenzaldehyde



n-butyl isocyanide

21105845

Reaction ID UCEXP174C/V2B34 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.226 M Precipitate Yes but the aldehyde alone is not soluble in methanol Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp174

+

5-nitrosalicylic acid

+

methylamine

+

phenanthrene-9-carboxaldehyde

Reaction ID UCEXP174E/V2B36 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.223 M Precipitate No

406



n-butyl isocyanide

21106205

Comments Reference

Protocol from Explan005 followed http://usefulchem.wikispaces.com/Exp174

+

Boc-Trp-OH

+

methylamine

+

2-hydroxybenzaldehyde



n-butyl isocyanide

21106201

Reaction ID UCEXP174N/V2B46

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.223 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp174

+

Boc-Trp-OH

+

methylamine

+

3-hydroxybenzaldehyde



n-butyl isocyanide

21106193

Reaction ID UCEXP174S/V2B52 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.225 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp174

+

5-nitrosalicylic acid

+

methylamine

+

4,7-dimethoxy-1-naphthaldehyde



n-butyl isocyanide

21106203

Reaction ID UCEXP175D Researcher Khalid Mirza/ Emily Messner Reaction Type Ugi Solvent methanol Limiting Reactant 0.398 M Precipitate Yes but the aldehyde alone is not soluble in methanol Yield - % Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp175

+

4-chlorophenylacetic acid

+

benzylamine

+

phenanthrene-9-carboxaldehyde

Reaction ID UCEXP176C Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant - M Precipitate Yes Yield 62 %

407



n-butyl isocyanide

21106077

Comments Reference

aldehyde not soluble until all reactants added http://usefulchem.wikispaces.com/Exp176

+

phenylacetic acid

+

furfurylamine

+

phenanthrene-9-carboxaldehyde



n-butyl isocyanide

21105594

Reaction ID UCEXP177

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Researcher Shannon Oseback Reaction Type Ugi Solvent methanol Limiting Reactant 0.224 M Precipitate Reactants Insoluble Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp177

+

phenylacetic acid

+

1-propylamine

+

phenanthrene-9-carboxaldehyde



n-butyl isocyanide

21105831

Reaction ID UCEXP178 Researcher Shannon Oseback Reaction Type Ugi Solvent methanol Limiting Reactant 0.388 M Precipitate Yes but the aldehyde alone is not soluble in methanol Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp178

+

phenylacetic acid

+

furfurylamine

+

phenanthrene-9-carboxaldehyde



n-butyl isocyanide

21105594

Reaction ID UCEXP180 Researcher Shannon Oseback Reaction Type Ugi Solvent methanol Limiting Reactant 0.403 M Precipitate no and aldehyde alone not solube Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp180

+

acetic acid

+

1-heptylamine

+

phenanthrene-9-carboxaldehyde

Reaction ID UCEXP181-055V2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.223 M Precipitate no and aldehyde alone not solube Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

408



n-butyl isocyanide

21105834

+

2,6-dihydroxybenzoic acid

+

5-methylfurfurylamine

+

phenanthrene-9-carboxaldehyde



n-butyl isocyanide

24528096

Reaction ID UCEXP181-056V2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.219 M Precipitate Reactants Insoluble Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

+

2,4,6-trihydroxybenzoic acid

+

furfurylamine

+

phenanthrene-9-carboxaldehyde



n-butyl isocyanide

24528097

Reaction ID UCEXP181-070V2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.22 M Precipitate Reactants Insoluble Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

+

1-pyrenebutyric acid

+

+

3-chloroaniline

2-methylbenzaldehyde



n-butyl isocyanide

24528530

Reaction ID UCEXP181-075V2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.218 M Precipitate no and aldehyde alone not solube Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

+

mandelic acid

+

furfurylamine

+

phenanthrene-9-carboxaldehyde

Reaction ID UCEXP181-076V2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.224 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

409



n-butyl isocyanide

24528111

+

diphenylacetic acid

+

1-propylamine

+

3,4-dihydroxybenzaldehyde



n-butyl isocyanide

24528112

Reaction ID UCEXP181-077V2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.225 M Precipitate Reactants Insoluble Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

+

2,4,6-trihydroxybenzoic acid

+

5-methylfurfurylamine

+

3-methoxybenzaldehyde



n-butyl isocyanide

24528113

Reaction ID UCEXP181-083V2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.221 M Precipitate Reactants Insoluble Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

+

1-pyrenebutyric acid

+

+

aniline

benzaldehyde



n-butyl isocyanide

21106208

Reaction ID UCEXP181-084V2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.225 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

+

mandelic acid

+

benzylamine

+

3-methoxybenzaldehyde

Reaction ID UCEXP181-088V2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.222 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

410



n-butyl isocyanide

24528119

+

diphenylacetic acid

+

5-methylfurfurylamine

+

3,4-dihydroxybenzaldehyde



n-butyl isocyanide

24528532

Reaction ID UCEXP181-103V2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.226 M Precipitate no and aldehyde alone not solube Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

+

+

mandelic acid

methylamine

+

phenanthrene-9-carboxaldehyde



n-butyl isocyanide

24528133

Reaction ID UCEXP181-114V2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.223 M Precipitate Reactants Insoluble Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

+

2,4,6-trihydroxybenzoic acid

+

5-methylfurfurylamine

+

phenanthrene-9-carboxaldehyde



n-butyl isocyanide

24528143

Reaction ID UCEXP181-119V2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.226 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

+

diphenylacetic acid

+

methylamine

+

3,4-dihydroxybenzaldehyde

Reaction ID UCEXP182 Researcher Emily Messner Reaction Type Ugi Solvent methanol Limiting Reactant 0.398 M Precipitate Reactants Insoluble Comments Reference http://usefulchem.wikispaces.com/Exp182

411



n-butyl isocyanide

24528148

+

furoic acid

+

1-heptylamine

+

phenanthrene-9-carboxaldehyde



n-butyl isocyanide

21168529

Reaction ID UCEXP215F Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 0.661 M Precipitate Yes but not at room temperature Yield - % Comments Reference http://usefulchem.wikispaces.com/Exp215

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

+

4-chlorophenylacetic acid

+

benzylamine

+

phenanthrene-9-carboxaldehyde



n-butyl isocyanide

21106077

Reaction ID UCEXP217-1 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 0.384 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp217

+

4-chlorophenylacetic acid

+

benzylamine

+

phenanthrene-9-carboxaldehyde



n-butyl isocyanide

21106077

Reaction ID UCEXP217-5 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 0.384 M Precipitate Yes Product Pending Comments Reference http://usefulchem.wikispaces.com/Exp217

+

Boc-Gly-OH

+

furfurylamine

+

phenanthrene-9-carboxaldehyde



n-butyl isocyanide

Reaction ID UCEXP225-2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.905 M Precipitate Yes Product Pending Comments 0.5 mmol of isocyanide was added to 500uL of a 2M solution of aldehyde; amine and acid

412

21105594

Reference

http://usefulchem.wikispaces.com/Exp225

+

Boc-Gly-OH

+

+

furfurylamine

piperonal



n-butyl isocyanide

24528158

Reaction ID UCEXP226-2 Researcher David Bulger Reaction Type Ugi Solvent THF Limiting Reactant 0.525 M Precipitate No Comments 0.5 mmol of isocyanide was added to 900uL of a 0.55M solution of aldehyde; amine and acid Reference http://usefulchem.wikispaces.com/Exp226

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

+

1-pyrenebutyric acid

+

+

5-methylfurfurylamine

benzaldehyde



n-butyl isocyanide

24528166

Reaction ID UCEXP227-2 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 0.453 M Precipitate No Comments 0.5 mmol of isocyanide was added to 500uL of a 0.5M solution of aldehyde; amine and acid Reference http://usefulchem.wikispaces.com/Exp227

+

1-pyrenebutyric acid

+

+

furfurylamine

piperonal



n-butyl isocyanide

24528174

Reaction ID UCEXP228-2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.265 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp228

+

Boc-Trp-OH

+

octadecylamine

+

3-hydroxybenzaldehyde

Reaction ID UCEXP228-3 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.551 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp228

413



n-butyl isocyanide

24528182

+

Boc-Trp-OH

+

octadecylamine

+

2,4-dimethylbenzaldehyde



n-butyl isocyanide

24534188

Reaction ID UCEXP228-4 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.634 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp228

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

+

Boc-Trp-OH

+

+

octadecylamine

benzaldehyde



n-butyl isocyanide

24534192

Reaction ID UCEXP228-6 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.627 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp228

+

Boc-Trp-OH

+

5-methylfurfurylamine

+

4-(trifluoromethyl)benzaldehyde



n-butyl isocyanide

24534190

Reaction ID UCEXP229-2 Researcher David Bulger Reaction Type Ugi Solvent methanol Limiting Reactant 0.667 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp229

+

Boc-Trp-OH

+

1-hexylamine

+

benzaldehyde

Reaction ID UCEXP231-4 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 2 M Precipitate Yes Product Pending Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp231

414



n-butyl isocyanide

24528183

+

methoxy acetic ac id

+

5-methylfurfurylamine

+

4-(trifluoromethyl)benzaldehyde



n-butyl isocyanide

21486238

Reaction ID UCEXP231-7 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 0.667 M Precipitate Yes Product Pending Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp231

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

+

1-pyrenebutyric acid

+

furfurylamine

+

2-furaldehyde



n-butyl isocyanide

24528187

Reaction ID UCEXP232-02 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.098 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde



n-butyl isocyanide

24528189

Reaction ID UCEXP232-07 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.082 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+

4-methylbenzaldehyde

Reaction ID UCEXP232-12 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.028 M Precipitate Yes Product Pending Comments Reference http://usefulchem.wikispaces.com/Exp232

415



n-butyl isocyanide

24528194

+

Boc-Gly-OH

+

furfurylamine

+

4-(trifluoromethyl)benzaldehyde



n-butyl isocyanide

24528199

Reaction ID UCEXP232-17 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.365 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

+

Boc-Gly-OH

+

+

furfurylamine

crotonaldehyde



n-butyl isocyanide

24528203

Reaction ID UCEXP232-22 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.007 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

+

furfurylamine

diphenylacetaldehyde



n-butyl isocyanide

24528208

Reaction ID UCEXP232-27 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.092 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+

cyclohexancarboxaldehyde

Reaction ID UCEXP232-32 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.11 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

416



n-butyl isocyanide

24528213

+

Boc-Gly-OH

+

+

furfurylamine

2-furaldehyde



n-butyl isocyanide

24528218

Reaction ID UCEXP232-37 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.081 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

+

Boc-Gly-OH

+

furfurylamine

+

2-hydroxybenzaldehyde



n-butyl isocyanide

24528223

Reaction ID UCEXP232-42 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.083 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

+

furfurylamine

o-tolualdehyde



n-butyl isocyanide

24528228

Reaction ID UCEXP232-47 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.066 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+

4-methoxybenzaldehyde

Reaction ID UCEXP232-52 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.105 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

417



n-butyl isocyanide

24528233

+

Boc-Gly-OH

+

+

furfurylamine

hexanaldehyde



n-butyl isocyanide

24528238

Reaction ID UCEXP232-57 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.109 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

+

Boc-Gly-OH

+

+

furfurylamine

trans-2-hexenal



n-butyl isocyanide

24528243

Reaction ID UCEXP232-62 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.069 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+

2-phenylpropionaldehyde



n-butyl isocyanide

24534417

Reaction ID UCEXP232-67 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.068 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+

m-anisaldehyde

Reaction ID UCEXP232-72 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.105 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

418



n-butyl isocyanide

24528252

+

Boc-Gly-OH

+

+

furfurylamine

2-ethylbutyraldehyde



n-butyl isocyanide

24528257

Reaction ID UCExp236-01 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.614 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp236

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

+

3,3'-dichloropivalic acid

+

t-butylamine

+

4-(trifluoromethyl)benzaldehyde



n-butyl isocyanide

24528275

Reaction ID UCExp236-02 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.614 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp236

+

3,3'-dichloropivalic acid

+

3-chloroaniline

+

4-(trifluoromethyl)benzaldehyde



n-butyl isocyanide

24528276

Reaction ID UCExp236-03 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.614 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp236

+

3,3'-dichloropivalic acid

+

benzylamine

+

4-(trifluoromethyl)benzaldehyde

Reaction ID UCExp236-10 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.888 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp236

419



n-butyl isocyanide

24528277

+

methacrylic acid

+

methylamine

+

4-(trifluoromethyl)benzaldehyde



n-butyl isocyanide

24528283

Reaction ID UCExp236-13 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.614 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp236

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

+

3,3'-dichloropivalic acid

+

1-propylamine

+

4-(trifluoromethyl)benzaldehyde



n-butyl isocyanide

24528286

Reaction ID UCExp236-17 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.614 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp236

+

+

3,3'-dichloropivalic acid

aniline

+

4-(trifluoromethyl)benzaldehyde



n-butyl isocyanide

24528290

Reaction ID UCExp236-19 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.927 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp236

+

formic acid

+

methylamine

+

4-(trifluoromethyl)benzaldehyde

Reaction ID UCExp236-20 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.631 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp236

420



n-butyl isocyanide

24528292

+

methacrylic acid

+

t-butylamine

+

4-(trifluoromethyl)benzaldehyde



n-butyl isocyanide

24528293

Reaction ID UCExp236-23 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.631 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp236

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

+

methacrylic acid

+

3-chloroaniline

+

4-(trifluoromethyl)benzaldehyde



n-butyl isocyanide

24528296

Reaction ID UCExp236-24 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.63 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp236

+

methacrylic acid

+

benzylamine

+

4-(trifluoromethyl)benzaldehyde



n-butyl isocyanide

24528297

Reaction ID UCExp237-01 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.778 M Precipitate Yes Product Awaiting Characterization Comments Reference http://usefulchem.wikispaces.com/Exp237

+

phenylacetic acid

+

furfurylamine

+

phenanthrene-9-carboxaldehyde

Reaction ID UCExp237-02 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 0.746 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp237

421



n-butyl isocyanide

21105594

+

+

phenylacetic acid

furfurylamine

+

phenanthrene-9-carboxaldehyde



n-butyl isocyanide

21105594

Reaction ID UCExp240-01 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.607 M Precipitate Yes but after 48h Comments Reference http://usefulchem.wikispaces.com/Exp240

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

+

+

phenylacetic acid

furfurylamine

+

phenanthrene-9-carboxaldehyde



n-butyl isocyanide

21105594

Reaction ID UCExp240-07 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.839 M Precipitate Yes Yield - % Comments Reference http://usefulchem.wikispaces.com/Exp240

+

phenylacetic acid

+

5-methylfurfurylamine

+

phenanthrene-9-carboxaldehyde



n-butyl isocyanide

21782451

Reaction ID UCExp241-04 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.525 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp241

+

3,4methylenedioxyphenylacetic acid

+

methylamine

+

veratraldehyde

Reaction ID UCExp241-05 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.525 M Precipitate No Comments -

422



n-butyl isocyanide

24528355

Reference

http://usefulchem.wikispaces.com/Exp241

+

3,4methylenedioxyphenylacetic acid

+

+

methylamine

veratraldehyde



n-butyl isocyanide

24528355

Reaction ID UCExp241-23

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.559 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp241

+

3,4methylenedioxyphenylacetic acid

+

+

5-bromo-2thiophenecarboxaldehyde

methylamine



n-butyl isocyanide

24528364

Reaction ID UCExp241-26 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.573 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp241

+

3,4methylenedioxyphenylacetic acid

+

methylamine

+

2,4-dimethylbenzaldehyde



n-butyl isocyanide

24528365

Reaction ID UCExp241-29 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.729 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp241

+

3,4methylenedioxyphenylacetic acid

+

1-hexylamine

+

4-(trifluoromethyl)benzaldehyde

Reaction ID UCExp241-31 Researcher

Khalid Mirza

423



n-butyl isocyanide

24528366

Reaction Type Ugi Solvent methanol Limiting Reactant 0.743 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp241

+

3,4methylenedioxyphenylacetic acid

+

2-chloroaniline

+

4-(trifluoromethyl)benzaldehyde



n-butyl isocyanide

24528368

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCExp241-32 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.751 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp241

+

+

3,4methylenedioxyphenylacetic acid

aniline

+

4-(trifluoromethyl)benzaldehyde



n-butyl isocyanide

24528369

Reaction ID UCExp241-44 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.72 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp241

+

3,4methylenedioxyphenylacetic acid

+

1-heptylamine

+

4-(trifluoromethyl)benzaldehyde



n-butyl isocyanide

24528377

Reaction ID UCExp242-1 Researcher Marshall Moritz Reaction Type Ugi Solvent benzene Limiting Reactant 0.435 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp242

+

phenylacetic acid

+

furfurylamine

+

phenanthrene-9-carboxaldehyde

424



n-butyl isocyanide

21105594

Reaction ID UCExp242-6 Researcher Marshall Moritz Reaction Type Ugi Solvent benzene Limiting Reactant 0.431 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp242

+

phenylacetic acid

+

5-methylfurfurylamine

+

phenanthrene-9-carboxaldehyde



n-butyl isocyanide

24528387

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCExp245-01 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.509 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp245

+

3,4methylenedioxyphenylacetic acid

+

furfurylamine

+

piperonal



n-butyl isocyanide

24528391

Reaction ID UCExp245-02 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.718 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp245

+

3,4methylenedioxyphenylacetic acid

+

furfurylamine

+

piperonal



n-butyl isocyanide

24528391

Reaction ID UCExp245-03 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.504 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp245

+

+

+

425



3,4methylenedioxyphenylacetic acid

5-methylfurfurylamine

piperonal

n-butyl isocyanide

24528392

Reaction ID UCExp245-04 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.706 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp245

+

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

3,4methylenedioxyphenylacetic acid

+

5-methylfurfurylamine

+

piperonal



n-butyl isocyanide

24528392

Reaction ID UCExp245-17 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.502 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp245

+

cbz-proline

+

furfurylamine

+

piperonal



n-butyl isocyanide

24528399

Reaction ID UCExp245-18 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.12 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp245

+

cbz-proline

+

furfurylamine

+

piperonal



n-butyl isocyanide

24528399

Reaction ID UCExp245-19 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.496 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp245

+

+

+

426



cbz-proline

5-methylfurfurylamine

piperonal

n-butyl isocyanide

24528400

Reaction ID UCExp245-20 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.092 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp245

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

+

cbz-proline

+

5-methylfurfurylamine

+

piperonal



n-butyl isocyanide

24528400

Reaction ID UCExp245-37 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.509 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp245

+

3,4methylenedioxyphenylacetic acid

+

furfurylamine

+

piperonal



n-butyl isocyanide

24528409

Reaction ID UCExp245-38 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.718 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp245

+

3,4methylenedioxyphenylacetic acid

+

furfurylamine

+

piperonal

Reaction ID UCExp245-39 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.504 M Precipitate No Comments -

427



n-butyl isocyanide

24528409

Reference

http://usefulchem.wikispaces.com/Exp245

+

3,4methylenedioxyphenylacetic acid

+

+

5-methylfurfurylamine

piperonal



n-butyl isocyanide

24528410

Reaction ID UCExp245-40

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.706 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp245

+

3,4methylenedioxyphenylacetic acid

+

+

5-methylfurfurylamine

piperonal



n-butyl isocyanide

24528410

Reaction ID UCExp252-01 Researcher Khalid Mirza Reaction Type Ugi Solvent benzene Limiting Reactant 0.403 M Precipitate Yes Yield - % Comments Reference http://usefulchem.wikispaces.com/Exp252

+

phenylacetic acid

+

furfurylamine

+

phenanthrene-9-carboxaldehyde



n-butyl isocyanide

21105594

Reaction ID UCExp253-01 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.53 M Precipitate Yes Yield 42.6 % Comments Reference http://usefulchem.wikispaces.com/Exp253

