Soil microbial community structure and catabolic

Soil microbial community structure and catabolic activity are significantly degenerated in successive rotations of Chinese fir plantations Zeyan Wu1,2,3, Jianjuan Li4,+, Jie Zheng4, Jinfu Liu4, Shuying Liu1, Wenxiong Lin1,2,3,*, Chengzhen Wu4,* 1. Life Sciences College of Fujian Agriculture and Forestry University, Fujian350002, China; 2. Fujian Provincial Key Laboratory of Agroecological Processing and Safety Monitoring, School of Life Sciences, Fujian Agriculture and Forestry University, Fuzhou 350002, China; 3. Key Laboratory of Crop Ecology and Molecular Physiology (Fujian Agriculture and Forestry University), Fujian Province University, Fuzhou 350002, China; 4. Forestry College of Fujian Agriculture and Forestry University, Fujian350002, China. *corresponding author: [email protected]; [email protected] + this authors contributed equally to this work

The optical density OD at 590nm change with incubation time (Day 1) Application: Tecan i-control Tecan i-control , 1.11.1.0 Device: infinite 200Pro Serial number: 1412005097 Serial number of connected stacker: Firmware: V_3.37_07/12_Infinite (JulMAI, 20 2012/13.56.47) V_3.37_07/12_Infinite (Jul 20 2012/13.56.47) System NLDX-PC User nldx-PC\nldx Plate Greiner 96 Flat Bottom Transparent Polystyrene Cat. No.: 655101/655161/655192 Plate-ID (Stacker) Label: Label1 Mode Absorbance Wavelength 590 nm Bandwidth 9 nm Number of Flashes 25 Settle Time 0 ms Start Time: 2016/3/30 13:11:27

A B C D E F G H

1 0.0495 0.0994 0.3155 0.0668 0.0802 0.0848 0.0611 0.0534

Supplementary Table S1. The optical density OD at 590nm change with incubation time (Day 1) 2 3 4 5 6 7 8 9 10 0.0715 0.0492 0.0512 0.0579 0.0551 0.1518 0.0684 0.0508 0.076 0.1214 0.1142 0.0765 0.0904 0.1236 0.0773 0.0854 0.0648 0.1101 0.048 0.0472 0.0773 0.0793 0.0449 0.0456 0.0453 0.1184 0.0602 0.0529 0.1999 0.0467 0.0726 0.0686 0.0461 0.0489 0.1162 0.047 0.1445 0.0535 0.0653 0.0987 0.0776 0.6944 0.0575 0.0502 0.0859 0.0779 0.0446 0.0773 0.0753 0.0734 0.0821 0.0564 0.0885 0.0994 0.0511 0.0649 0.0861 0.0686 0.0597 0.0512 0.0455 0.0493 0.0539 0.0979 0.0513 0.0498 0.0795 0.0574 0.0686 0.1118 0.0619 0.0713

11 0.0501 0.067 0.0456 0.0545 0.0907 0.1001 0.0661 0.0695

12 0.0474 0.0537 0.0836 0.1087 0.0512 0.0688 0.0575 0.0514

The optical density OD at 590nm change with incubation time (Day 2) Application: Tecan i-control Tecan i-control , 1.11.1.0 Device: infinite 200Pro Serial number: 1412005097 Serial number of connected stacker: Firmware: V_3.37_07/12_Infinite (Jul 20 2012/13.56.47) MAI, V_3.37_07/12_Infinite (Jul 20 2012/13.56.47) System NLDX-PC User nldx-PC\nldx Plate Greiner 96 Flat Bottom Transparent Polystyrene Cat. No.: 655101/655161/655192 [GRE96ft.pdfx] Plate-ID (Stacker) Label: Label1 Mode Absorbance Wavelength 590 nm Bandwidth 9 nm Number of Flashes 25 Settle Time 0 ms Start Time:2016/3/31 12:33:52

Supplementary Table S2. The optical density OD at 590nm change with incubation time (Day 2) A B C D E F G H