+

phenylacetic acid

+

furfurylamine

+

phenanthrene-9-carboxaldehyde

Reaction ID UCExp254-01 Researcher Reaction Type Solvent

Khalid Mirza Ugi methanol

428



n-butyl isocyanide

21105594

Limiting Reactant 0.08 M Precipitate Yes Yield - % Comments Reference http://usefulchem.wikispaces.com/Exp254

+

phenylacetic acid

+

furfurylamine

+

phenanthrene-9-carboxaldehyde



n-butyl isocyanide

21105594

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCExp255-01 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.4 M Precipitate Yes Yield 65.8 % Comments Reference http://usefulchem.wikispaces.com/Exp255

+

phenylacetic acid

+

furfurylamine

+

phenanthrene-9-carboxaldehyde



n-butyl isocyanide

21105594

Reaction ID UCExp255-02 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.4 M Precipitate Yes Yield 65.1 % Comments Reference http://usefulchem.wikispaces.com/Exp255

+

phenylacetic acid

+

furfurylamine

+

phenanthrene-9-carboxaldehyde



n-butyl isocyanide

21105594

Reaction ID UCExp255-03 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.4 M Precipitate Yes Yield 66.4 % Comments Reference http://usefulchem.wikispaces.com/Exp255

+

phenylacetic acid

+

furfurylamine

+

phenanthrene-9-carboxaldehyde

429



n-butyl isocyanide

21105594

Reaction ID UCExp255-04 Researcher Khalid Mirza Reaction Type Ugi Solvent benzene Limiting Reactant 0.4 M Precipitate Yes Yield 29.7 % Comments Reference http://usefulchem.wikispaces.com/Exp255

+

phenylacetic acid

+

furfurylamine

+

phenanthrene-9-carboxaldehyde



n-butyl isocyanide

21105594

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCExp255-05 Researcher Khalid Mirza Reaction Type Ugi Solvent benzene Limiting Reactant 0.4 M Precipitate Yes Yield 30.5 % Comments Reference http://usefulchem.wikispaces.com/Exp255

+

phenylacetic acid

+

furfurylamine

+

phenanthrene-9-carboxaldehyde



n-butyl isocyanide

21105594

Reaction ID UCExp255-06 Researcher Khalid Mirza Reaction Type Ugi Solvent benzene Limiting Reactant 0.4 M Precipitate Yes Yield 28.9 % Comments Reference http://usefulchem.wikispaces.com/Exp255

+

phenylacetic acid

+

furfurylamine

+

phenanthrene-9-carboxaldehyde



n-butyl isocyanide

21105594

Reaction ID UCExp256-01 Researcher Khalid Mirza Reaction Type Ugi Solvent benzene Limiting Reactant 0.4 M Precipitate Yes Yield 17 % Comments Reference http://usefulchem.wikispaces.com/Exp256

+

+

+

430



phenylacetic acid

furfurylamine

phenanthrene-9-carboxaldehyde

n-butyl isocyanide

21105594

Reaction ID UCExp257-01 Researcher Khalid Mirza Reaction Type Ugi Solvent ethyl acetate Limiting Reactant 0.37 M Precipitate Yes Yield 24 % Comments Reference http://usefulchem.wikispaces.com/Exp257

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

+

phenylacetic acid

+

furfurylamine

+

phenanthrene-9-carboxaldehyde



n-butyl isocyanide

21105594

o-tolualdehyde Reaction ID UCEXP232-41 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.083 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+

o-tolualdehyde



t-butyl isocyanide

24528227

Reaction ID UCEXP232-42 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.083 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+

o-tolualdehyde

Reaction ID UCEXP232-43 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.083 M Precipitate No

431



n-butyl isocyanide

24528228

Comments Reference

http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+

o-tolualdehyde



1-pentyl isocyanide

24528229

Reaction ID UCEXP232-44

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.083 M Precipitate Yes Product Pending Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+

o-tolualdehyde



cyclohexylisocyanide

24528230

Reaction ID UCEXP232-45 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.083 M Precipitate Yes Product Pending Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+



1,1,3,3tetramethylbutyl isocyanide

o-tolualdehyde

24528231

Reaction ID UCExp241-22 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.578 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp241

+

3,4methylenedioxyphenylacetic acid

+

methylamine

+

o-tolualdehyde

o-vanillin 432



t-butyl isocyanide

24528363

Reaction ID UCEXP131-4 Researcher Rikesh Parikh Reaction Type Ugi Solvent methanol Limiting Reactant 0.612 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp131

+

Boc-Trp-OH

+

1-heptylamine

+

o-vanillin



benzyl isocyanide

21106061

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCEXP131-5 Researcher Rikesh Parikh Reaction Type Ugi Solvent methanol Limiting Reactant 0.605 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp131

+

Boc-Trp-OH

+

1-octylamine

+

o-vanillin



benzyl isocyanide

21106062

Reaction ID UCEXP131-6 Researcher Rikesh Parikh Reaction Type Ugi Solvent methanol Limiting Reactant 0.625 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp131

+

Boc-Trp-OH

+

1-hexylamine

+

o-vanillin



n-butyl isocyanide

21106063

Reaction ID UCEXP131-7 Researcher Rikesh Parikh Reaction Type Ugi Solvent methanol Limiting Reactant 0.617 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp131

+

Boc-Trp-OH

+

1-hexylamine

+

o-vanillin

Reaction ID UCEXP131-8

433



1-pentyl isocyanide

21106064

Researcher Rikesh Parikh Reaction Type Ugi Solvent methanol Limiting Reactant 0.618 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp131

+

Boc-Trp-OH

+

1-heptylamine

+

o-vanillin



n-butyl isocyanide

21106065

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCEXP131-9 Researcher Rikesh Parikh Reaction Type Ugi Solvent methanol Limiting Reactant 0.61 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp131

+

Boc-Trp-OH

+

1-heptylamine

+

o-vanillin



1-pentyl isocyanide

21106066

Reaction ID UCEXP134-1 Researcher Rikesh Parikh Reaction Type Ugi Solvent methanol Limiting Reactant 0.645 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp134

+

Boc-Trp-OH

+

1-propylamine

+

o-vanillin



n-butyl isocyanide

21106070

Reaction ID UCEXP134-2 Researcher Rikesh Parikh Reaction Type Ugi Solvent methanol Limiting Reactant 0.636 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp134

+

Boc-Trp-OH

+

1-propylamine

+

o-vanillin

Reaction ID UCEXP134-3 Researcher Reaction Type

Rikesh Parikh Ugi

434



1-pentyl isocyanide

21106071

Solvent methanol Limiting Reactant 0.612 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp134

+

+

Boc-Trp-OH

1-octylamine

+

o-vanillin



n-butyl isocyanide

21106072

Reaction ID UCEXP134-4

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Researcher Rikesh Parikh Reaction Type Ugi Solvent methanol Limiting Reactant 0.604 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp134

+

+

Boc-Trp-OH

1-octylamine

+

o-vanillin



1-pentyl isocyanide

21106073

Reaction ID UCEXP171B/V2B2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.219 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp171

+

1-pyrenebutyric acid

+

5-methylfurfurylamine

+

o-vanillin



t-butyl isocyanide

21106056

Reaction ID UCEXP171D/V2B4 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.219 M Precipitate Yes Product No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp171

+

1-pyrenebutyric acid

+

benzylamine

+

o-vanillin

Reaction ID UCEXP173N/V2B26 Researcher Reaction Type Solvent

Khalid Mirza Ugi methanol

435



t-butyl isocyanide

21105846

Limiting Reactant 0.217 M Precipitate Reactants Insoluble Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp173

+

decanoic acid

+

+

2-chloroaniline

o-vanillin



tosylmethyl isocyanide

21105847

Reaction ID UCEXP181-068V2

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.224 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

+

3,4-dihydroxyphenylacetic acid

+

+

methylamine

o-vanillin



tosylmethyl isocyanide

24528107

octadecylamine Reaction ID UCEXP228-1 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.253 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp228

+

Boc-Trp-OH

+

octadecylamine

+

4,7-dimethoxy-1-naphthaldehyde



tosylmethyl isocyanide

24528181

Reaction ID UCEXP228-2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.265 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp228

+

Boc-Trp-OH

+

octadecylamine

+

3-hydroxybenzaldehyde

Reaction ID UCEXP228-3 Researcher

Khalid Mirza

436



n-butyl isocyanide

24528182

Reaction Type Ugi Solvent methanol Limiting Reactant 0.551 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp228

+

Boc-Trp-OH

+

octadecylamine

+

2,4-dimethylbenzaldehyde



n-butyl isocyanide

24534188

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCEXP228-4 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.634 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp228

+

Boc-Trp-OH

+

+

octadecylamine

benzaldehyde



n-butyl isocyanide

24534192

Reaction ID UCEXP229-1 Researcher David Bulger Reaction Type Ugi Solvent methanol Limiting Reactant 0.667 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp229

+

Boc-Trp-OH

+

octadecylamine

+

4-methylbenzaldehyde



t-butyl isocyanide

24534189

phenanthrene-9-carboxaldehyde Reaction ID UCEXP148A-V1B153 Researcher Khalid Mirza/ Emily Messner Reaction Type Ugi Solvent methanol Limiting Reactant 0.398 M Precipitate Yes but the aldehyde alone is not soluble in methanol Yield 50.1 % Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp148

+

crotonic acid

+

1-heptylamine

+

phenanthrene-9-carboxaldehyde

437



t-butyl isocyanide

21106058

Reaction ID UCEXP150D-V1B155 Researcher Khalid Mirza/ Emily Messner Reaction Type Ugi Solvent methanol Limiting Reactant 0.404 M Precipitate Yes but the aldehyde alone is not soluble in methanol Yield 59 % Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp150

+

crotonic acid

+

benzylamine

+

phenanthrene-9-carboxaldehyde



t-butyl isocyanide

21105601

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCEXP156B-V1B155 Researcher Emily Messner Reaction Type Ugi Solvent methanol Limiting Reactant 0.678 M Precipitate Yes but reactants initially insoluble Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp156

+

crotonic acid

+

benzylamine

+

phenanthrene-9-carboxaldehyde



t-butyl isocyanide

21106075

Reaction ID UCEXP159C-V1B18 Researcher Emily Messner Reaction Type Ugi Solvent methanol Limiting Reactant 0.661 M Precipitate Yes but the aldehyde alone is not soluble in methanol Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp159

+

4-chlorophenylacetic acid

+

benzylamine

+

phenanthrene-9-carboxaldehyde



n-butyl isocyanide

21106077

Reaction ID UCEXP160C-V1B19 Researcher Emily Messner Reaction Type Ugi Solvent methanol Limiting Reactant 0.388 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp160

+

3,4-dihydroxyphenylacetic acid

+

furfurylamine

+

phenanthrene-9-carboxaldehyde

438



n-butyl isocyanide

21105579

Reaction ID UCEXP162 Researcher Shannon Oseback Reaction Type Ugi Solvent methanol Limiting Reactant 0.285 M Precipitate Reactants Insoluble Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp162

+

phenylacetic acid

+

cyclohexylamine

+

phenanthrene-9-carboxaldehyde



t-butyl isocyanide

21105590

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCEXP163A-V1B14 Researcher Tim Bohinsky Reaction Type Ugi Solvent methanol Limiting Reactant 0.387 M Precipitate no and aldehyde alone not solube Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp163

+

mandelic acid

+

furfurylamine

+

phenanthrene-9-carboxaldehyde



t-butyl isocyanide

21105596

Reaction ID UCEXP164 Researcher Emily Messner/Shannon Oseback Reaction Type Ugi Solvent methanol Limiting Reactant 0.287 M Precipitate Reactants Insoluble Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp164

+

phenylacetic acid

+

aniline

+

phenanthrene-9-carboxaldehyde



n-butyl isocyanide

21106183

Reaction ID UCEXP167A-V1B12 Researcher Tim Bohinsky Reaction Type Ugi Solvent methanol Limiting Reactant 0.403 M Precipitate Reactants Insoluble Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp167

+

3,4methylenedioxyphenylacetic acid

+

1-propylamine

+

phenanthrene-9-carboxaldehyde

439



n-butyl isocyanide

21105597

Reaction ID UCEXP171C/V2B3 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.222 M Precipitate Reactants Insoluble Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp171

+

2,4,6-trihydroxybenzoic acid

+

methylamine

+

phenanthrene-9-carboxaldehyde



tosylmethyl isocyanide

21106040

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCEXP171LV2B-12 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.22 M Precipitate Reactants Insoluble Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp171

+

1-pyrenebutyric acid

+

methylamine

+

phenanthrene-9-carboxaldehyde



t-butyl isocyanide

21106039

Reaction ID UCEXP173F/V2B18 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.219 M Precipitate no and aldehyde alone not solube Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp173

+

2,3-dihydroxybenzoic acid

+

furfurylamine

+

phenanthrene-9-carboxaldehyde



t-butyl isocyanide

21106041

Reaction ID UCEXP174C/V2B34 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.226 M Precipitate Yes but the aldehyde alone is not soluble in methanol Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp174

+

5-nitrosalicylic acid

+

methylamine

+

phenanthrene-9-carboxaldehyde

Reaction ID UCEXP175D

440



n-butyl isocyanide

21106205

Researcher Khalid Mirza/ Emily Messner Reaction Type Ugi Solvent methanol Limiting Reactant 0.398 M Precipitate Yes but the aldehyde alone is not soluble in methanol Yield - % Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp175

+

+

4-chlorophenylacetic acid

benzylamine

+

phenanthrene-9-carboxaldehyde



n-butyl isocyanide

21106077

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCEXP176C Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant - M Precipitate Yes Yield 62 % Comments aldehyde not soluble until all reactants added Reference http://usefulchem.wikispaces.com/Exp176

+

phenylacetic acid

+

furfurylamine

+

phenanthrene-9-carboxaldehyde



n-butyl isocyanide

21105594

Reaction ID UCEXP177 Researcher Shannon Oseback Reaction Type Ugi Solvent methanol Limiting Reactant 0.224 M Precipitate Reactants Insoluble Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp177

+

phenylacetic acid

+

1-propylamine

+

phenanthrene-9-carboxaldehyde



n-butyl isocyanide

21105831

Reaction ID UCEXP178 Researcher Shannon Oseback Reaction Type Ugi Solvent methanol Limiting Reactant 0.388 M Precipitate Yes but the aldehyde alone is not soluble in methanol Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp178

+

phenylacetic acid

+

furfurylamine

+

phenanthrene-9-carboxaldehyde

Reaction ID UCEXP179

441



n-butyl isocyanide

21105594

Researcher Shannon Oseback Reaction Type Ugi Solvent methanol Limiting Reactant 0.286 M Precipitate Reactants Insoluble Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp179

+

+

4-chlorophenylacetic acid

aniline

+

phenanthrene-9-carboxaldehyde



t-butyl isocyanide

21105833

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCEXP180 Researcher Shannon Oseback Reaction Type Ugi Solvent methanol Limiting Reactant 0.403 M Precipitate no and aldehyde alone not solube Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp180

+

+

acetic acid

1-heptylamine

+

phenanthrene-9-carboxaldehyde



n-butyl isocyanide

21105834

Reaction ID UCEXP181-055V2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.223 M Precipitate no and aldehyde alone not solube Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

+

2,6-dihydroxybenzoic acid

+

5-methylfurfurylamine

+

phenanthrene-9-carboxaldehyde



n-butyl isocyanide

24528096

Reaction ID UCEXP181-056V2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.219 M Precipitate Reactants Insoluble Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

+

2,4,6-trihydroxybenzoic acid

+

furfurylamine

+

phenanthrene-9-carboxaldehyde

Reaction ID UCEXP181-075V2 Researcher

Khalid Mirza

442



n-butyl isocyanide

24528097

Reaction Type Ugi Solvent methanol Limiting Reactant 0.218 M Precipitate no and aldehyde alone not solube Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

+

mandelic acid

+

furfurylamine

+

phenanthrene-9-carboxaldehyde



n-butyl isocyanide

24528111

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCEXP181-079V2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.218 M Precipitate Reactants Insoluble Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

+

2,4,6-trihydroxybenzoic acid

+

furfurylamine

+

phenanthrene-9-carboxaldehyde



t-butyl isocyanide

24528115

Reaction ID UCEXP181-103V2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.226 M Precipitate no and aldehyde alone not solube Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

+

mandelic acid

+

methylamine

+

phenanthrene-9-carboxaldehyde



n-butyl isocyanide

24528133

Reaction ID UCEXP181-111V2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.226 M Precipitate Reactants Insoluble Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

+

2,4,6-trihydroxybenzoic acid

+

methylamine

+

phenanthrene-9-carboxaldehyde

Reaction ID UCEXP181-114V2 Researcher

Khalid Mirza

443



t-butyl isocyanide

24528534

Reaction Type Ugi Solvent methanol Limiting Reactant 0.223 M Precipitate Reactants Insoluble Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

+

2,4,6-trihydroxybenzoic acid

+

5-methylfurfurylamine

+

phenanthrene-9-carboxaldehyde



n-butyl isocyanide

24528143

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCEXP181-123V2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.214 M Precipitate no and aldehyde alone not solube Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

+

+

3,4-dihydroxyphenylacetic acid

furfurylamine

+

phenanthrene-9-carboxaldehyde



tosylmethyl isocyanide

24528151

Reaction ID UCEXP182 Researcher Emily Messner Reaction Type Ugi Solvent methanol Limiting Reactant 0.398 M Precipitate Reactants Insoluble Comments Reference http://usefulchem.wikispaces.com/Exp182

+

furoic acid

+

1-heptylamine

+

phenanthrene-9-carboxaldehyde



n-butyl isocyanide

21168529

Reaction ID UCEXP183-049V1 Researcher Emily Messner Reaction Type Ugi Solvent methanol Limiting Reactant 0.398 M Precipitate Reactants Insoluble Comments Reference http://usefulchem.wikispaces.com/Exp183

+

mandelic acid

+

cyclohexylamine

+

phenanthrene-9-carboxaldehyde

Reaction ID UCEXP184-1/49 Researcher

Emily Messner

444



t-butyl isocyanide

24528153

Reaction Type Ugi Solvent ethanol Limiting Reactant 0.398 M Precipitate Reactants insoluble Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp184

+

mandelic acid

+

cyclohexylamine

+

phenanthrene-9-carboxaldehyde



t-butyl isocyanide

24528154

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCEXP184-2/49 Researcher Emily Messner Reaction Type Ugi Solvent acetonitrile Limiting Reactant 0.398 M Precipitate Reactants insoluble Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp184

+

mandelic acid

+

cyclohexylamine

+

phenanthrene-9-carboxaldehyde



t-butyl isocyanide

24528154

Reaction ID UCEXP184-3/49 Researcher Emily Messner Reaction Type Ugi Solvent dichloromethane Limiting Reactant 0.398 M Precipitate Reactants insoluble Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp184

+

mandelic acid

+

cyclohexylamine

+

phenanthrene-9-carboxaldehyde



t-butyl isocyanide

24528154

Reaction ID UCEXP214C Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.404 M Precipitate Yes but the aldehyde alone is not soluble in methanol Yield - % Comments Reference http://usefulchem.wikispaces.com/Exp214

+

crotonic acid

+

benzylamine

+

phenanthrene-9-carboxaldehyde

Reaction ID UCEXP215A Researcher Reaction Type

Khalid Mirza Ugi

445



t-butyl isocyanide

21105601

Solvent THF Limiting Reactant 0.661 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp215

+

crotonic acid

+

1-heptylamine

+

phenanthrene-9-carboxaldehyde



t-butyl isocyanide

21106058

Reaction ID UCEXP215B

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 0.678 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp215

+

crotonic acid

+

benzylamine

+

phenanthrene-9-carboxaldehyde



t-butyl isocyanide

21105601

Reaction ID UCEXP215F Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 0.661 M Precipitate Yes but not at room temperature Yield - % Comments Reference http://usefulchem.wikispaces.com/Exp215

+

4-chlorophenylacetic acid

+

benzylamine

+

phenanthrene-9-carboxaldehyde



n-butyl isocyanide

21106077

Reaction ID UCEXP217-1 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 0.384 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp217

+

4-chlorophenylacetic acid

+

benzylamine

+

phenanthrene-9-carboxaldehyde

Reaction ID UCEXP217-2 Researcher Reaction Type Solvent

Khalid Mirza Ugi THF

446



n-butyl isocyanide

21106077

Limiting Reactant 0.383 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp217

+

crotonic acid

+

benzylamine

+

phenanthrene-9-carboxaldehyde



t-butyl isocyanide

21105601

Reaction ID UCEXP217-5

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 0.384 M Precipitate Yes Product Pending Comments Reference http://usefulchem.wikispaces.com/Exp217

+

Boc-Gly-OH

+

furfurylamine

+

phenanthrene-9-carboxaldehyde



n-butyl isocyanide

21105594

Reaction ID UCEXP231-2 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1 M Precipitate aldehyde insoluble at this concentration Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp231

+

crotonic acid

+

benzylamine

+

phenanthrene-9-carboxaldehyde



t-butyl isocyanide

21105601

Reaction ID UCExp237-01 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.778 M Precipitate Yes Product Awaiting Characterization Comments Reference http://usefulchem.wikispaces.com/Exp237

+

phenylacetic acid

+

furfurylamine

+

phenanthrene-9-carboxaldehyde

Reaction ID UCExp237-02 Researcher Reaction Type Solvent

Khalid Mirza Ugi THF

447



n-butyl isocyanide

21105594

Limiting Reactant 0.746 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp237

+

phenylacetic acid

+

furfurylamine

+

phenanthrene-9-carboxaldehyde



n-butyl isocyanide

21105594

Reaction ID UCExp238-01

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.881 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp238

+

crotonic acid

+

2-chloroaniline

+

phenanthrene-9-carboxaldehyde



cyclohexylisocyanide

24528303

Reaction ID UCExp238-02 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.879 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp238

+

crotonic acid

+

3-chloroaniline

+

phenanthrene-9-carboxaldehyde



cyclohexylisocyanide

24528304

Reaction ID UCExp238-03 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.931 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp238

+

crotonic acid

+

aniline

+

phenanthrene-9-carboxaldehyde

Reaction ID UCExp238-04 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.866 M Precipitate No

448



cyclohexylisocyanide

24528305

Comments Reference

http://usefulchem.wikispaces.com/Exp238

+

crotonic acid

+

benzylamine

+

phenanthrene-9-carboxaldehyde



cyclohexylisocyanide

24528306

Reaction ID UCExp238-05

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.903 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp238

+

crotonic acid

+

butylamine

+

phenanthrene-9-carboxaldehyde



cyclohexylisocyanide

24528307

Reaction ID UCExp238-06 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.849 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp238

+

crotonic acid

+

cyclohexylamine

+

phenanthrene-9-carboxaldehyde



cyclohexylisocyanide

24528308

Reaction ID UCExp238-07 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.628 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp238

+

crotonic acid

+

furfurylamine

+

phenanthrene-9-carboxaldehyde

Reaction ID UCExp238-08 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.74 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp238

449



cyclohexylisocyanide

24528309

+

crotonic acid

+

1-heptylamine

+

phenanthrene-9-carboxaldehyde



cyclohexylisocyanide

24528310

Reaction ID UCExp238-09 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.794 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp238

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

+

crotonic acid

+

1-hexylamine

+

phenanthrene-9-carboxaldehyde



cyclohexylisocyanide

24528311

Reaction ID UCExp238-10 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.825 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp238

+

crotonic acid

+

methylamine

+

phenanthrene-9-carboxaldehyde



cyclohexylisocyanide

24528312

Reaction ID UCExp238-11 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.965 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp238

+

crotonic acid

+

1-propylamine

+

phenanthrene-9-carboxaldehyde

Reaction ID UCExp238-12 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.881 M Precipitate Yes but solvent evaporated Comments Reference http://usefulchem.wikispaces.com/Exp238

450



cyclohexylisocyanide

24528313

+

crotonic acid

+

t-butylamine

+

phenanthrene-9-carboxaldehyde



cyclohexylisocyanide

24528314

Reaction ID UCExp238-13 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.921 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp238

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

+

crotonic acid

+

2-chloroaniline

+

phenanthrene-9-carboxaldehyde



t-butyl isocyanide

24528315

Reaction ID UCExp238-14 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.919 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp238

+

crotonic acid

+

3-chloroaniline

+

phenanthrene-9-carboxaldehyde



t-butyl isocyanide

24528316

Reaction ID UCExp238-15 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.974 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp238

+

crotonic acid

+

aniline

+

phenanthrene-9-carboxaldehyde

Reaction ID UCExp238-16 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.906 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp238

451



t-butyl isocyanide

24528317

+

crotonic acid

+

benzylamine

+

phenanthrene-9-carboxaldehyde



t-butyl isocyanide

21105601

Reaction ID UCExp238-17 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.945 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp238

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

+

crotonic acid

+

butylamine

+

phenanthrene-9-carboxaldehyde



t-butyl isocyanide

24528318

Reaction ID UCExp238-18 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.888 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp238

+

crotonic acid

+

cyclohexylamine

+

phenanthrene-9-carboxaldehyde



t-butyl isocyanide

24528319

Reaction ID UCExp238-19 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.658 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp238

+

crotonic acid

+

furfurylamine

+

phenanthrene-9-carboxaldehyde

Reaction ID UCExp238-20 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.775 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp238

452



t-butyl isocyanide

24528320

+

crotonic acid

+

1-heptylamine

+

phenanthrene-9-carboxaldehyde



t-butyl isocyanide

21106058

Reaction ID UCExp238-21 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.831 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp238

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

+

crotonic acid

+

1-hexylamine

+

phenanthrene-9-carboxaldehyde



t-butyl isocyanide

24528321

Reaction ID UCExp238-22 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.867 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp238

+

crotonic acid

+

methylamine

+

phenanthrene-9-carboxaldehyde



t-butyl isocyanide

24528322

Reaction ID UCExp238-23 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 2.009 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp238

+

crotonic acid

+

1-propylamine

+

phenanthrene-9-carboxaldehyde

Reaction ID UCExp238-24 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.921 M Precipitate Yes but solvent evaporated Comments Reference http://usefulchem.wikispaces.com/Exp238

453



t-butyl isocyanide

24528323

+

crotonic acid

+

t-butylamine

+

phenanthrene-9-carboxaldehyde



t-butyl isocyanide

24528324

Reaction ID UCExp238-25 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.686 M Precipitate Yes Product Awaiting Characterization Comments Reference http://usefulchem.wikispaces.com/Exp238

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

+

Boc-Gly-OH

+

2-chloroaniline

+

phenanthrene-9-carboxaldehyde



cyclohexylisocyanide

24528325

Reaction ID UCExp238-26 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.684 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp238

+

Boc-Gly-OH

+

3-chloroaniline

+

phenanthrene-9-carboxaldehyde



cyclohexylisocyanide

24528326

Reaction ID UCExp238-27 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.726 M Precipitate Yes Product Awaiting Characterization Comments Reference http://usefulchem.wikispaces.com/Exp238

+

Boc-Gly-OH

+

aniline

+

phenanthrene-9-carboxaldehyde

Reaction ID UCExp238-28 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.674 M Precipitate Yes Product Awaiting Characterization Comments -

454



cyclohexylisocyanide

24528327

Reference

http://usefulchem.wikispaces.com/Exp238

+

Boc-Gly-OH

+

benzylamine

+

phenanthrene-9-carboxaldehyde



cyclohexylisocyanide

24528328

Reaction ID UCExp238-29

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.704 M Precipitate Yes Product Awaiting Characterization Comments Reference http://usefulchem.wikispaces.com/Exp238

+

Boc-Gly-OH

+

butylamine

+

phenanthrene-9-carboxaldehyde



cyclohexylisocyanide

24528329

Reaction ID UCExp238-30 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.378 M Precipitate Yes but solvent evaporated Comments Reference http://usefulchem.wikispaces.com/Exp238

+

Boc-Gly-OH

+

cyclohexylamine

+

phenanthrene-9-carboxaldehyde



cyclohexylisocyanide

24528330

Reaction ID UCExp238-31 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.48 M Precipitate Yes but solvent evaporated Comments Reference http://usefulchem.wikispaces.com/Exp238

+

Boc-Gly-OH

+

furfurylamine

+

phenanthrene-9-carboxaldehyde

Reaction ID UCExp238-32 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.572 M Precipitate Yes Product Awaiting Characterization Comments -

455



cyclohexylisocyanide

24528331

Reference

http://usefulchem.wikispaces.com/Exp238

+

Boc-Gly-OH

+

1-heptylamine

+

phenanthrene-9-carboxaldehyde



cyclohexylisocyanide

24528332

Reaction ID UCExp238-33

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.616 M Precipitate Yes Product Awaiting Characterization Comments Reference http://usefulchem.wikispaces.com/Exp238

+

Boc-Gly-OH

+

1-hexylamine

+

phenanthrene-9-carboxaldehyde



cyclohexylisocyanide

24528333

Reaction ID UCExp238-34 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.648 M Precipitate Yes Product Awaiting Characterization Comments Reference http://usefulchem.wikispaces.com/Exp238

+

Boc-Gly-OH

+

methylamine

+

phenanthrene-9-carboxaldehyde



cyclohexylisocyanide

24528334

Reaction ID UCExp238-35 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.753 M Precipitate Yes Product Awaiting Characterization Comments Reference http://usefulchem.wikispaces.com/Exp238

+

Boc-Gly-OH

+

1-propylamine

+

phenanthrene-9-carboxaldehyde

Reaction ID UCExp238-36 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.686 M Precipitate Yes but solvent evaporated

456



cyclohexylisocyanide

24528335

Comments Reference

http://usefulchem.wikispaces.com/Exp238

+

Boc-Gly-OH

+

t-butylamine

+

phenanthrene-9-carboxaldehyde



cyclohexylisocyanide

24528336

Reaction ID UCExp238-37

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.718 M Precipitate Yes but solvent evaporated Comments Reference http://usefulchem.wikispaces.com/Exp238

+

Boc-Gly-OH

+

2-chloroaniline

+

phenanthrene-9-carboxaldehyde



t-butyl isocyanide

24528337

Reaction ID UCExp238-38 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.716 M Precipitate Yes but solvent evaporated Comments Reference http://usefulchem.wikispaces.com/Exp238

+

Boc-Gly-OH

+

3-chloroaniline

+

phenanthrene-9-carboxaldehyde



t-butyl isocyanide

24528338

Reaction ID UCExp238-39 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.76 M Precipitate Yes Product Awaiting Characterization Comments Reference http://usefulchem.wikispaces.com/Exp238

+

Boc-Gly-OH

+

aniline

+

phenanthrene-9-carboxaldehyde

Reaction ID UCExp238-40 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.706 M Precipitate Yes Product Awaiting Characterization

457



t-butyl isocyanide

24528339

Comments Reference

http://usefulchem.wikispaces.com/Exp238

+

Boc-Gly-OH

+

benzylamine

+

phenanthrene-9-carboxaldehyde



t-butyl isocyanide

24528340

Reaction ID UCExp238-41

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.737 M Precipitate Yes but solvent evaporated Comments Reference http://usefulchem.wikispaces.com/Exp238

+

Boc-Gly-OH

+

butylamine

+

phenanthrene-9-carboxaldehyde



t-butyl isocyanide

24528341

Reaction ID UCExp238-42 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.399 M Precipitate Yes but solvent evaporated Comments Reference http://usefulchem.wikispaces.com/Exp238

+

Boc-Gly-OH

+

cyclohexylamine

+

phenanthrene-9-carboxaldehyde



t-butyl isocyanide

24528342

Reaction ID UCExp238-43 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.505 M Precipitate Yes Product Awaiting Characterization Comments Reference http://usefulchem.wikispaces.com/Exp238

+

Boc-Gly-OH

+

furfurylamine

+

phenanthrene-9-carboxaldehyde

Reaction ID UCExp238-44 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.6 M Precipitate Yes Product Awaiting Characterization

458



t-butyl isocyanide

24528343

Comments Reference

http://usefulchem.wikispaces.com/Exp238

+

Boc-Gly-OH

+

1-heptylamine

+

phenanthrene-9-carboxaldehyde



t-butyl isocyanide

24528344

Reaction ID UCExp240-01

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.607 M Precipitate Yes but after 48h Comments Reference http://usefulchem.wikispaces.com/Exp240

+

phenylacetic acid

+

furfurylamine

+

phenanthrene-9-carboxaldehyde



n-butyl isocyanide

21105594

Reaction ID UCExp240-02 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.587 M Precipitate Yes Yield - % Comments Reference http://usefulchem.wikispaces.com/Exp240

+

phenylacetic acid

+

furfurylamine

+

phenanthrene-9-carboxaldehyde



t-butyl isocyanide

21791788

Reaction ID UCExp240-03 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.562 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp240

+

phenylacetic acid

+

furfurylamine

+

phenanthrene-9-carboxaldehyde

Reaction ID UCExp240-04 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.458 M Precipitate No Comments -

459



cyclohexylisocyanide

24528345

Reference

http://usefulchem.wikispaces.com/Exp240

+

+

phenylacetic acid

furfurylamine

+



1,1,3,3tetramethylbutyl isocyanide

phenanthrene-9-carboxaldehyde

21782583

Reaction ID UCExp240-05

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.568 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp240

+

+

phenylacetic acid

furfurylamine

+

phenanthrene-9-carboxaldehyde



benzyl isocyanide

24528346

Reaction ID UCExp240-06 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.559 M Precipitate Yes Yield - % Comments Reference http://usefulchem.wikispaces.com/Exp240

+

+

phenylacetic acid

furfurylamine

+

phenanthrene-9-carboxaldehyde



1-pentyl isocyanide

24528347

Reaction ID UCExp240-07 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.839 M Precipitate Yes Yield - % Comments Reference http://usefulchem.wikispaces.com/Exp240

+

phenylacetic acid

+

5-methylfurfurylamine

+

phenanthrene-9-carboxaldehyde

Reaction ID UCExp240-08 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.813 M

460



n-butyl isocyanide

21782451

Precipitate Comments Reference

Yes but 48h http://usefulchem.wikispaces.com/Exp240

+

phenylacetic acid

+

5-methylfurfurylamine

+

phenanthrene-9-carboxaldehyde



t-butyl isocyanide

24528348

Reaction ID UCExp240-09

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.78 M Precipitate Yes Yield - % Comments Reference http://usefulchem.wikispaces.com/Exp240

+

phenylacetic acid

+

5-methylfurfurylamine

+

phenanthrene-9-carboxaldehyde



cyclohexylisocyanide

21782450

Reaction ID UCExp240-10 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.646 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp240

+

phenylacetic acid

+

5-methylfurfurylamine

+



1,1,3,3tetramethylbutyl isocyanide

phenanthrene-9-carboxaldehyde

24528349

Reaction ID UCExp240-11 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.788 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp240

+

phenylacetic acid

+

5-methylfurfurylamine

+

phenanthrene-9-carboxaldehyde

Reaction ID UCExp240-12 Researcher Reaction Type Solvent

Khalid Mirza Ugi THF

461



benzyl isocyanide

24528350

Limiting Reactant 1.776 M Precipitate Yes but 48h Comments Reference http://usefulchem.wikispaces.com/Exp240

+

phenylacetic acid

+

5-methylfurfurylamine

+

phenanthrene-9-carboxaldehyde



1-pentyl isocyanide

24528351

Reaction ID UCExp242-1

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Researcher Marshall Moritz Reaction Type Ugi Solvent benzene Limiting Reactant 0.435 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp242

+

phenylacetic acid

+

furfurylamine

+

phenanthrene-9-carboxaldehyde



n-butyl isocyanide

21105594

Reaction ID UCExp242-10 Researcher Marshall Moritz Reaction Type Ugi Solvent benzene Limiting Reactant 0.424 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp242

+

phenylacetic acid

+

5-methylfurfurylamine

+

phenanthrene-9-carboxaldehyde



1-pentyl isocyanide

24528382

Reaction ID UCExp242-2 Researcher Marshall Moritz Reaction Type Ugi Solvent benzene Limiting Reactant 0.436 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp242

+

phenylacetic acid

+

furfurylamine

+

phenanthrene-9-carboxaldehyde

Reaction ID UCExp242-3 Researcher Marshall Moritz Reaction Type Ugi Solvent benzene Limiting Reactant 0.432 M Precipitate Yes

462



t-butyl isocyanide

24528383

Product Comments Reference

No http://usefulchem.wikispaces.com/Exp242

+

phenylacetic acid

+

furfurylamine

+

phenanthrene-9-carboxaldehyde



cyclohexylisocyanide

24528384

Reaction ID UCExp242-4

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Researcher Marshall Moritz Reaction Type Ugi Solvent benzene Limiting Reactant 0.414 M Precipitate Yes Product No Comments Reference http://usefulchem.wikispaces.com/Exp242

+

phenylacetic acid

+

furfurylamine

+



1,1,3,3tetramethylbutyl isocyanide

phenanthrene-9-carboxaldehyde

24528385

Reaction ID UCExp242-5 Researcher Marshall Moritz Reaction Type Ugi Solvent benzene Limiting Reactant 0.432 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp242

+

phenylacetic acid

+

furfurylamine

+

phenanthrene-9-carboxaldehyde



1-pentyl isocyanide

24528386

Reaction ID UCExp242-6 Researcher Marshall Moritz Reaction Type Ugi Solvent benzene Limiting Reactant 0.431 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp242

+

phenylacetic acid

+

5-methylfurfurylamine

+

phenanthrene-9-carboxaldehyde

Reaction ID UCExp242-7 Researcher Reaction Type Solvent

Marshall Moritz Ugi benzene

463



n-butyl isocyanide

24528387

Limiting Reactant 0.428 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp242

+

phenylacetic acid

+

5-methylfurfurylamine

+

phenanthrene-9-carboxaldehyde



t-butyl isocyanide

24528388

Reaction ID UCExp242-8

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Researcher Marshall Moritz Reaction Type Ugi Solvent benzene Limiting Reactant 0.424 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp242

+

phenylacetic acid

+

5-methylfurfurylamine

+

phenanthrene-9-carboxaldehyde



cyclohexylisocyanide

24528389

Reaction ID UCExp242-9 Researcher Marshall Moritz Reaction Type Ugi Solvent benzene Limiting Reactant 0.406 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp242

+

phenylacetic acid

+

5-methylfurfurylamine

+



1,1,3,3tetramethylbutyl isocyanide

phenanthrene-9-carboxaldehyde

24528390

Reaction ID UCExp252-01 Researcher Khalid Mirza Reaction Type Ugi Solvent benzene Limiting Reactant 0.403 M Precipitate Yes Yield - % Comments Reference http://usefulchem.wikispaces.com/Exp252

+

phenylacetic acid

+

furfurylamine

+

phenanthrene-9-carboxaldehyde

Reaction ID UCExp253-01 Researcher Reaction Type

Khalid Mirza Ugi

464



n-butyl isocyanide

21105594

Solvent methanol Limiting Reactant 0.53 M Precipitate Yes Yield 42.6 % Comments Reference http://usefulchem.wikispaces.com/Exp253

+

phenylacetic acid

+

furfurylamine

+

phenanthrene-9-carboxaldehyde



n-butyl isocyanide

21105594

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCExp254-01 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.08 M Precipitate Yes Yield - % Comments Reference http://usefulchem.wikispaces.com/Exp254

+

phenylacetic acid

+

furfurylamine

+

phenanthrene-9-carboxaldehyde



n-butyl isocyanide

21105594

Reaction ID UCExp255-01 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.4 M Precipitate Yes Yield 65.8 % Comments Reference http://usefulchem.wikispaces.com/Exp255

+

phenylacetic acid

+

furfurylamine

+

phenanthrene-9-carboxaldehyde



n-butyl isocyanide

21105594

Reaction ID UCExp255-02 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.4 M Precipitate Yes Yield 65.1 % Comments Reference http://usefulchem.wikispaces.com/Exp255