1 0.0489 0.7902 1.0588 0.4808 0.0867 0.1002 0.0695 0.1054

2 0.0657 0.1208 0.0563 0.1308 0.5877 0.7041 0.0718 0.1369

3 0.0525 1.0191 0.049 0.1878 0.0544 0.0469 0.0642 0.0544

4 0.0518 0.1216 0.356 0.0646 0.0665 0.1204 0.3973 0.0895

5 0.0486 0.0782 0.0757 0.1163 0.0908 0.0706 0.0695 0.0756

6 0.0652 0.1113 0.0462 0.6629 0.0932 0.0729 0.0611 0.0714

7 0.5915 0.7485 0.1418 0.0445 0.7282 0.0945 0.0497 1.8805

8 0.4109 0.1028 0.2912 0.0492 0.0556 0.0939 0.0454 0.1124

9 0.0521 0.7909 0.6247 0.1509 0.0727 0.0929 0.0688 0.0615

10 0.0594 0.0979 0.0616 0.152 0.1035 0.9831 0.0649 0.0679

11 0.0516 0.0641 0.0466 0.4602 0.0904 0.3878 0.0791 0.2221

12 0.0572 0.6421 0.4175 0.0927 0.0828 0.0834 0.3162 0.3673

The optical density OD at 590nm change with incubation time (Day 3) Application: Tecan i-control Tecan i-control , 1.11.1.0 Device: infinite 200Pro Serial number: 1412005097 Serial number of connected stacker: Firmware: V_3.37_07/12_Infinite (Jul 20 2012/13.56.47) MAI, V_3.37_07/12_Infinite (Jul 20 2012/13.56.47) System NLDX-PC User nldx-PC\nldx Plate Greiner 96 Flat Bottom Transparent Polystyrene Cat. No.: 655101/655161/655192 Plate-ID (Stacker) Label: Label1 Mode Absorbance Wavelength 590 nm Bandwidth 9 nm Number of Flashes 25 Settle Time 0 ms Start Time:2016/4/1 12:29:08

A B C D E F G H

1 0.0498 1.075 1.1221 0.6989 0.0783 0.1844 0.078 0.3621

Supplementary Table S3. The optical density OD at 590nm change with incubation time (Day 3) 2 3 4 5 6 7 8 9 10 0.0604 0.058 0.3244 0.0471 0.063 0.5691 0.5206 0.0497 0.053 0.1153 1.1181 0.433 0.0782 0.1068 1.0845 0.1299 1.2627 0.093 0.0555 0.0478 0.6391 0.2771 0.0446 0.4647 0.5514 0.925 0.0522 0.8118 0.3201 0.0887 0.1083 0.8278 0.0499 0.0478 0.1241 0.7939 0.7662 0.058 0.0791 0.3298 0.1498 0.7535 0.0552 0.3797 0.5629 0.8813 0.047 0.2295 0.0805 0.09 0.0788 0.1025 0.0986 1.2471 0.072 0.073 0.5962 0.0776 0.0579 0.0492 0.0453 0.067 0.1101 0.2427 0.0551 0.2628 0.0682 0.0817 2.0064 0.1077 0.0648 0.0632

11 0.0625 0.6725 0.0463 0.4773 0.0795 0.5187 0.0844 0.7789

12 0.082 1.4814 0.6437 0.0783 0.5947 0.0943 0.5581 0.5619

The optical density OD at 590nm change with incubation time (Day 4) Application: Tecan i-control Tecan i-control , 1.11.1.0 Device: infinite 200Pro Serial number: 1412005097 Serial number of connected stacker: Firmware: V_3.37_07/12_Infinite (Jul 20 2012/13.56.47) MAI, V_3.37_07/12_Infinite (Jul 20 2012/13.56.47) System NLDX-PC User nldx-PC\nldx Plate Greiner 96 Flat Bottom Transparent Polystyrene Cat. No.: 655101/655161/655192 Plate-ID (Stacker) Label: Label1 Mode Absorbance Wavelength 590 nm Bandwidth 9 nm Number of Flashes 25 Settle Time 0 ms Start Time:2016/4/2 12:36:28