+

phenylacetic acid

+

furfurylamine

+

phenanthrene-9-carboxaldehyde

465



n-butyl isocyanide

21105594

Reaction ID UCExp255-03 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.4 M Precipitate Yes Yield 66.4 % Comments Reference http://usefulchem.wikispaces.com/Exp255

+

phenylacetic acid

+

furfurylamine

+

phenanthrene-9-carboxaldehyde



n-butyl isocyanide

21105594

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCExp255-04 Researcher Khalid Mirza Reaction Type Ugi Solvent benzene Limiting Reactant 0.4 M Precipitate Yes Yield 29.7 % Comments Reference http://usefulchem.wikispaces.com/Exp255

+

phenylacetic acid

+

furfurylamine

+

phenanthrene-9-carboxaldehyde



n-butyl isocyanide

21105594

Reaction ID UCExp255-05 Researcher Khalid Mirza Reaction Type Ugi Solvent benzene Limiting Reactant 0.4 M Precipitate Yes Yield 30.5 % Comments Reference http://usefulchem.wikispaces.com/Exp255

+

phenylacetic acid

+

furfurylamine

+

phenanthrene-9-carboxaldehyde



n-butyl isocyanide

21105594

Reaction ID UCExp255-06 Researcher Khalid Mirza Reaction Type Ugi Solvent benzene Limiting Reactant 0.4 M Precipitate Yes Yield 28.9 % Comments Reference http://usefulchem.wikispaces.com/Exp255

+

+

+

466



phenylacetic acid

furfurylamine

phenanthrene-9-carboxaldehyde

n-butyl isocyanide

21105594

Reaction ID UCExp256-01 Researcher Khalid Mirza Reaction Type Ugi Solvent benzene Limiting Reactant 0.4 M Precipitate Yes Yield 17 % Comments Reference http://usefulchem.wikispaces.com/Exp256

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

+

phenylacetic acid

+

furfurylamine

+

phenanthrene-9-carboxaldehyde



n-butyl isocyanide

21105594

Reaction ID UCExp257-01 Researcher Khalid Mirza Reaction Type Ugi Solvent ethyl acetate Limiting Reactant 0.37 M Precipitate Yes Yield 24 % Comments Reference http://usefulchem.wikispaces.com/Exp257

+

phenylacetic acid

+

furfurylamine

+

phenanthrene-9-carboxaldehyde



n-butyl isocyanide

21105594

phenylacetic acid Reaction ID UCEXP162 Researcher Shannon Oseback Reaction Type Ugi Solvent methanol Limiting Reactant 0.285 M Precipitate Reactants Insoluble Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp162

+

phenylacetic acid

+

cyclohexylamine

+

phenanthrene-9-carboxaldehyde

Reaction ID UCEXP164 Researcher Emily Messner/Shannon Oseback Reaction Type Ugi Solvent methanol Limiting Reactant 0.287 M

467



t-butyl isocyanide

21105590

Precipitate Comments Reference

Reactants Insoluble Protocol from Explan005 followed http://usefulchem.wikispaces.com/Exp164

+

+

phenylacetic acid

aniline

+

phenanthrene-9-carboxaldehyde



n-butyl isocyanide

21106183

Reaction ID UCEXP176C

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant - M Precipitate Yes Yield 62 % Comments aldehyde not soluble until all reactants added Reference http://usefulchem.wikispaces.com/Exp176

+

phenylacetic acid

+

furfurylamine

+

phenanthrene-9-carboxaldehyde



n-butyl isocyanide

21105594

Reaction ID UCEXP177 Researcher Shannon Oseback Reaction Type Ugi Solvent methanol Limiting Reactant 0.224 M Precipitate Reactants Insoluble Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp177

+

phenylacetic acid

+

1-propylamine

+

phenanthrene-9-carboxaldehyde



n-butyl isocyanide

21105831

Reaction ID UCEXP178 Researcher Shannon Oseback Reaction Type Ugi Solvent methanol Limiting Reactant 0.388 M Precipitate Yes but the aldehyde alone is not soluble in methanol Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp178

+

phenylacetic acid

+

furfurylamine

+

phenanthrene-9-carboxaldehyde

Reaction ID UCExp237-01 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.778 M Precipitate Yes

468



n-butyl isocyanide

21105594

Product Comments Reference

Awaiting Characterization http://usefulchem.wikispaces.com/Exp237

+

phenylacetic acid

+

furfurylamine

+

phenanthrene-9-carboxaldehyde



n-butyl isocyanide

21105594

Reaction ID UCExp237-02

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 0.746 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp237

+

phenylacetic acid

+

furfurylamine

+

phenanthrene-9-carboxaldehyde



n-butyl isocyanide

21105594

Reaction ID UCExp240-01 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.607 M Precipitate Yes but after 48h Comments Reference http://usefulchem.wikispaces.com/Exp240

+

phenylacetic acid

+

furfurylamine

+

phenanthrene-9-carboxaldehyde



n-butyl isocyanide

21105594

Reaction ID UCExp240-02 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.587 M Precipitate Yes Yield - % Comments Reference http://usefulchem.wikispaces.com/Exp240

+

phenylacetic acid

+

furfurylamine

+

phenanthrene-9-carboxaldehyde

Reaction ID UCExp240-03 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.562 M Precipitate No

469



t-butyl isocyanide

21791788

Comments Reference

http://usefulchem.wikispaces.com/Exp240

+

phenylacetic acid

+

furfurylamine

+

phenanthrene-9-carboxaldehyde



cyclohexylisocyanide

24528345

Reaction ID UCExp240-04

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.458 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp240

+

phenylacetic acid

+

furfurylamine

+



1,1,3,3tetramethylbutyl isocyanide

phenanthrene-9-carboxaldehyde

21782583

Reaction ID UCExp240-05 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.568 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp240

+

phenylacetic acid

+

furfurylamine

+

phenanthrene-9-carboxaldehyde



benzyl isocyanide

24528346

Reaction ID UCExp240-06 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.559 M Precipitate Yes Yield - % Comments Reference http://usefulchem.wikispaces.com/Exp240

+

phenylacetic acid

+

furfurylamine

+

phenanthrene-9-carboxaldehyde

Reaction ID UCExp240-07 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.839 M

470



1-pentyl isocyanide

24528347

Precipitate Yield Comments Reference

Yes - % http://usefulchem.wikispaces.com/Exp240

+

phenylacetic acid

+

5-methylfurfurylamine

+

phenanthrene-9-carboxaldehyde



n-butyl isocyanide

21782451

Reaction ID UCExp240-08

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.813 M Precipitate Yes but 48h Comments Reference http://usefulchem.wikispaces.com/Exp240

+

phenylacetic acid

+

5-methylfurfurylamine

+

phenanthrene-9-carboxaldehyde



t-butyl isocyanide

24528348

Reaction ID UCExp240-09 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.78 M Precipitate Yes Yield - % Comments Reference http://usefulchem.wikispaces.com/Exp240

+

phenylacetic acid

+

5-methylfurfurylamine

+

phenanthrene-9-carboxaldehyde



cyclohexylisocyanide

21782450

Reaction ID UCExp240-10 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.646 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp240

+

phenylacetic acid

+

5-methylfurfurylamine

+

phenanthrene-9-carboxaldehyde

Reaction ID UCExp240-11 Researcher Reaction Type

Khalid Mirza Ugi

471



1,1,3,3tetramethylbutyl isocyanide

24528349

Solvent THF Limiting Reactant 1.788 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp240

+

phenylacetic acid

+

5-methylfurfurylamine

+

phenanthrene-9-carboxaldehyde



benzyl isocyanide

24528350

Reaction ID UCExp240-12

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.776 M Precipitate Yes but 48h Comments Reference http://usefulchem.wikispaces.com/Exp240

+

phenylacetic acid

+

5-methylfurfurylamine

+

phenanthrene-9-carboxaldehyde



1-pentyl isocyanide

24528351

Reaction ID UCExp242-1 Researcher Marshall Moritz Reaction Type Ugi Solvent benzene Limiting Reactant 0.435 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp242

+

phenylacetic acid

+

furfurylamine

+

phenanthrene-9-carboxaldehyde



n-butyl isocyanide

21105594

Reaction ID UCExp242-10 Researcher Marshall Moritz Reaction Type Ugi Solvent benzene Limiting Reactant 0.424 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp242

+

phenylacetic acid

+

5-methylfurfurylamine

+

phenanthrene-9-carboxaldehyde

Reaction ID UCExp242-2 Researcher Marshall Moritz Reaction Type Ugi Solvent benzene Limiting Reactant 0.436 M

472



1-pentyl isocyanide

24528382

Precipitate Comments Reference

No http://usefulchem.wikispaces.com/Exp242

+

phenylacetic acid

+

furfurylamine

+

phenanthrene-9-carboxaldehyde



t-butyl isocyanide

24528383

Reaction ID UCExp242-3

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Researcher Marshall Moritz Reaction Type Ugi Solvent benzene Limiting Reactant 0.432 M Precipitate Yes Product No Comments Reference http://usefulchem.wikispaces.com/Exp242

+

phenylacetic acid

+

furfurylamine

+

phenanthrene-9-carboxaldehyde



cyclohexylisocyanide

24528384

Reaction ID UCExp242-4 Researcher Marshall Moritz Reaction Type Ugi Solvent benzene Limiting Reactant 0.414 M Precipitate Yes Product No Comments Reference http://usefulchem.wikispaces.com/Exp242

+

phenylacetic acid

+

furfurylamine

+



1,1,3,3tetramethylbutyl isocyanide

phenanthrene-9-carboxaldehyde

24528385

Reaction ID UCExp242-5 Researcher Marshall Moritz Reaction Type Ugi Solvent benzene Limiting Reactant 0.432 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp242

+

phenylacetic acid

+

furfurylamine

+

phenanthrene-9-carboxaldehyde

Reaction ID UCExp242-6 Researcher Reaction Type

Marshall Moritz Ugi

473



1-pentyl isocyanide

24528386

Solvent benzene Limiting Reactant 0.431 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp242

+

phenylacetic acid

+

5-methylfurfurylamine

+

phenanthrene-9-carboxaldehyde



n-butyl isocyanide

24528387

Reaction ID UCExp242-7

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Researcher Marshall Moritz Reaction Type Ugi Solvent benzene Limiting Reactant 0.428 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp242

+

phenylacetic acid

+

5-methylfurfurylamine

+

phenanthrene-9-carboxaldehyde



t-butyl isocyanide

24528388

Reaction ID UCExp242-8 Researcher Marshall Moritz Reaction Type Ugi Solvent benzene Limiting Reactant 0.424 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp242

+

phenylacetic acid

+

5-methylfurfurylamine

+

phenanthrene-9-carboxaldehyde



cyclohexylisocyanide

24528389

Reaction ID UCExp242-9 Researcher Marshall Moritz Reaction Type Ugi Solvent benzene Limiting Reactant 0.406 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp242

+

phenylacetic acid

+

5-methylfurfurylamine

+

phenanthrene-9-carboxaldehyde

Reaction ID UCExp252-01 Researcher Reaction Type

Khalid Mirza Ugi

474



1,1,3,3tetramethylbutyl isocyanide

24528390

Solvent benzene Limiting Reactant 0.403 M Precipitate Yes Yield - % Comments Reference http://usefulchem.wikispaces.com/Exp252

+

phenylacetic acid

+

furfurylamine

+

phenanthrene-9-carboxaldehyde



n-butyl isocyanide

21105594

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCExp253-01 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.53 M Precipitate Yes Yield 42.6 % Comments Reference http://usefulchem.wikispaces.com/Exp253

+

phenylacetic acid

+

furfurylamine

+

phenanthrene-9-carboxaldehyde



n-butyl isocyanide

21105594

Reaction ID UCExp254-01 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.08 M Precipitate Yes Yield - % Comments Reference http://usefulchem.wikispaces.com/Exp254

+

phenylacetic acid

+

furfurylamine

+

phenanthrene-9-carboxaldehyde



n-butyl isocyanide

21105594

Reaction ID UCExp255-01 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.4 M Precipitate Yes Yield 65.8 % Comments Reference http://usefulchem.wikispaces.com/Exp255

+

phenylacetic acid

+

furfurylamine

+

phenanthrene-9-carboxaldehyde

475



n-butyl isocyanide

21105594

Reaction ID UCExp255-02 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.4 M Precipitate Yes Yield 65.1 % Comments Reference http://usefulchem.wikispaces.com/Exp255

+

phenylacetic acid

+

furfurylamine

+

phenanthrene-9-carboxaldehyde



n-butyl isocyanide

21105594

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCExp255-03 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.4 M Precipitate Yes Yield 66.4 % Comments Reference http://usefulchem.wikispaces.com/Exp255

+

phenylacetic acid

+

furfurylamine

+

phenanthrene-9-carboxaldehyde



n-butyl isocyanide

21105594

Reaction ID UCExp255-04 Researcher Khalid Mirza Reaction Type Ugi Solvent benzene Limiting Reactant 0.4 M Precipitate Yes Yield 29.7 % Comments Reference http://usefulchem.wikispaces.com/Exp255

+

phenylacetic acid

+

furfurylamine

+

phenanthrene-9-carboxaldehyde



n-butyl isocyanide

21105594

Reaction ID UCExp255-05 Researcher Khalid Mirza Reaction Type Ugi Solvent benzene Limiting Reactant 0.4 M Precipitate Yes Yield 30.5 % Comments Reference http://usefulchem.wikispaces.com/Exp255

+

+

+

476



phenylacetic acid

furfurylamine

phenanthrene-9-carboxaldehyde

n-butyl isocyanide

21105594

Reaction ID UCExp255-06 Researcher Khalid Mirza Reaction Type Ugi Solvent benzene Limiting Reactant 0.4 M Precipitate Yes Yield 28.9 % Comments Reference http://usefulchem.wikispaces.com/Exp255

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

+

phenylacetic acid

+

furfurylamine

+

phenanthrene-9-carboxaldehyde



n-butyl isocyanide

21105594

Reaction ID UCExp256-01 Researcher Khalid Mirza Reaction Type Ugi Solvent benzene Limiting Reactant 0.4 M Precipitate Yes Yield 17 % Comments Reference http://usefulchem.wikispaces.com/Exp256

+

phenylacetic acid

+

furfurylamine

+

phenanthrene-9-carboxaldehyde



n-butyl isocyanide

21105594

Reaction ID UCExp257-01 Researcher Khalid Mirza Reaction Type Ugi Solvent ethyl acetate Limiting Reactant 0.37 M Precipitate Yes Yield 24 % Comments Reference http://usefulchem.wikispaces.com/Exp257

+

phenylacetic acid

+

furfurylamine

+

phenanthrene-9-carboxaldehyde

phenylpropynoic acid Reaction ID UCEXP173G/V2B19 Researcher Reaction Type Solvent

Khalid Mirza Ugi methanol

477



n-butyl isocyanide

21105594

Limiting Reactant 0.223 M Precipitate Yes Yield - % Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp173

+

phenylpropynoic acid

+

benzylamine

+

3,5-dimethoxybenzaldehyde



n-butyl isocyanide

21105845

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCEXP181-057V2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.224 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

+

phenylpropynoic acid

+

methylamine

+

2-hydroxybenzaldehyde



tosylmethyl isocyanide

24528098

Reaction ID UCEXP181-060V2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.221 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

+

phenylpropynoic acid

+

furfurylamine

+

2-hydroxybenzaldehyde



tosylmethyl isocyanide

24528100

Reaction ID UCEXP181-107V2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.222 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

+

phenylpropynoic acid

+

aniline

+

2-hydroxybenzaldehyde

Reaction ID UCEXP233-10 Researcher

David Bulger

478



tosylmethyl isocyanide

24528137

Reaction Type Ugi Solvent methanol Limiting Reactant 1.018 M Precipitate Yes Product Pending Comments Reference http://usefulchem.wikispaces.com/Exp233

+

phenylpropynoic acid

+

benzylamine

+

3,5-dimethoxybenzaldehyde



cyclohexylisocyanide

23078615

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCEXP233-3 Researcher David Bulger Reaction Type Ugi Solvent methanol Limiting Reactant 0.918 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp233

+

phenylpropynoic acid

+

benzylamine

+

3,5-dimethoxybenzaldehyde



t-butyl isocyanide

24528265

Reaction ID UCEXP233-4 Researcher David Bulger Reaction Type Ugi Solvent methanol Limiting Reactant 0.917 M Precipitate Yes Product Pending Comments Reference http://usefulchem.wikispaces.com/Exp233

+

phenylpropynoic acid

+

benzylamine

+

3,5-dimethoxybenzaldehyde



cyclohexylisocyanide

23078615

Reaction ID UCEXP233-9 Researcher David Bulger Reaction Type Ugi Solvent methanol Limiting Reactant 1.021 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp233

+

phenylpropynoic acid

+

benzylamine

+

3,5-dimethoxybenzaldehyde

Reaction ID UCEXP234-1 Researcher

David Bulger

479



t-butyl isocyanide

24528265

Reaction Type Ugi Solvent methanol Limiting Reactant 1.004 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp234

+

phenylpropynoic acid

+

+

3,5Bis(trifluoromethyl)benzaldehyde

benzylamine



t-butyl isocyanide

24528266

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCEXP234-2 Researcher David Bulger Reaction Type Ugi Solvent methanol Limiting Reactant 1.002 M Precipitate Yes Product Pending Comments Reference http://usefulchem.wikispaces.com/Exp234

+

phenylpropynoic acid

+

+

3,5Bis(trifluoromethyl)benzaldehyde

benzylamine



cyclohexylisocyanide

23078614

Reaction ID UCEXP234-3 Researcher David Bulger Reaction Type Ugi Solvent methanol Limiting Reactant 1.004 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp234

+

phenylpropynoic acid

+

+

3,5Bis(trifluoromethyl)benzaldehyde

benzylamine



t-butyl isocyanide

24528266

Reaction ID UCEXP234-4 Researcher David Bulger Reaction Type Ugi Solvent methanol Limiting Reactant 1.002 M Precipitate Yes Product Pending Comments Reference http://usefulchem.wikispaces.com/Exp234

+

phenylpropynoic acid

+

benzylamine

+

3,5Bis(trifluoromethyl)benzaldehyde

480



cyclohexylisocyanide

23078614

piperonal Reaction ID UCEXP052E Researcher Alicia Holsey Reaction Type Ugi Solvent methanol Limiting Reactant 0.223 M Precipitate Yes Yield 32 % Comments 1M solutions of the starting materials was made Reference http://usefulchem.wikispaces.com/Exp052

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

+

Boc-Gly-OH

+

5-methylfurfurylamine

+

piperonal



t-butyl isocyanide

10481872

Reaction ID UCEXP225-1 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.631 M Precipitate Yes Yield - % Comments 0.5 mmol of isocyanide was added to 500uL of a 2M solution of aldehyde; amine and acid Reference http://usefulchem.wikispaces.com/Exp225

+

Boc-Gly-OH

+

furfurylamine

+

piperonal



t-butyl isocyanide

24528157

Reaction ID UCEXP225-2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.905 M Precipitate Yes Product Pending Comments 0.5 mmol of isocyanide was added to 500uL of a 2M solution of aldehyde; amine and acid Reference http://usefulchem.wikispaces.com/Exp225

+

Boc-Gly-OH

+

furfurylamine

+

piperonal



n-butyl isocyanide

Reaction ID UCEXP225-3 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.888 M Precipitate Yes Product Pending Comments 0.5 mmol of isocyanide was added to 500uL of a 2M solution of aldehyde; amine and acid Reference http://usefulchem.wikispaces.com/Exp225

481

24528158

+

Boc-Gly-OH

+

furfurylamine

+

piperonal



1-pentyl isocyanide

24528159

Reaction ID UCEXP225-4 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.889 M Precipitate Yes Product Pending Comments 0.5 mmol of isocyanide was added to 500uL of a 2M solution of aldehyde; amine and acid Reference http://usefulchem.wikispaces.com/Exp225

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

+

Boc-Gly-OH

+

furfurylamine

+

piperonal



cyclohexylisocyanide

24528160

Reaction ID UCEXP225-5 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.891 M Precipitate Yes Product Pending Comments 0.5 mmol of isocyanide was added to 500uL of a 2M solution of aldehyde; amine and acid Reference http://usefulchem.wikispaces.com/Exp225

+

Boc-Gly-OH

+

furfurylamine

+

piperonal



benzyl isocyanide

24528161

Reaction ID UCEXP225-6 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.438 M Precipitate No Comments 0.5 mmol of isocyanide was added to 500uL of a 2M solution of aldehyde; amine and acid Reference http://usefulchem.wikispaces.com/Exp225

+

Boc-Gly-OH

+

furfurylamine

+

piperonal



tosylmethyl isocyanide

Reaction ID UCEXP225-7 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.879 M Precipitate No Comments 0.5 mmol of isocyanide was added to 500uL of a 2M solution of aldehyde; amine and acid Reference http://usefulchem.wikispaces.com/Exp225

482

24528162

+

Boc-Gly-OH

+

furfurylamine

+



2-morpholinoethyl isocyanide

piperonal

24528163

Reaction ID UCEXP225-8 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.868 M Precipitate No Comments 0.5 mmol of isocyanide was added to 500uL of a 2M solution of aldehyde; amine and acid Reference http://usefulchem.wikispaces.com/Exp225

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

+

Boc-Gly-OH

+

furfurylamine

+



2-chloro-6methylphenyl isocyanide

piperonal

24528164

Reaction ID UCEXP227-1 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 0.261 M Precipitate No Comments 0.5 mmol of isocyanide was added to 500uL of a 0.5M solution of aldehyde; amine and acid Reference http://usefulchem.wikispaces.com/Exp227

+

1-pyrenebutyric acid

+

furfurylamine

+

piperonal



t-butyl isocyanide

24528173

Reaction ID UCEXP227-2 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 0.453 M Precipitate No Comments 0.5 mmol of isocyanide was added to 500uL of a 0.5M solution of aldehyde; amine and acid Reference http://usefulchem.wikispaces.com/Exp227

+

1-pyrenebutyric acid

+

furfurylamine

+

piperonal



n-butyl isocyanide

Reaction ID UCEXP227-3 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 0.444 M Precipitate No Comments 0.5 mmol of isocyanide was added to 500uL of a 0.5M solution of aldehyde; amine and acid Reference http://usefulchem.wikispaces.com/Exp227

483

24528174

+

1-pyrenebutyric acid

+

furfurylamine

+

piperonal



1-pentyl isocyanide

24528175

Reaction ID UCEXP227-4 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 0.445 M Precipitate No Comments 0.5 mmol of isocyanide was added to 500uL of a 0.5M solution of aldehyde; amine and acid Reference http://usefulchem.wikispaces.com/Exp227

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

+

1-pyrenebutyric acid

+

furfurylamine

+

piperonal



cyclohexylisocyanide

24528176

Reaction ID UCEXP227-5 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 0.446 M Precipitate No Comments 0.5 mmol of isocyanide was added to 500uL of a 0.5M solution of aldehyde; amine and acid Reference http://usefulchem.wikispaces.com/Exp227

+

1-pyrenebutyric acid

+

furfurylamine

+

piperonal



benzyl isocyanide

24528177

Reaction ID UCEXP227-6 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 0.251 M Precipitate No Comments 0.5 mmol of isocyanide was added to 500uL of a 0.5M solution of aldehyde; amine and acid Reference http://usefulchem.wikispaces.com/Exp227

+

1-pyrenebutyric acid

+

furfurylamine

+

piperonal



tosylmethyl isocyanide

Reaction ID UCEXP227-7 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 0.439 M Precipitate No Comments 0.5 mmol of isocyanide was added to 500uL of a 0.5M solution of aldehyde; amine and acid Reference http://usefulchem.wikispaces.com/Exp227

484

24528178

+

1-pyrenebutyric acid

+

furfurylamine

+



2-morpholinoethyl isocyanide

piperonal

24528179

Reaction ID UCEXP227-8 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 0.434 M Precipitate No Comments 0.5 mmol of isocyanide was added to 500uL of a 0.5M solution of aldehyde; amine and acid Reference http://usefulchem.wikispaces.com/Exp227

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

+

1-pyrenebutyric acid

+

furfurylamine

+



2-chloro-6methylphenyl isocyanide

piperonal

24528180

Reaction ID UCExp245-01 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.509 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp245

+

3,4methylenedioxyphenylacetic acid

+

furfurylamine

+

piperonal



n-butyl isocyanide

24528391

Reaction ID UCExp245-02 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.718 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp245

+

3,4methylenedioxyphenylacetic acid

+

furfurylamine

+

piperonal

Reaction ID UCExp245-03 Researcher Reaction Type Solvent

Khalid Mirza Ugi methanol

485



n-butyl isocyanide

24528391

Limiting Reactant 0.504 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp245

+

3,4methylenedioxyphenylacetic acid

+

5-methylfurfurylamine

+

piperonal



n-butyl isocyanide

24528392

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCExp245-04 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.706 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp245

+

3,4methylenedioxyphenylacetic acid

+

5-methylfurfurylamine

+

piperonal



n-butyl isocyanide

24528392

Reaction ID UCExp245-05 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.507 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp245

+

3,4methylenedioxyphenylacetic acid

+

furfurylamine

+

piperonal



t-butyl isocyanide

24528393

Reaction ID UCExp245-06 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.714 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp245

+

3,4methylenedioxyphenylacetic acid

+

furfurylamine

+

piperonal

486



t-butyl isocyanide

24528393

Reaction ID UCExp245-07 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.504 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp245

+

3,4methylenedioxyphenylacetic acid

+

furfurylamine

+

piperonal



cyclohexylisocyanide

24528394

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCExp245-08 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.708 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp245

+

3,4methylenedioxyphenylacetic acid

+

furfurylamine

+

piperonal



cyclohexylisocyanide

24528394

Reaction ID UCExp245-09 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.492 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp245

+

3,4methylenedioxyphenylacetic acid

+

furfurylamine

+



1,1,3,3tetramethylbutyl isocyanide

piperonal

24528395

Reaction ID UCExp245-10 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.683 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp245

+

+

+

487



3,4methylenedioxyphenylacetic acid

furfurylamine

1,1,3,3tetramethylbutyl isocyanide

piperonal

24528395

Reaction ID UCExp245-11

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.504 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp245

+

3,4methylenedioxyphenylacetic acid

+

5-methylfurfurylamine

+

piperonal



t-butyl isocyanide

24528396

Reaction ID UCExp245-12 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.706 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp245

+

3,4methylenedioxyphenylacetic acid

+

5-methylfurfurylamine

+

piperonal



t-butyl isocyanide

24528396

Reaction ID UCExp245-13 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.499 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp245

+

3,4methylenedioxyphenylacetic acid

+

5-methylfurfurylamine

+

piperonal

Reaction ID UCExp245-14 Researcher Reaction Type

Khalid Mirza Ugi

488



cyclohexylisocyanide

24528397

Solvent methanol Limiting Reactant 0.696 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp245

+

3,4methylenedioxyphenylacetic acid

+

5-methylfurfurylamine

+

piperonal



cyclohexylisocyanide

24528397

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCExp245-15 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.486 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp245

+

3,4methylenedioxyphenylacetic acid

+

5-methylfurfurylamine

+



1,1,3,3tetramethylbutyl isocyanide

piperonal

24528398

Reaction ID UCExp245-16 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.673 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp245

+

3,4methylenedioxyphenylacetic acid

+

5-methylfurfurylamine

+



1,1,3,3tetramethylbutyl isocyanide

piperonal

24528398

Reaction ID UCExp245-17 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.502 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp245

+

cbz-proline

+

furfurylamine

+

piperonal

489



n-butyl isocyanide

24528399

Reaction ID UCExp245-18 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.12 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp245

+

cbz-proline

+

furfurylamine

+

piperonal



n-butyl isocyanide

24528399

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCExp245-19 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.496 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp245

+

cbz-proline

+

5-methylfurfurylamine

+

piperonal



n-butyl isocyanide

24528400

Reaction ID UCExp245-20 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.092 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp245

+

cbz-proline

+

5-methylfurfurylamine

+

piperonal



n-butyl isocyanide

24528400

Reaction ID UCExp245-21 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.5 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp245

+

cbz-proline

+

furfurylamine

+

piperonal

Reaction ID UCExp245-22

490



t-butyl isocyanide

24528401

Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.109 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp245

+

cbz-proline

+

furfurylamine

+

piperonal



t-butyl isocyanide

24528401

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCExp245-23 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.497 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp245

+

cbz-proline

+

furfurylamine

+

piperonal



cyclohexylisocyanide

24528402

Reaction ID UCExp245-24 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.096 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp245

+

cbz-proline

+

furfurylamine

+

piperonal



cyclohexylisocyanide

24528402

Reaction ID UCExp245-25 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.509 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp245

+

cbz-proline

+

furfurylamine

+

piperonal

Reaction ID UCExp245-26

491



1,1,3,3tetramethylbutyl isocyanide

24528403

Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.038 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp245

+

cbz-proline

+

furfurylamine

+



1,1,3,3tetramethylbutyl isocyanide

piperonal

24528403

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCExp245-27 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.494 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp245

+

cbz-proline

+

5-methylfurfurylamine

+

piperonal



t-butyl isocyanide

24528404

Reaction ID UCExp245-28 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.082 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp245

+

cbz-proline

+

5-methylfurfurylamine

+

piperonal



t-butyl isocyanide

24528404

Reaction ID UCExp245-29 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.503 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp245

+

cbz-proline

+

5-methylfurfurylamine

+

piperonal

492



1,1,3,3tetramethylbutyl isocyanide

24528405

Reaction ID UCExp245-30 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.013 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp245

+

cbz-proline

+

5-methylfurfurylamine

+



1,1,3,3tetramethylbutyl isocyanide

piperonal

24528405

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCExp245-31 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.504 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp245

+

cbz-proline

+

5-methylfurfurylamine

+

piperonal



cyclohexylisocyanide

24528406

Reaction ID UCExp245-32 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.002 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp245

+

cbz-proline

+

5-methylfurfurylamine

+

piperonal



cyclohexylisocyanide

24528406

Reaction ID UCExp245-33 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.507 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp245

+

3,4methylenedioxyphenylacetic acid

+

furfurylamine

+

piperonal

493



t-butyl isocyanide

24528407

Reaction ID UCExp245-34 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.714 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp245

+

3,4methylenedioxyphenylacetic acid

+

furfurylamine

+

piperonal



t-butyl isocyanide

24528407

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCExp245-35 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.492 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp245

+

3,4methylenedioxyphenylacetic acid

+

furfurylamine

+



1,1,3,3tetramethylbutyl isocyanide

piperonal

24528408

Reaction ID UCExp245-36 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.683 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp245

+

3,4methylenedioxyphenylacetic acid

+

furfurylamine

+



1,1,3,3tetramethylbutyl isocyanide

piperonal

24528408

Reaction ID UCExp245-37 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.509 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp245

+

+

+

494



3,4methylenedioxyphenylacetic acid

furfurylamine

piperonal

n-butyl isocyanide

24528409

Reaction ID UCExp245-38

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.718 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp245

+

3,4methylenedioxyphenylacetic acid

+

furfurylamine

+

piperonal



n-butyl isocyanide

24528409

Reaction ID UCExp245-39 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.504 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp245

+

3,4methylenedioxyphenylacetic acid

+

5-methylfurfurylamine

+

piperonal



n-butyl isocyanide

24528410

Reaction ID UCExp245-40 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.706 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp245

+

3,4methylenedioxyphenylacetic acid

+

5-methylfurfurylamine

+

piperonal

salicylic acid 495



n-butyl isocyanide

24528410

Reaction ID UCEXP158B-V1B16 Researcher Emily Messner Reaction Type Ugi Solvent methanol Limiting Reactant 0.658 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp158

+

salicylic acid

+

5-methylfurfurylamine

+

4-chlorobenzaldehyde



tosylmethyl isocyanide

21106076

t-butyl isocyanide Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCEXP052E Researcher Alicia Holsey Reaction Type Ugi Solvent methanol Limiting Reactant 0.223 M Precipitate Yes Yield 32 % Comments 1M solutions of the starting materials was made Reference http://usefulchem.wikispaces.com/Exp052

+

Boc-Gly-OH

+

5-methylfurfurylamine

+

piperonal



t-butyl isocyanide

10481872

Reaction ID UCEXP086B Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.402 M Precipitate Yes Yield 38 % Comments Solution was made up to 4 mL - methanol amount probably closer to 3 mL Reference http://usefulchem.wikispaces.com/Exp086

+

Boc-Gly-OH

+

5-methylfurfurylamine

+

benzaldehyde

Reaction ID UCEXP099C Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.405 M Precipitate Yes Yield 47.2 % Comments Solution was made up to 4 mL - methanol amount probably closer to 3 mL Reference http://usefulchem.wikispaces.com/Exp099

496



t-butyl isocyanide

10481766

+

Boc-Gly-OH

+

+

furfurylamine

benzaldehyde



t-butyl isocyanide

21106059

Reaction ID UCEXP104C Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.398 M Precipitate Yes Yield 12 % Comments Imine was preformed Reference http://usefulchem.wikispaces.com/Exp104

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

+

Boc-Gly-OH

+

+

furfurylamine

veratraldehyde



t-butyl isocyanide

21106057

Reaction ID UCEXP147-3V2B6 Researcher Mitesh Shah Reaction Type Ugi Solvent methanol Limiting Reactant 0.662 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp+147

+

1-pyrenebutyric acid

+

methylamine

+

2-naphthaldehyde



t-butyl isocyanide

21105841

Reaction ID UCEXP148A-V1B153 Researcher Khalid Mirza/ Emily Messner Reaction Type Ugi Solvent methanol Limiting Reactant 0.398 M Precipitate Yes but the aldehyde alone is not soluble in methanol Yield 50.1 % Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp148

+

crotonic acid

+

1-heptylamine

+

phenanthrene-9-carboxaldehyde

Reaction ID UCEXP150D-V1B155 Researcher Khalid Mirza/ Emily Messner Reaction Type Ugi Solvent methanol Limiting Reactant 0.404 M Precipitate Yes but the aldehyde alone is not soluble in methanol Yield 59 % Comments Protocol from Explan005 followed

497



t-butyl isocyanide

21106058

Reference

http://usefulchem.wikispaces.com/Exp150

+

+

crotonic acid

benzylamine

+

phenanthrene-9-carboxaldehyde



t-butyl isocyanide

21105601

Reaction ID UCEXP155B-V1B159 Researcher Emily Messner Reaction Type Ugi Solvent methanol Limiting Reactant 0.674 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp155

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

+

3-(4methoxyphenyl)propionic acid

+

+

5-methylfurfurylamine

benzaldehyde



t-butyl isocyanide

21106074

Reaction ID UCEXP156B-V1B155 Researcher Emily Messner Reaction Type Ugi Solvent methanol Limiting Reactant 0.678 M Precipitate Yes but reactants initially insoluble Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp156

+

crotonic acid

+

benzylamine

+

phenanthrene-9-carboxaldehyde



t-butyl isocyanide

21106075

Reaction ID UCEXP162 Researcher Shannon Oseback Reaction Type Ugi Solvent methanol Limiting Reactant 0.285 M Precipitate Reactants Insoluble Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp162

+

phenylacetic acid

+

cyclohexylamine

+

phenanthrene-9-carboxaldehyde

Reaction ID UCEXP163A-V1B14 Researcher Tim Bohinsky Reaction Type Ugi Solvent methanol Limiting Reactant 0.387 M Precipitate no and aldehyde alone not solube Comments Protocol from Explan005 followed

498



t-butyl isocyanide

21105590

Reference

http://usefulchem.wikispaces.com/Exp163

+

+

mandelic acid

furfurylamine

+

phenanthrene-9-carboxaldehyde



t-butyl isocyanide

21105596

Reaction ID UCEXP171B/V2B2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.219 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp171

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

+

1-pyrenebutyric acid

+

5-methylfurfurylamine

+

o-vanillin



t-butyl isocyanide

21106056

Reaction ID UCEXP171D/V2B4 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.219 M Precipitate Yes Product No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp171

+

1-pyrenebutyric acid

+

benzylamine

+

o-vanillin



t-butyl isocyanide

21105846

Reaction ID UCEXP171FV2B6 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.222 M Precipitate Yes but reactants initially insoluble Yield - % Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp171

+

1-pyrenebutyric acid

+

methylamine

+

2-naphthaldehyde

Reaction ID UCEXP171KV2B11 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.222 M Precipitate Yes Yield - %

499



t-butyl isocyanide

21105841

Comments Reference

Protocol from Explan005 followed http://usefulchem.wikispaces.com/Exp171

+

1-pyrenebutyric acid

+

methylamine

+

4-(dimethylamino)benzaldehyde



t-butyl isocyanide

21105842

Reaction ID UCEXP171LV2B-12

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.22 M Precipitate Reactants Insoluble Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp171

+

1-pyrenebutyric acid

+

methylamine

+

phenanthrene-9-carboxaldehyde



t-butyl isocyanide

21106039

Reaction ID UCEXP173B/V2B14 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.223 M Precipitate Yes but reactants initially insoluble Yield - % Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp173

+

1-pyrenebutyric acid

+

+

methylamine

4-methylbenzaldehyde



t-butyl isocyanide

21105844

Reaction ID UCEXP173C/V2B15 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.222 M Precipitate Reactants Insoluble Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp173

+

1-pyrenebutyric acid

+

methylamine

+

4-(trifluoromethyl)benzaldehyde

Reaction ID UCEXP173E/V2B17 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.223 M Precipitate No Comments Protocol from Explan005 followed

500



t-butyl isocyanide

21106044

Reference

http://usefulchem.wikispaces.com/Exp173

+

Boc-Trp-OH

+

methylamine

+

3,4-dihydroxybenzaldehyde



t-butyl isocyanide

21106045

Reaction ID UCEXP173F/V2B18 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.219 M Precipitate no and aldehyde alone not solube Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp173

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

+

2,3-dihydroxybenzoic acid

+

furfurylamine

+

phenanthrene-9-carboxaldehyde



t-butyl isocyanide

21106041

Reaction ID UCEXP173J/V2B22 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.224 M Precipitate Reactants Insoluble Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp173

+

1-pyrenebutyric acid

+

methylamine

+

3,4-dihydroxybenzaldehyde



t-butyl isocyanide

21106038

Reaction ID UCEXP173P/V2B28 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.222 M Precipitate Reactants Insoluble Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp173

+

1-pyrenebutyric acid

+

methylamine

+

3-methoxybenzaldehyde

Reaction ID UCEXP174O/V2B47 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.223 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp174

501



t-butyl isocyanide

21106050

+

D-(−)-Quinic acid

+

5-methylfurfurylamine

+

3,5-dimethoxybenzaldehyde



t-butyl isocyanide

21106186

Reaction ID UCEXP179 Researcher Shannon Oseback Reaction Type Ugi Solvent methanol Limiting Reactant 0.286 M Precipitate Reactants Insoluble Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp179

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

+

4-chlorophenylacetic acid

+

aniline

+

phenanthrene-9-carboxaldehyde



t-butyl isocyanide

21105833

Reaction ID UCEXP181-065V2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.223 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

+

D-(−)-Quinic acid

+

benzylamine

+

3,5-dimethoxybenzaldehyde



t-butyl isocyanide

24528104

Reaction ID UCEXP181-073V2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.222 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

+

Boc-Trp-OH

+

methylamine

+

benzaldehyde

Reaction ID UCEXP181-074V2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.226 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

502



t-butyl isocyanide

24528109

+

3,4-dihydroxyphenylacetic acid

+

aniline

+

3,4-dihydroxybenzaldehyde



t-butyl isocyanide

24528110

Reaction ID UCEXP181-078V2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.219 M Precipitate Reactants Insoluble Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

+

1-pyrenebutyric acid

+

1-hexylamine

+

2-hydroxybenzaldehyde



t-butyl isocyanide

24528114

Reaction ID UCEXP181-079V2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.218 M Precipitate Reactants Insoluble Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

+

2,4,6-trihydroxybenzoic acid

+

furfurylamine

+

phenanthrene-9-carboxaldehyde



t-butyl isocyanide

24528115

Reaction ID UCEXP181-081V2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.224 M Precipitate Reactants Insoluble Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

+

3,4-dihydroxyphenylacetic acid

+

2-chloroaniline

+

2-naphthaldehyde

Reaction ID UCEXP181-087V2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.222 M Precipitate Reactants Insoluble Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

503



t-butyl isocyanide

24528117

+

1-pyrenebutyric acid

+

methylamine

+

2,4-dimethylbenzaldehyde



t-butyl isocyanide

21106206

Reaction ID UCEXP181-111V2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.226 M Precipitate Reactants Insoluble Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

+

2,4,6-trihydroxybenzoic acid

+

methylamine

+

phenanthrene-9-carboxaldehyde



t-butyl isocyanide

24528534

Reaction ID UCEXP181-115V2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.224 M Precipitate Reactants Insoluble Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

+

3,4-dihydroxyphenylacetic acid

+

+

3-chloroaniline

2-naphthaldehyde



t-butyl isocyanide

24528144

Reaction ID UCEXP183-049V1 Researcher Emily Messner Reaction Type Ugi Solvent methanol Limiting Reactant 0.398 M Precipitate Reactants Insoluble Comments Reference http://usefulchem.wikispaces.com/Exp183

+

mandelic acid

+

cyclohexylamine

+

phenanthrene-9-carboxaldehyde

Reaction ID UCEXP184-1/49 Researcher Emily Messner Reaction Type Ugi Solvent ethanol Limiting Reactant 0.398 M Precipitate Reactants insoluble Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp184

504



t-butyl isocyanide

24528153

+

mandelic acid

+

cyclohexylamine

+

phenanthrene-9-carboxaldehyde



t-butyl isocyanide

24528154

Reaction ID UCEXP184-2/49 Researcher Emily Messner Reaction Type Ugi Solvent acetonitrile Limiting Reactant 0.398 M Precipitate Reactants insoluble Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp184

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

+

mandelic acid

+

cyclohexylamine

+

phenanthrene-9-carboxaldehyde



t-butyl isocyanide

24528154

Reaction ID UCEXP184-3/49 Researcher Emily Messner Reaction Type Ugi Solvent dichloromethane Limiting Reactant 0.398 M Precipitate Reactants insoluble Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp184

+

mandelic acid

+

cyclohexylamine

+

phenanthrene-9-carboxaldehyde



t-butyl isocyanide

24528154

Reaction ID UCEXP185-1 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.409 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp185

+

methacrylic acid

+

5-methylfurfurylamine

+

4-(trifluoromethyl)benzaldehyde

Reaction ID UCEXP185-2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.409 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp185

505



t-butyl isocyanide

21111670

+

methacrylic acid

+

benzylamine

+

4-(trifluoromethyl)benzaldehyde



t-butyl isocyanide

21111671

Reaction ID UCEXP187-1 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.057 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp187

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

+

methacrylic acid

+

5-methylfurfurylamine

+

4-(trifluoromethyl)benzaldehyde



t-butyl isocyanide

21111670

Reaction ID UCEXP187-2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.06 M Precipitate Yes Yield - % Comments Reference http://usefulchem.wikispaces.com/Exp187

+

methacrylic acid

+

benzylamine

+

4-(trifluoromethyl)benzaldehyde



t-butyl isocyanide

21111671

Reaction ID UCEXP187-3 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.064 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp187

+

methacrylic acid

+

t-butylamine

+

4-(trifluoromethyl)benzaldehyde

Reaction ID UCEXP188-1 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.225 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp188

506



t-butyl isocyanide

21143155

+

methacrylic acid

+

5-methylfurfurylamine

+

4-(trifluoromethyl)benzaldehyde



t-butyl isocyanide

21111670

Reaction ID UCEXP188-2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.225 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp188

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

+

methacrylic acid

+

benzylamine

+

4-(trifluoromethyl)benzaldehyde



t-butyl isocyanide

21111671

Reaction ID UCEXP188-3 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.225 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp188

+

methacrylic acid

+

t-butylamine

+

4-(trifluoromethyl)benzaldehyde



t-butyl isocyanide

21143155

Reaction ID UCEXP201-01 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.039 M Precipitate Yes Yield 50.73 % Comments Automated liquid handling Reference http://usefulchem.wikispaces.com/Exp201

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde

Reaction ID UCEXP201-02 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.019 M Precipitate Yes Yield 59.07 % Comments Automated liquid handling Reference http://usefulchem.wikispaces.com/Exp201

507



t-butyl isocyanide

21106059

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde



t-butyl isocyanide

21106059

Reaction ID UCEXP201-03 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.018 M Precipitate Yes Yield 61.55 % Comments Automated liquid handling Reference http://usefulchem.wikispaces.com/Exp201

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde



t-butyl isocyanide

21106059

Reaction ID UCEXP201-04 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.007 M Precipitate Yes Yield 60.31 % Comments Automated liquid handling Reference http://usefulchem.wikispaces.com/Exp201

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde



t-butyl isocyanide

21106059

Reaction ID UCEXP201-05 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.015 M Precipitate Yes Yield 60.2 % Comments Automated liquid handling Reference http://usefulchem.wikispaces.com/Exp201

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde

Reaction ID UCEXP201-06 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.998 M Precipitate Yes Yield 69.22 %

508



t-butyl isocyanide

21106059

Comments Reference

Automated liquid handling http://usefulchem.wikispaces.com/Exp201

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde



t-butyl isocyanide

21106059

Reaction ID UCEXP201-07

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.289 M Precipitate Yes Yield 52.42 % Comments Automated liquid handling Reference http://usefulchem.wikispaces.com/Exp201

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde



t-butyl isocyanide

21106059

Reaction ID UCEXP201-08 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.287 M Precipitate Yes Yield 44.64 % Comments Automated liquid handling Reference http://usefulchem.wikispaces.com/Exp201

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde



t-butyl isocyanide

21106059

Reaction ID UCEXP201-09 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.287 M Precipitate Yes Yield 50.28 % Comments Automated liquid handling Reference http://usefulchem.wikispaces.com/Exp201

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde

Reaction ID UCEXP201-10 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.286 M

509



t-butyl isocyanide

21106059

Precipitate Yield Comments Reference

Yes 54.79 % Automated liquid handling http://usefulchem.wikispaces.com/Exp201

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde



t-butyl isocyanide

21106059

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCEXP201-11 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.287 M Precipitate Yes Yield 53.43 % Comments Automated liquid handling Reference http://usefulchem.wikispaces.com/Exp201

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde



t-butyl isocyanide

21106059

Reaction ID UCEXP201-12 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.286 M Precipitate Yes Yield 54.67 % Comments Automated liquid handling Reference http://usefulchem.wikispaces.com/Exp201

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde



t-butyl isocyanide

21106059

Reaction ID UCEXP201-13 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.074 M Precipitate Yes Yield 0.34 % Comments Automated liquid handling Reference http://usefulchem.wikispaces.com/Exp201

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde

510



t-butyl isocyanide

21106059

Reaction ID UCEXP201-14 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.074 M Precipitate Yes Yield 1.35 % Comments Automated liquid handling Reference http://usefulchem.wikispaces.com/Exp201

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde



t-butyl isocyanide

21106059

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCEXP201-15 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.074 M Precipitate Yes Yield 10.37 % Comments Automated liquid handling Reference http://usefulchem.wikispaces.com/Exp201

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde



t-butyl isocyanide

21106059

Reaction ID UCEXP201-16 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.074 M Precipitate Yes Yield 16.35 % Comments Automated liquid handling Reference http://usefulchem.wikispaces.com/Exp201

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde



t-butyl isocyanide

21106059

Reaction ID UCEXP201-17 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.074 M Precipitate Yes Yield 8.68 % Comments Automated liquid handling Reference http://usefulchem.wikispaces.com/Exp201

+

+

+

511



Boc-Gly-OH

furfurylamine

benzaldehyde

t-butyl isocyanide

21106059

Reaction ID UCEXP201-18 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.074 M Precipitate Yes Yield 5.64 % Comments Automated liquid handling Reference http://usefulchem.wikispaces.com/Exp201

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde



t-butyl isocyanide

21106059

Reaction ID UCEXP201-19 Researcher Khalid Mirza Reaction Type Ugi Solvent ethanol Limiting Reactant 0.289 M Precipitate Yes Yield 51.52 % Comments Automated liquid handling Reference http://usefulchem.wikispaces.com/Exp201

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde



t-butyl isocyanide

21106059

Reaction ID UCEXP201-20 Researcher Khalid Mirza Reaction Type Ugi Solvent ethanol Limiting Reactant 0.287 M Precipitate Yes Yield 46.78 % Comments Automated liquid handling Reference http://usefulchem.wikispaces.com/Exp201

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde

Reaction ID UCEXP201-21 Researcher Khalid Mirza Reaction Type Ugi Solvent ethanol Limiting Reactant 0.287 M Precipitate Yes Yield 51.29 %

512



t-butyl isocyanide

21106059

Comments Reference

Automated liquid handling http://usefulchem.wikispaces.com/Exp201

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde



t-butyl isocyanide

21106059

Reaction ID UCEXP201-22

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Researcher Khalid Mirza Reaction Type Ugi Solvent ethanol Limiting Reactant 0.286 M Precipitate Yes Yield 54.11 % Comments Automated liquid handling Reference http://usefulchem.wikispaces.com/Exp201

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde



t-butyl isocyanide

21106059

Reaction ID UCEXP201-23 Researcher Khalid Mirza Reaction Type Ugi Solvent ethanol Limiting Reactant 0.287 M Precipitate Yes Yield 55.91 % Comments Automated liquid handling Reference http://usefulchem.wikispaces.com/Exp201

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde



t-butyl isocyanide

21106059

Reaction ID UCEXP201-24 Researcher Khalid Mirza Reaction Type Ugi Solvent ethanol Limiting Reactant 0.286 M Precipitate Yes Yield 58.28 % Comments Automated liquid handling Reference http://usefulchem.wikispaces.com/Exp201

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde

Reaction ID UCEXP201-25 Researcher Khalid Mirza Reaction Type Ugi Solvent ethanol Limiting Reactant 0.074 M

513



t-butyl isocyanide

21106059

Precipitate Yield Comments Reference

Yes 1.24 % Automated liquid handling http://usefulchem.wikispaces.com/Exp201

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde



t-butyl isocyanide

21106059

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCEXP201-26 Researcher Khalid Mirza Reaction Type Ugi Solvent ethanol Limiting Reactant 0.074 M Precipitate Yes Yield 2.25 % Comments Automated liquid handling Reference http://usefulchem.wikispaces.com/Exp201

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde



t-butyl isocyanide

21106059

Reaction ID UCEXP201-27 Researcher Khalid Mirza Reaction Type Ugi Solvent ethanol Limiting Reactant 0.074 M Precipitate Yes Yield 7.78 % Comments Automated liquid handling Reference http://usefulchem.wikispaces.com/Exp201

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde



t-butyl isocyanide

21106059

Reaction ID UCEXP201-28 Researcher Khalid Mirza Reaction Type Ugi Solvent ethanol Limiting Reactant 0.074 M Precipitate Yes Yield 1.13 % Comments Automated liquid handling Reference http://usefulchem.wikispaces.com/Exp201

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde

514



t-butyl isocyanide

21106059

Reaction ID UCEXP201-29 Researcher Khalid Mirza Reaction Type Ugi Solvent ethanol Limiting Reactant 0.074 M Precipitate Yes Yield 0.79 % Comments Automated liquid handling Reference http://usefulchem.wikispaces.com/Exp201

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde



t-butyl isocyanide

21106059

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCEXP201-30 Researcher Khalid Mirza Reaction Type Ugi Solvent ethanol Limiting Reactant 0.074 M Precipitate Yes Yield 0.23 % Comments Automated liquid handling Reference http://usefulchem.wikispaces.com/Exp201

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde



t-butyl isocyanide

21106059

Reaction ID UCEXP201-31 Researcher Khalid Mirza Reaction Type Ugi Solvent acetonitrile Limiting Reactant 0.289 M Precipitate Yes Yield 39.23 % Comments Automated liquid handling Reference http://usefulchem.wikispaces.com/Exp201

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde



t-butyl isocyanide

21106059

Reaction ID UCEXP201-32 Researcher Khalid Mirza Reaction Type Ugi Solvent acetonitrile Limiting Reactant 0.287 M Precipitate Yes Yield 40.58 % Comments Automated liquid handling Reference http://usefulchem.wikispaces.com/Exp201

+

+

+

515



Boc-Gly-OH

furfurylamine

benzaldehyde

t-butyl isocyanide

21106059

Reaction ID UCEXP201-33 Researcher Khalid Mirza Reaction Type Ugi Solvent acetonitrile Limiting Reactant 0.287 M Precipitate Yes Yield 43.85 % Comments Automated liquid handling Reference http://usefulchem.wikispaces.com/Exp201

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde



t-butyl isocyanide

21106059

Reaction ID UCEXP201-34 Researcher Khalid Mirza Reaction Type Ugi Solvent acetonitrile Limiting Reactant 0.286 M Precipitate Yes Yield 35.4 % Comments Automated liquid handling Reference http://usefulchem.wikispaces.com/Exp201

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde



t-butyl isocyanide

21106059

Reaction ID UCEXP201-35 Researcher Khalid Mirza Reaction Type Ugi Solvent acetonitrile Limiting Reactant 0.287 M Precipitate Yes Yield 41.37 % Comments Automated liquid handling Reference http://usefulchem.wikispaces.com/Exp201

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde

Reaction ID UCEXP201-36 Researcher Khalid Mirza Reaction Type Ugi Solvent acetonitrile Limiting Reactant 0.286 M Precipitate Yes Yield 39.23 %

516



t-butyl isocyanide

21106059

Comments Reference

Automated liquid handling http://usefulchem.wikispaces.com/Exp201

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde



t-butyl isocyanide

21106059

Reaction ID UCEXP201-37

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Researcher Khalid Mirza Reaction Type Ugi Solvent acetonitrile Limiting Reactant 0.074 M Precipitate Yes Yield 0.68 % Comments Automated liquid handling Reference http://usefulchem.wikispaces.com/Exp201

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde



t-butyl isocyanide

21106059

Reaction ID UCEXP201-38 Researcher Khalid Mirza Reaction Type Ugi Solvent acetonitrile Limiting Reactant 0.074 M Precipitate Yes Yield 1.8 % Comments Automated liquid handling Reference http://usefulchem.wikispaces.com/Exp201

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde



t-butyl isocyanide

21106059

Reaction ID UCEXP201-39 Researcher Khalid Mirza Reaction Type Ugi Solvent acetonitrile Limiting Reactant 0.002 M Precipitate Yes Yield 1.01 % Comments Automated liquid handling Reference http://usefulchem.wikispaces.com/Exp201

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde

Reaction ID UCEXP201-40 Researcher Khalid Mirza Reaction Type Ugi Solvent acetonitrile Limiting Reactant 0.074 M

517



t-butyl isocyanide

21106059

Precipitate Yield Comments Reference

Yes 0.9 % Automated liquid handling http://usefulchem.wikispaces.com/Exp201

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde



t-butyl isocyanide

21106059

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCEXP201-41 Researcher Khalid Mirza Reaction Type Ugi Solvent acetonitrile Limiting Reactant 0.074 M Precipitate Yes Yield 1.01 % Comments Automated liquid handling Reference http://usefulchem.wikispaces.com/Exp201

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde



t-butyl isocyanide

21106059

Reaction ID UCEXP201-42 Researcher Khalid Mirza Reaction Type Ugi Solvent acetonitrile Limiting Reactant 0.074 M Precipitate Yes Yield 0.45 % Comments Automated liquid handling Reference http://usefulchem.wikispaces.com/Exp201

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde



t-butyl isocyanide

21106059

Reaction ID UCEXP201-43 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 0.289 M Precipitate Yes Yield 6.54 % Comments Automated liquid handling Reference http://usefulchem.wikispaces.com/Exp201

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde

518



t-butyl isocyanide

21106059

Reaction ID UCEXP201-44 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 0.287 M Precipitate Yes Yield 7.89 % Comments Automated liquid handling Reference http://usefulchem.wikispaces.com/Exp201

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde



t-butyl isocyanide

21106059

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCEXP201-45 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 0.287 M Precipitate Yes Yield 10.03 % Comments Automated liquid handling Reference http://usefulchem.wikispaces.com/Exp201

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde



t-butyl isocyanide

21106059

Reaction ID UCEXP201-46 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 0.286 M Precipitate Yes Yield 9.92 % Comments Automated liquid handling Reference http://usefulchem.wikispaces.com/Exp201

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde



t-butyl isocyanide

21106059

Reaction ID UCEXP201-47 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 0.287 M Precipitate Yes Yield 7.44 % Comments Automated liquid handling Reference http://usefulchem.wikispaces.com/Exp201

+

+

+

519



Boc-Gly-OH

furfurylamine

benzaldehyde

t-butyl isocyanide

21106059

Reaction ID UCEXP201-48 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 0.286 M Precipitate Yes Yield 12.06 % Comments Automated liquid handling Reference http://usefulchem.wikispaces.com/Exp201

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

+

Boc-Gly-OH

+

+

furfurylamine

benzaldehyde



t-butyl isocyanide

21106059

Reaction ID UCEXP214C Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.404 M Precipitate Yes but the aldehyde alone is not soluble in methanol Yield - % Comments Reference http://usefulchem.wikispaces.com/Exp214

+

+

crotonic acid

benzylamine

+

phenanthrene-9-carboxaldehyde



t-butyl isocyanide

21105601

Reaction ID UCEXP215A Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 0.661 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp215

+

crotonic acid

+

1-heptylamine

+

phenanthrene-9-carboxaldehyde

Reaction ID UCEXP215B Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 0.678 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp215

520



t-butyl isocyanide

21106058

+

+

crotonic acid

benzylamine

+

phenanthrene-9-carboxaldehyde



t-butyl isocyanide

21105601

Reaction ID UCEXP215C Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 0.662 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp215

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

+

1-pyrenebutyric acid

+

+

methylamine

2-naphthaldehyde



t-butyl isocyanide

21105841

Reaction ID UCEXP215D Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 0.66 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp215

+

1-pyrenebutyric acid

+

methylamine

+

4-(dimethylamino)benzaldehyde



t-butyl isocyanide

21105842

Reaction ID UCEXP215E Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 0.715 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp215

+

4-chlorophenylacetic acid

+

methylamine

+

4-methylbenzaldehyde

Reaction ID UCEXP217-2 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 0.383 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp217

521



t-butyl isocyanide

24528155

+

crotonic acid

+

benzylamine

+

phenanthrene-9-carboxaldehyde



t-butyl isocyanide

21105601

Reaction ID UCEXP217-3 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 0.383 M Precipitate Yes Product Pending Comments Reference http://usefulchem.wikispaces.com/Exp217

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde



t-butyl isocyanide

21106059

Reaction ID UCEXP217-4 Researcher Khalid Mirza Reaction Type Ugi Solvent DMSO Limiting Reactant 0.383 M Precipitate Yes Product Pending Comments Reference http://usefulchem.wikispaces.com/Exp217

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde



t-butyl isocyanide

21106059

Reaction ID UCEXP222-1 Researcher Khalid Mirza Reaction Type Ugi Solvent DMSO Limiting Reactant 0.898 M Precipitate Yes Yield - % Comments Reference http://usefulchem.wikispaces.com/Exp222

+

Boc-Gly-OH

+

furfurylamine

+

benzaldehyde

Reaction ID UCEXP222-2 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 0.898 M Precipitate Yes Yield - %

522



t-butyl isocyanide

21106059

Comments Reference

http://usefulchem.wikispaces.com/Exp222

+

Boc-Gly-OH

+

+

furfurylamine

benzaldehyde



t-butyl isocyanide

21106059

Reaction ID UCEXP222-3

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Researcher Khalid Mirza Reaction Type Ugi Solvent DMSO Limiting Reactant 0.473 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp222

+

Boc-Gly-OH

+

+

furfurylamine

benzaldehyde



t-butyl isocyanide

21106059

Reaction ID UCEXP222-4 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 0.473 M Precipitate Yes Yield - % Comments Reference http://usefulchem.wikispaces.com/Exp222

+

Boc-Gly-OH

+

+

furfurylamine

benzaldehyde



t-butyl isocyanide

21106059

Reaction ID UCEXP222-5 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 0.898 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp222

+

1-pyrenebutyric acid

+

methylamine

+

4-(dimethylamino)benzaldehyde

Reaction ID UCEXP222-6 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 0.898 M Precipitate No Comments -

523



t-butyl isocyanide

21105842

Reference

http://usefulchem.wikispaces.com/Exp222

+

1-pyrenebutyric acid

+

methylamine

+

4-methylbenzaldehyde



t-butyl isocyanide

21105844

Reaction ID UCEXP225-1

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.631 M Precipitate Yes Yield - % Comments 0.5 mmol of isocyanide was added to 500uL of a 2M solution of aldehyde; amine and acid Reference http://usefulchem.wikispaces.com/Exp225

+

Boc-Gly-OH

+

furfurylamine

+

piperonal



t-butyl isocyanide

24528157

Reaction ID UCEXP226-1 Researcher David Bulger Reaction Type Ugi Solvent THF Limiting Reactant 0.523 M Precipitate No Comments 0.5 mmol of isocyanide was added to 900uL of a 0.55M solution of aldehyde; amine and acid Reference http://usefulchem.wikispaces.com/Exp226

+

1-pyrenebutyric acid

+

5-methylfurfurylamine

+

benzaldehyde



t-butyl isocyanide

24528165

Reaction ID UCEXP227-1 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 0.261 M Precipitate No Comments 0.5 mmol of isocyanide was added to 500uL of a 0.5M solution of aldehyde; amine and acid Reference http://usefulchem.wikispaces.com/Exp227

+

1-pyrenebutyric acid

+

furfurylamine

+

piperonal

Reaction ID UCEXP228-7 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 0.67 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp228

524



t-butyl isocyanide

24528173

+

1-pyrenebutyric acid

+

+

methylamine

4-methylbenzaldehyde



t-butyl isocyanide

21105844

Reaction ID UCEXP229-1 Researcher David Bulger Reaction Type Ugi Solvent methanol Limiting Reactant 0.667 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp229

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

+

Boc-Trp-OH

+

+

octadecylamine

4-methylbenzaldehyde



t-butyl isocyanide

24534189

Reaction ID UCEXP231-2 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1 M Precipitate aldehyde insoluble at this concentration Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp231

+

crotonic acid

+

benzylamine

+

phenanthrene-9-carboxaldehyde



t-butyl isocyanide

21105601

Reaction ID UCEXP231-3 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 0.75 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp231

+

1-pyrenebutyric acid

+

methylamine

+

2-naphthaldehyde

Reaction ID UCEXP232-01 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.098 M Precipitate Yes Product Pending Comments Reference http://usefulchem.wikispaces.com/Exp232

525



t-butyl isocyanide

21105841

+

Boc-Gly-OH

+

+

furfurylamine

benzaldehyde



t-butyl isocyanide

21106059

Reaction ID UCEXP232-06 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.083 M Precipitate Yes Product Pending Comments Reference http://usefulchem.wikispaces.com/Exp232

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

+

Boc-Gly-OH

+

+

furfurylamine

4-methylbenzaldehyde



t-butyl isocyanide

24528193

Reaction ID UCEXP232-11 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.029 M Precipitate Yes Product Pending Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+

4-(trifluoromethyl)benzaldehyde



t-butyl isocyanide

24528198

Reaction ID UCEXP232-16 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.366 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+

crotonaldehyde

Reaction ID UCEXP232-21 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.008 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

526



t-butyl isocyanide

24528202

+

Boc-Gly-OH

+

+

furfurylamine

diphenylacetaldehyde



t-butyl isocyanide

24528207

Reaction ID UCEXP232-26 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.092 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

+

Boc-Gly-OH

+

furfurylamine

+

cyclohexancarboxaldehyde



t-butyl isocyanide

24528212

Reaction ID UCEXP232-31 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.11 M Precipitate Yes Product Pending Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

+

furfurylamine

2-furaldehyde



t-butyl isocyanide

24528217

Reaction ID UCEXP232-36 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.081 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+

2-hydroxybenzaldehyde

Reaction ID UCEXP232-41 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.083 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

527



t-butyl isocyanide

24528222

+

Boc-Gly-OH

+

+

furfurylamine

o-tolualdehyde



t-butyl isocyanide

24528227

Reaction ID UCEXP232-46 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.066 M Precipitate Yes Product Pending Comments Reference http://usefulchem.wikispaces.com/Exp232

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

+

Boc-Gly-OH

+

furfurylamine

+

4-methoxybenzaldehyde



t-butyl isocyanide

24528232

Reaction ID UCEXP232-51 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.106 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+

hexanaldehyde



t-butyl isocyanide

24528237

Reaction ID UCEXP232-56 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.109 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

furfurylamine

+

trans-2-hexenal

Reaction ID UCEXP232-61 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.069 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

528



t-butyl isocyanide

24528242

+

Boc-Gly-OH

+

furfurylamine

+

2-phenylpropionaldehyde



t-butyl isocyanide

24534409

Reaction ID UCEXP232-66 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.067 M Precipitate Yes Product Pending Comments Reference http://usefulchem.wikispaces.com/Exp232

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

+

Boc-Gly-OH

+

+

furfurylamine

m-anisaldehyde



t-butyl isocyanide

24528251

Reaction ID UCEXP232-71 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.106 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp232

+

Boc-Gly-OH

+

+

furfurylamine

2-ethylbutyraldehyde



t-butyl isocyanide

24528256

Reaction ID UCEXP233-1 Researcher David Bulger Reaction Type Ugi Solvent methanol Limiting Reactant 0.921 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp233

+

1-aminocyclohexane-1carboxylic acid

+

benzylamine

+

3,5-dimethoxybenzaldehyde

Reaction ID UCEXP233-11 Researcher David Bulger Reaction Type Ugi Solvent methanol Limiting Reactant 1.021 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp233

529



t-butyl isocyanide

24534439

+

Boc-Pro-OH

+

benzylamine

+

3,5-dimethoxybenzaldehyde



t-butyl isocyanide

24528262

Reaction ID UCEXP233-3 Researcher David Bulger Reaction Type Ugi Solvent methanol Limiting Reactant 0.918 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp233

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

+

phenylpropynoic acid

+

benzylamine

+

3,5-dimethoxybenzaldehyde



t-butyl isocyanide

24528265

Reaction ID UCEXP233-5 Researcher David Bulger Reaction Type Ugi Solvent methanol Limiting Reactant 0.919 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp233

+

Boc-Pro-OH

+

benzylamine

+

3,5-dimethoxybenzaldehyde



t-butyl isocyanide

24528262

Reaction ID UCEXP233-7 Researcher David Bulger Reaction Type Ugi Solvent methanol Limiting Reactant 1.02 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp233

+

1-aminocyclohexane-1carboxylic acid

+

benzylamine

+

3,5-dimethoxybenzaldehyde

Reaction ID UCEXP233-9 Researcher David Bulger Reaction Type Ugi Solvent methanol Limiting Reactant 1.021 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp233

530



t-butyl isocyanide

24534439

+

phenylpropynoic acid

+

benzylamine

+

3,5-dimethoxybenzaldehyde



t-butyl isocyanide

24528265

Reaction ID UCEXP234-1 Researcher David Bulger Reaction Type Ugi Solvent methanol Limiting Reactant 1.004 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp234

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

+

phenylpropynoic acid

+

+

3,5Bis(trifluoromethyl)benzaldehyde

benzylamine



t-butyl isocyanide

24528266

Reaction ID UCEXP234-11 Researcher David Bulger Reaction Type Ugi Solvent methanol Limiting Reactant 0.893 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp234

+

+

glycine methyl ester hydrochloride

Boc-L-Threonine

+

3,5-dimethoxybenzaldehyde



t-butyl isocyanide

24528268

Reaction ID UCEXP234-3 Researcher David Bulger Reaction Type Ugi Solvent methanol Limiting Reactant 1.004 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp234

+

phenylpropynoic acid

+

benzylamine

+

3,5Bis(trifluoromethyl)benzaldehyde

Reaction ID UCEXP234-5 Researcher David Bulger Reaction Type Ugi Solvent methanol Limiting Reactant 0.918 M Precipitate Reactants insoluble Comments Reference http://usefulchem.wikispaces.com/Exp234

531



t-butyl isocyanide

24528266

+

+

Fmoc-Diglycine

benzylamine

+

3,5-dimethoxybenzaldehyde



t-butyl isocyanide

24528270

Reaction ID UCEXP234-7 Researcher David Bulger Reaction Type Ugi Solvent methanol Limiting Reactant 0.918 M Precipitate Reactants insoluble Comments Reference http://usefulchem.wikispaces.com/Exp234

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

+

+

Boc-diglycine

benzylamine

+

3,5-dimethoxybenzaldehyde



t-butyl isocyanide

24528272

Reaction ID UCEXP234-9 Researcher David Bulger Reaction Type Ugi Solvent methanol Limiting Reactant 0.918 M Precipitate Reactants insoluble Comments Reference http://usefulchem.wikispaces.com/Exp234

+

+

Boc-L-Serine

benzylamine

+

3,5-dimethoxybenzaldehyde



t-butyl isocyanide

24528274

Reaction ID UCExp235-1 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1 M Precipitate Yes Product No Comments Reference http://usefulchem.wikispaces.com/Exp235

+

Boc-Gly-OH

+

furfurylamine

+

4-(trifluoromethyl)benzaldehyde

Reaction ID UCExp236-04 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.844 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp236

532



t-butyl isocyanide

24528198

+

methacrylic acid

+

butylamine

+

4-(trifluoromethyl)benzaldehyde



t-butyl isocyanide

24528278

Reaction ID UCExp236-05 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.65 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp236

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

+

formic acid

+

t-butylamine

+

4-(trifluoromethyl)benzaldehyde



t-butyl isocyanide

24528279

Reaction ID UCExp236-07 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.614 M Precipitate Yes Yield - % Comments Reference http://usefulchem.wikispaces.com/Exp236

+

3,3'-dichloropivalic acid

+

1-hexylamine

+

4-(trifluoromethyl)benzaldehyde



t-butyl isocyanide

24528280

Reaction ID UCExp236-08 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.65 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp236

+

formic acid

+

3-chloroaniline

+

4-(trifluoromethyl)benzaldehyde

Reaction ID UCExp236-09 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.614 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp236

533



t-butyl isocyanide

24528281

+

3,3'-dichloropivalic acid

+

2-chloroaniline

+

4-(trifluoromethyl)benzaldehyde



t-butyl isocyanide

24528282

Reaction ID UCExp236-11 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.65 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp236

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

+

formic acid

+

benzylamine

+

4-(trifluoromethyl)benzaldehyde



t-butyl isocyanide

24528284

Reaction ID UCExp236-12 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.636 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp236

+

+

methacrylic acid

aniline

+

4-(trifluoromethyl)benzaldehyde



t-butyl isocyanide

24528285

Reaction ID UCExp236-14 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.856 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp236

+

3,3'-dichloropivalic acid

+

methylamine

+

5-bromo-2thiophenecarboxaldehyde

Reaction ID UCExp236-15 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.614 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp236

534



t-butyl isocyanide

24528287

+

3,3'-dichloropivalic acid

+

1-heptylamine

+

4-(trifluoromethyl)benzaldehyde



t-butyl isocyanide

24528288

Reaction ID UCExp236-16 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.872 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp236

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

+

formic acid

+

butylamine

+

4-(trifluoromethyl)benzaldehyde



t-butyl isocyanide

24528289

Reaction ID UCExp236-18 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.858 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp236

+

3,3'-dichloropivalic acid

+

methylamine

+

2,4-dimethylbenzaldehyde



t-butyl isocyanide

24528291

Reaction ID UCExp236-21 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.65 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp236

+

formic acid

+

aniline

+

4-(trifluoromethyl)benzaldehyde

Reaction ID UCExp236-22 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.614 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp236

535



t-butyl isocyanide

24528294

+

3,3'-dichloropivalic acid

+

+

5-bromo-2thiophenecarboxaldehyde

t-butylamine



t-butyl isocyanide

24528295

Reaction ID UCExp236-25 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.615 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp236

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

+

3,3'-dichloropivalic acid

+

+

5-bromo-2thiophenecarboxaldehyde

3-chloroaniline



t-butyl isocyanide

24528298

Reaction ID UCExp236-26 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.612 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp236

+

3,3'-dichloropivalic acid

+

+

5-bromo-2thiophenecarboxaldehyde

benzylamine



t-butyl isocyanide

24528299

Reaction ID UCExp236-27 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.617 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp236

+

3,3'-dichloropivalic acid

+

t-butylamine

+

2,4-dimethylbenzaldehyde

Reaction ID UCExp236-28 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.631 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp236

536



t-butyl isocyanide

24528300

+

methacrylic acid

+

1-hexylamine

+

4-(trifluoromethyl)benzaldehyde



t-butyl isocyanide

24528301

Reaction ID UCExp236-29 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.614 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp236

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

+

3,3'-dichloropivalic acid

+

cyclohexylamine

+

4-(trifluoromethyl)benzaldehyde



t-butyl isocyanide

24528302

Reaction ID UCExp238-13 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.921 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp238

+

crotonic acid

+

2-chloroaniline

+

phenanthrene-9-carboxaldehyde



t-butyl isocyanide

24528315

Reaction ID UCExp238-14 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.919 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp238

+

crotonic acid

+

3-chloroaniline

+

phenanthrene-9-carboxaldehyde

Reaction ID UCExp238-15 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.974 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp238

537



t-butyl isocyanide

24528316

+

+

crotonic acid

aniline

+

phenanthrene-9-carboxaldehyde



t-butyl isocyanide

24528317

Reaction ID UCExp238-16 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.906 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp238

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

+

crotonic acid

+

benzylamine

+

phenanthrene-9-carboxaldehyde



t-butyl isocyanide

21105601

Reaction ID UCExp238-17 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.945 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp238

+

crotonic acid

+

butylamine

+

phenanthrene-9-carboxaldehyde



t-butyl isocyanide

24528318

Reaction ID UCExp238-18 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.888 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp238

+

crotonic acid

+

cyclohexylamine

+

phenanthrene-9-carboxaldehyde

Reaction ID UCExp238-19 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.658 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp238

538



t-butyl isocyanide

24528319

+

crotonic acid

+

furfurylamine

+

phenanthrene-9-carboxaldehyde



t-butyl isocyanide

24528320

Reaction ID UCExp238-20 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.775 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp238

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

+

crotonic acid

+

1-heptylamine

+

phenanthrene-9-carboxaldehyde



t-butyl isocyanide

21106058

Reaction ID UCExp238-21 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.831 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp238

+

crotonic acid

+

1-hexylamine

+

phenanthrene-9-carboxaldehyde



t-butyl isocyanide

24528321

Reaction ID UCExp238-22 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.867 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp238

+

crotonic acid

+

methylamine

+

phenanthrene-9-carboxaldehyde

Reaction ID UCExp238-23 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 2.009 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp238

539



t-butyl isocyanide

24528322

+

crotonic acid

+

1-propylamine

+

phenanthrene-9-carboxaldehyde



t-butyl isocyanide

24528323

Reaction ID UCExp238-24 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.921 M Precipitate Yes but solvent evaporated Comments Reference http://usefulchem.wikispaces.com/Exp238

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

+

crotonic acid

+

t-butylamine

+

phenanthrene-9-carboxaldehyde



t-butyl isocyanide

24528324

Reaction ID UCExp238-37 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.718 M Precipitate Yes but solvent evaporated Comments Reference http://usefulchem.wikispaces.com/Exp238

+

Boc-Gly-OH

+

2-chloroaniline

+

phenanthrene-9-carboxaldehyde



t-butyl isocyanide

24528337

Reaction ID UCExp238-38 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.716 M Precipitate Yes but solvent evaporated Comments Reference http://usefulchem.wikispaces.com/Exp238

+

Boc-Gly-OH

+

3-chloroaniline

+

phenanthrene-9-carboxaldehyde

Reaction ID UCExp238-39 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.76 M Precipitate Yes Product Awaiting Characterization Comments Reference http://usefulchem.wikispaces.com/Exp238

540



t-butyl isocyanide

24528338

+

+

Boc-Gly-OH

aniline

+

phenanthrene-9-carboxaldehyde



t-butyl isocyanide

24528339

Reaction ID UCExp238-40 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.706 M Precipitate Yes Product Awaiting Characterization Comments Reference http://usefulchem.wikispaces.com/Exp238

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

+

Boc-Gly-OH

+

benzylamine

+

phenanthrene-9-carboxaldehyde



t-butyl isocyanide

24528340

Reaction ID UCExp238-41 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.737 M Precipitate Yes but solvent evaporated Comments Reference http://usefulchem.wikispaces.com/Exp238

+

Boc-Gly-OH

+

butylamine

+

phenanthrene-9-carboxaldehyde



t-butyl isocyanide

24528341

Reaction ID UCExp238-42 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.399 M Precipitate Yes but solvent evaporated Comments Reference http://usefulchem.wikispaces.com/Exp238

+

Boc-Gly-OH

+

cyclohexylamine

+

phenanthrene-9-carboxaldehyde

Reaction ID UCExp238-43 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.505 M Precipitate Yes Product Awaiting Characterization Comments Reference http://usefulchem.wikispaces.com/Exp238

541



t-butyl isocyanide

24528342

+

Boc-Gly-OH

+

furfurylamine

+

phenanthrene-9-carboxaldehyde



t-butyl isocyanide

24528343

Reaction ID UCExp238-44 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.6 M Precipitate Yes Product Awaiting Characterization Comments Reference http://usefulchem.wikispaces.com/Exp238

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

+

Boc-Gly-OH

+

1-heptylamine

+

phenanthrene-9-carboxaldehyde



t-butyl isocyanide

24528344

Reaction ID UCExp240-02 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.587 M Precipitate Yes Yield - % Comments Reference http://usefulchem.wikispaces.com/Exp240

+

phenylacetic acid

+

furfurylamine

+

phenanthrene-9-carboxaldehyde



t-butyl isocyanide

21791788

Reaction ID UCExp240-08 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.813 M Precipitate Yes but 48h Comments Reference http://usefulchem.wikispaces.com/Exp240

+

phenylacetic acid

+

5-methylfurfurylamine

+

phenanthrene-9-carboxaldehyde

Reaction ID UCExp241-06 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.523 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp241

542



t-butyl isocyanide

24528348

+

3,4methylenedioxyphenylacetic acid

+

+

methylamine

veratraldehyde



t-butyl isocyanide

24528356

Reaction ID UCExp241-07

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.523 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp241

+

3,4methylenedioxyphenylacetic acid

+

+

methylamine

veratraldehyde



t-butyl isocyanide

24528356

Reaction ID UCExp241-17 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.577 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp241

+

3,4methylenedioxyphenylacetic acid

+

+

5-bromo-2thiophenecarboxaldehyde

methylamine



t-butyl isocyanide

24528360

Reaction ID UCExp241-18 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.571 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp241

+

3,4methylenedioxyphenylacetic acid

+

methylamine

+

2,4-dimethylbenzaldehyde

Reaction ID UCExp241-21 Researcher Reaction Type

Khalid Mirza Ugi

543



t-butyl isocyanide

24528361

Solvent methanol Limiting Reactant 0.576 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp241

+

3,4methylenedioxyphenylacetic acid

+

+

methylamine

4-methylbenzaldehyde



t-butyl isocyanide

24528362

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCExp241-22 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.578 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp241

+

3,4methylenedioxyphenylacetic acid

+

+

methylamine

o-tolualdehyde



t-butyl isocyanide

24528363

Reaction ID UCExp241-30 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.717 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp241

+

3,4methylenedioxyphenylacetic acid

+

+

5-bromo-2thiophenecarboxaldehyde

butylamine



t-butyl isocyanide

24528367

Reaction ID UCExp241-33 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.747 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp241

+

3,4methylenedioxyphenylacetic acid

+

3-chloroaniline

+

5-bromo-2thiophenecarboxaldehyde

544



t-butyl isocyanide

24528370

Reaction ID UCExp241-35 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.737 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp241

+

3,4methylenedioxyphenylacetic acid

+

t-butylamine

+

2,4-dimethylbenzaldehyde



t-butyl isocyanide

24528371

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCExp241-37 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.733 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp241

+

3,4methylenedioxyphenylacetic acid

+

cyclohexylamine

+

4-(trifluoromethyl)benzaldehyde



t-butyl isocyanide

24528373

Reaction ID UCExp241-39 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.721 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp241

+

3,4methylenedioxyphenylacetic acid

+

+

5-bromo-2thiophenecarboxaldehyde

aniline



t-butyl isocyanide

24528374

Reaction ID UCExp241-40 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.749 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp241

+

+

+

545



3,4methylenedioxyphenylacetic acid

1-propylamine

2,4-dimethylbenzaldehyde

t-butyl isocyanide

24528375

Reaction ID UCExp241-43

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.71 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp241

+

3,4methylenedioxyphenylacetic acid

+

furfurylamine

+

4-(trifluoromethyl)benzaldehyde



t-butyl isocyanide

24528376

Reaction ID UCExp241-45 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.748 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp241

+

3,4methylenedioxyphenylacetic acid

+

+

5-bromo-2thiophenecarboxaldehyde

t-butylamine



t-butyl isocyanide

24528378

Reaction ID UCExp241-46 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.736 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp241

+

3,4methylenedioxyphenylacetic acid

+

3-chloroaniline

+

2,4-dimethylbenzaldehyde

Reaction ID UCExp241-47 Researcher Reaction Type

Khalid Mirza Ugi

546



t-butyl isocyanide

24528379

Solvent methanol Limiting Reactant 0.715 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp241

+

+

3,4methylenedioxyphenylacetic acid

1-heptylamine

+

4-(trifluoromethyl)benzaldehyde



t-butyl isocyanide

24528380

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCExp241-48 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.734 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp241

+

+

3,4methylenedioxyphenylacetic acid

benzylamine

+

2,4-dimethylbenzaldehyde



t-butyl isocyanide

24528381

Reaction ID UCExp242-2 Researcher Marshall Moritz Reaction Type Ugi Solvent benzene Limiting Reactant 0.436 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp242

+

+

phenylacetic acid

furfurylamine

+

phenanthrene-9-carboxaldehyde



t-butyl isocyanide

24528383

Reaction ID UCExp242-7 Researcher Marshall Moritz Reaction Type Ugi Solvent benzene Limiting Reactant 0.428 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp242

+

phenylacetic acid

+

5-methylfurfurylamine

+

phenanthrene-9-carboxaldehyde

Reaction ID UCExp245-05 Researcher

Khalid Mirza

547



t-butyl isocyanide

24528388

Reaction Type Ugi Solvent methanol Limiting Reactant 0.507 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp245

+

3,4methylenedioxyphenylacetic acid

+

furfurylamine

+

piperonal



t-butyl isocyanide

24528393

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCExp245-06 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.714 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp245

+

3,4methylenedioxyphenylacetic acid

+

furfurylamine

+

piperonal



t-butyl isocyanide

24528393

Reaction ID UCExp245-11 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.504 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp245

+

3,4methylenedioxyphenylacetic acid

+

5-methylfurfurylamine

+

piperonal



t-butyl isocyanide

24528396

Reaction ID UCExp245-12 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.706 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp245

+

3,4methylenedioxyphenylacetic

+

5-methylfurfurylamine

+

piperonal

548



t-butyl isocyanide

24528396

acid

Reaction ID UCExp245-21 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.5 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp245

+

cbz-proline

+

furfurylamine

+

piperonal



t-butyl isocyanide

24528401

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCExp245-22 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.109 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp245

+

cbz-proline

+

furfurylamine

+

piperonal



t-butyl isocyanide

24528401

Reaction ID UCExp245-27 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.494 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp245

+

cbz-proline

+

5-methylfurfurylamine

+

piperonal



t-butyl isocyanide

24528404

Reaction ID UCExp245-28 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.082 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp245

+

cbz-proline

+

5-methylfurfurylamine

+

piperonal

549



t-butyl isocyanide

24528404

Reaction ID UCExp245-33 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.507 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp245

+

3,4methylenedioxyphenylacetic acid

+

+

furfurylamine

piperonal



t-butyl isocyanide

24528407

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCExp245-34 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.714 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp245

+

3,4methylenedioxyphenylacetic acid

+

+

furfurylamine

piperonal



t-butyl isocyanide

24528407

t-butylamine Reaction ID UCEXP181-105V2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.221 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

+

4-chlorophenylacetic acid

+

t-butylamine

+

3,4-dihydroxybenzaldehyde



tosylmethyl isocyanide

24528135

Reaction ID UCEXP187-3 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 1.064 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp187

+

+

+

550



methacrylic acid

t-butylamine

4-(trifluoromethyl)benzaldehyde

t-butyl isocyanide

21143155

Reaction ID UCEXP188-3 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.225 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp188

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

+

methacrylic acid

+

t-butylamine

+

4-(trifluoromethyl)benzaldehyde



t-butyl isocyanide

21143155

Reaction ID UCExp236-01 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.614 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp236

+

3,3'-dichloropivalic acid

+

t-butylamine

+

4-(trifluoromethyl)benzaldehyde



n-butyl isocyanide

24528275

Reaction ID UCExp236-05 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.65 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp236

+

formic acid

+

t-butylamine

+

4-(trifluoromethyl)benzaldehyde

Reaction ID UCExp236-20 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.631 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp236

551



t-butyl isocyanide

24528279

+

methacrylic acid

+

t-butylamine

+

4-(trifluoromethyl)benzaldehyde



n-butyl isocyanide

24528293

Reaction ID UCExp236-22 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.614 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp236

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

+

3,3'-dichloropivalic acid

+

+

5-bromo-2thiophenecarboxaldehyde

t-butylamine



t-butyl isocyanide

24528295

Reaction ID UCExp236-27 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.617 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp236

+

3,3'-dichloropivalic acid

+

t-butylamine

+

2,4-dimethylbenzaldehyde



t-butyl isocyanide

24528300

Reaction ID UCExp238-12 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.881 M Precipitate Yes but solvent evaporated Comments Reference http://usefulchem.wikispaces.com/Exp238

+

crotonic acid

+

t-butylamine

+

phenanthrene-9-carboxaldehyde

Reaction ID UCExp238-24 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.921 M Precipitate Yes but solvent evaporated Comments Reference http://usefulchem.wikispaces.com/Exp238

552



cyclohexylisocyanide

24528314

+

crotonic acid

+

t-butylamine

+

phenanthrene-9-carboxaldehyde



t-butyl isocyanide

24528324

Reaction ID UCExp238-36 Researcher Khalid Mirza Reaction Type Ugi Solvent THF Limiting Reactant 1.686 M Precipitate Yes but solvent evaporated Comments Reference http://usefulchem.wikispaces.com/Exp238

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

+

Boc-Gly-OH

+

t-butylamine

+

phenanthrene-9-carboxaldehyde



cyclohexylisocyanide

24528336

Reaction ID UCExp241-35 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.737 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp241

+

3,4methylenedioxyphenylacetic acid

+

t-butylamine

+

2,4-dimethylbenzaldehyde



t-butyl isocyanide

24528371

Reaction ID UCExp241-45 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.748 M Precipitate No Comments Reference http://usefulchem.wikispaces.com/Exp241

+

3,4methylenedioxyphenylacetic acid

+

t-butylamine

+

5-bromo-2thiophenecarboxaldehyde

tosylmethyl isocyanide Reaction ID UCEXP130-3 Researcher Reaction Type Solvent

Rikesh Parikh Ugi methanol

553



t-butyl isocyanide

24528378

Limiting Reactant 0.429 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp130

+

formic acid

+

+

5-methylfurfurylamine

benzaldehyde



tosylmethyl isocyanide

21106060

Reaction ID UCEXP147-1V2B1

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Researcher Mitesh Shah Reaction Type Ugi Solvent methanol Limiting Reactant 0.659 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp147

+

+

2,3-dihydroxybenzoic acid

methylamine

+

4,7-dimethoxy-1-naphthaldehyde



tosylmethyl isocyanide

21105839

Reaction ID UCEXP151-1V2B10 Researcher Mitesh Shah Reaction Type Ugi Solvent methanol Limiting Reactant 0.694 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp151

+

+

2,4,6-trihydroxybenzoic acid

methylamine

+

3,4-dihydroxybenzaldehyde



tosylmethyl isocyanide

21106049

Reaction ID UCEXP158B-V1B16 Researcher Emily Messner Reaction Type Ugi Solvent methanol Limiting Reactant 0.658 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp158

+

salicylic acid

+

5-methylfurfurylamine

+

4-chlorobenzaldehyde

Reaction ID UCEXP171A/V2B1 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.221 M

554



tosylmethyl isocyanide

21106076

Precipitate Product Comments Reference

Yes Impurities found Protocol from Explan005 followed http://usefulchem.wikispaces.com/Exp171

+

2,3-dihydroxybenzoic acid

+

methylamine

+

4,7-dimethoxy-1-naphthaldehyde



tosylmethyl isocyanide

21105839

Reaction ID UCEXP171C/V2B3

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.222 M Precipitate Reactants Insoluble Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp171

+

2,4,6-trihydroxybenzoic acid

+

methylamine

+

phenanthrene-9-carboxaldehyde



tosylmethyl isocyanide

21106040

Reaction ID UCEXP171EV2B5 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.22 M Precipitate Reactants Insoluble Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp171

+

3,4methylenedioxyphenylacetic acid

+

3-chloroaniline

+

2-hydroxybenzaldehyde



tosylmethyl isocyanide

21106047

Reaction ID UCEXP171GV2B7 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.218 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp171

+

3,4-dihydroxyphenylacetic acid

+

furfurylamine

+

2-naphthaldehyde

Reaction ID UCEXP171HV2B8 Researcher Reaction Type

Khalid Mirza Ugi

555



tosylmethyl isocyanide

21106054

Solvent methanol Limiting Reactant 0.223 M Precipitate Yes Product No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp171

+

2,4,6-trihydroxybenzoic acid

+

methylamine

+

3,5-dimethoxybenzaldehyde



tosylmethyl isocyanide

21105832

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCEXP171IV2B9 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.221 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp171

+

3,4methylenedioxyphenylacetic acid

+

aniline

+

2-hydroxybenzaldehyde



tosylmethyl isocyanide

21106055

Reaction ID UCEXP171JV2B10 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.225 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp171

+

2,4,6-trihydroxybenzoic acid

+

methylamine

+

3,4-dihydroxybenzaldehyde



tosylmethyl isocyanide

21106049

Reaction ID UCEXP173A/V2B13 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.221 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp173

+

4-chlorophenylacetic acid

+

aniline

+

2-hydroxybenzaldehyde

Reaction ID UCEXP173H/V2B20

556



tosylmethyl isocyanide

21106046

Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.22 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp173

+

3,4-dihydroxyphenylacetic acid

+

+

5-methylfurfurylamine

2-naphthaldehyde



tosylmethyl isocyanide

21106053

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCEXP173I/V3B21 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.225 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp173

+

3,4-dihydroxyphenylacetic acid

+

methylamine

+

3-hydroxybenzaldehyde



tosylmethyl isocyanide

21106052

Reaction ID UCEXP173L/V2B24 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.221 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp173

+

3,4-dihydroxyphenylacetic acid

+

furfurylamine

+

3-hydroxybenzaldehyde



tosylmethyl isocyanide

21106051

Reaction ID UCEXP173M/V2B25 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.22 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp173

+

3,4-dihydroxyphenylacetic acid

+

furfurylamine

+

4-chlorobenzaldehyde

557



tosylmethyl isocyanide

21106043

Reaction ID UCEXP173N/V2B26 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.217 M Precipitate Reactants Insoluble Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp173

+

decanoic acid

+

2-chloroaniline

+

o-vanillin



tosylmethyl isocyanide

21105847

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCEXP173O/V2B27 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.222 M Precipitate Yes Product pending Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp173

+

3,4-dihydroxyphenylacetic acid

+

furfurylamine

+

benzaldehyde



tosylmethyl isocyanide

21105843

Reaction ID UCEXP173Q/V2B29 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.22 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp173

+

3,4-dihydroxyphenylacetic acid

+

furfurylamine

+

4-methylbenzaldehyde



tosylmethyl isocyanide

21106042

Reaction ID UCEXP174A/V2B31 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.221 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp174

+

3,4-dihydroxyphenylacetic

+

5-methylfurfurylamine

+

benzaldehyde

558



tosylmethyl isocyanide

21106189

acid

Reaction ID UCEXP174B/V2B33 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.22 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp174

+

3,4-dihydroxyphenylacetic acid

+

furfurylamine

+

3-methoxybenzaldehyde



tosylmethyl isocyanide

21106204

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCEXP174D/V2B35 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.221 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp174

+

benzoic acid

+

furfurylamine

+

2-hydroxybenzaldehyde



tosylmethyl isocyanide

21106202

Reaction ID UCEXP174F/V2B38 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.222 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp174

+

3,4-dihydroxyphenylacetic acid

+

methylamine

+

veratraldehyde



tosylmethyl isocyanide

21106200

Reaction ID UCEXP174G/V2B39 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.222 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp174

+

+

+

559



3,4-dihydroxyphenylacetic acid

1-propylamine

4-methylbenzaldehyde

tosylmethyl isocyanide

21106199

Reaction ID UCEXP174H/V2B40 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.223 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp174

+

2,4,6-trihydroxybenzoic acid

+

+

methylamine

2-naphthaldehyde



tosylmethyl isocyanide

21106188

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Reaction ID UCEXP174I/V2B41 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.224 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp174

+

methacrylic acid

+

aniline

+

3,4-dihydroxybenzaldehyde



tosylmethyl isocyanide

21106198

Reaction ID UCEXP174J/V2B42 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.221 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp174

+

3,4-dihydroxyphenyl acetic acid

+

5-methylfurfurylamine

+

4-chlorobenzaldehyde



tosylmethyl isocyanide

21106197

Reaction ID UCEXP174L/V2B44 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.224 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp174

+

+

+

560



2,4,6-trihydroxybenzoic acid

methylamine

4-methoxybenzaldehyde

tosylmethyl isocyanide

21106195

Reaction ID UCEXP174M/V2B45 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.22 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp174

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

+

2-phenylbutyric acid

+

3-chloroaniline

+

3,4-dihydroxybenzaldehyde



tosylmethyl isocyanide

21106194

Reaction ID UCEXP174P/V2B49 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.22 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp174

+

3,4-dihydroxyphenylacetic acid

+

5-methylfurfurylamine

+

3-methoxybenzaldehyde



tosylmethyl isocyanide

21106192

Reaction ID UCEXP174Q/V2B50 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.222 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp174

+

butyric acid

+

3-chloroaniline

+

2-hydroxybenzaldehyde

Reaction ID UCEXP174R/V2B51 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.221 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp174

561



tosylmethyl isocyanide

21106191

+

mandelic acid

+

3-chloroaniline

+

2-hydroxybenzaldehyde



tosylmethyl isocyanide

21106190

Reaction ID UCEXP174T/V2B53 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.219 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp174

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

+

2,5-dimethoxyphenylacetic acid

+

aniline

+

2-hydroxybenzaldehyde



tosylmethyl isocyanide

21106185

Reaction ID UCEXP174U/V2B54 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.22 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp174

+

3,4-dihydroxyphenylacetic acid

+

furfurylamine

+

4-methoxybenzaldehyde



tosylmethyl isocyanide

21106187

Reaction ID UCEXP181-057V2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.224 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

+

phenylpropynoic acid

+

methylamine

+

2-hydroxybenzaldehyde

Reaction ID UCEXP181-059V2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.225 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

562



tosylmethyl isocyanide

24528098

+

4-hydroxybenzoic acid

+

+

methylamine

2-methylbenzaldehyde



tosylmethyl isocyanide

24528099

Reaction ID UCEXP181-060V2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.221 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

+

phenylpropynoic acid

+

furfurylamine

+

2-hydroxybenzaldehyde



tosylmethyl isocyanide

24528100

Reaction ID UCEXP181-062V2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.223 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

+

4-hydroxybenzoic acid

+

methylamine

+

3,5-dimethoxybenzaldehyde



tosylmethyl isocyanide

24528101

Reaction ID UCEXP181-063V2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.222 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

+

3,4-dihydroxyphenylacetic acid

+

1-propylamine

+

2-hydroxybenzaldehyde

Reaction ID UCEXP181-064V2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.221 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

563



tosylmethyl isocyanide

24528102

+

3-methylbut-2-enoic acid

+

1-hexylamine

+

3,4-dihydroxybenzaldehyde



tosylmethyl isocyanide

24528103

Reaction ID UCEXP181-066V2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.225 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

+

2,4,6-trihydroxybenzoic acid

+

methylamine

+

3-hydroxybenzaldehyde



tosylmethyl isocyanide

24528105

Reaction ID UCEXP181-067V2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.221 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

+

3,4-dihydroxyphenylacetic acid

+

furfurylamine

+

4-hydroxybenzaldehyde



tosylmethyl isocyanide

24528106

Reaction ID UCEXP181-068V2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.224 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

+

3,4-dihydroxyphenylacetic acid

+

methylamine

+

o-vanillin

Reaction ID UCEXP181-069V2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.221 M Precipitate Reactants Insoluble Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

564



tosylmethyl isocyanide

24528107

+

2,4,6-trihydroxybenzoic acid

+

+

aniline

2-naphthaldehyde



tosylmethyl isocyanide

24528108

Reaction ID UCEXP181-071V2

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.221 M Precipitate Yes Product No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

+

mandelic acid

+

+

benzylamine

benzaldehyde



tosylmethyl isocyanide

24528531

Reaction ID UCEXP181-072V2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.224 M Precipitate No Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

+

2,6-dihydroxybenzoic acid

+

methylamine

+

4-(trifluoromethyl)benzaldehyde



tosylmethyl isocyanide

21106207

Reaction ID UCEXP181-080V2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.221 M Precipitate Yes Product Not determined Comments Protocol from Explan005 followed Reference http://usefulchem.wikispaces.com/Exp181

+

2,4,6-trihydroxybenzoic acid

+

aniline

+

3-methoxybenzaldehyde

Reaction ID UCEXP181-082V2 Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.221 M Precipitate No

565



tosylmethyl isocyanide

24528116

Comments Reference

Protocol from Explan005 followed http://usefulchem.wikispaces.com/Exp181

+

3,4-dihydroxyphenylacetic acid

+

furfurylamine

+

3,4-dihydroxybenzaldehyde



tosylmethyl isocyanide

24528118

Reaction ID UCEXP181-085V2

Nature Precedings : doi:10.1038/npre.2010.4416.1 : Posted 4 May 2010

Researcher Khalid Mirza Reaction Type Ugi Solvent methanol Limiting Reactant 0.219 M Precipitate No Comm