A B C D E F G H

1 0.05 1.4326 1.1278 0.9215 0.0743 0.3331 0.0981 0.5237

Supplementary Table S4. The optical density OD at 590nm change with incubation time (Day 4) 2 3 4 5 6 7 8 9 10 0.0587 0.062 0.7757 0.0475 0.076 0.5694 0.8352 0.0505 0.0511 0.1072 1.5836 0.617 0.0842 0.1006 1.4596 0.3858 1.5634 0.0892 0.0629 0.0485 1.0148 0.7128 0.0458 0.6947 1.0012 1.1535 0.0575 1.1537 0.5896 0.169 0.1377 1.1744 0.0605 0.0479 0.1553 1.23 0.8935 0.0616 0.1388 0.6032 0.3523 0.7382 0.0537 0.6768 0.8956 1.0209 0.0482 0.6679 0.2648 0.2801 0.089 0.1606 0.1101 1.5658 0.1036 0.1348 0.8423 0.4695 0.0609 0.0498 0.0463 0.0994 0.1145 0.3511 0.0562 0.5536 0.0763 0.1224 2.0548 0.0485 0.068 0.0737

11 0.0671 1.4498 0.0469 0.7938 0.1275 0.5527 0.1107 0.9026

12 0.2836 1.8908 0.7051 0.187 1.2487 0.1318 0.7091 0.6866

The optical density OD at 590nm change with incubation time (Day 5) Application: Tecan i-control Tecan i-control , 1.11.1.0 Device: infinite 200Pro Serial number: 1412005097 Serial number of connected stacker: Firmware: V_3.37_07/12_Infinite (Jul 20 2012/13.56.47) MAI, V_3.37_07/12_Infinite (Jul 20 2012/13.56.47) System NLDX-PC User nldx-PC\nldx Plate Greiner 96 Flat Bottom Transparent Polystyrene Cat. No.: 655101/655161/655192 Plate-ID (Stacker) Label: Label1 Mode Absorbance Wavelength 590 nm Bandwidth 9 nm Number of Flashes 25 Settle Time 0 ms Start Time:2016/4/3 12:46:44

A B C D E F G H

1 0.051 0.9789 1.2072 1.0208 0.0667 0.435 0.1183 0.5575

Supplementary Table S5. The optical density OD at 590nm change with incubation time (Day 5) 2 3 4 5 6 7 8 9 10 0.0597 0.0671 0.6175 0.0478 0.1439 0.5596 0.5227 0.0497 0.051 0.104 1.124 0.799 0.0936 0.0997 1.4038 0.4717 1.5557 0.0891 0.0563 0.0492 0.8585 0.7885 0.0465 0.731 0.4798 1.3287 0.0528 1.1422 0.2948 0.2102 0.1168 1.0738 0.0625 0.0483 0.161 1.0591 1.0026 0.0603 0.1346 0.6634 0.2649 0.7346 0.0539 0.6372 1.1063 1.2583 0.0493 0.6383 0.2137 0.6035 0.0672 0.1043 0.0783 1.5404 0.0769 0.1854 0.6336 0.6876 0.0623 0.0497 0.0468 0.075 0.1094 0.2273 0.0569 0.3357 0.0772 0.1324 1.8354 0.0493 0.0751 0.0784

11 0.0749 1.5403 0.0478 0.4901 0.1187 0.5822 0.1114 0.7953

12 0.2519 1.9098 0.7627 0.2024 1.3099 0.1251 0.7205 0.7265

The optical density OD at 590nm change with incubation time (Day 6) Application: Tecan i-control Tecan i-control , 1.11.1.0 Device: infinite 200Pro Serial number: 1412005097 Serial number of connected stacker: Firmware: V_3.37_07/12_Infinite (Jul 20 2012/13.56.47) MAI, V_3.37_07/12_Infinite (Jul 20 2012/13.56.47) System NLDX-PC User nldx-PC\nldx Plate Greiner 96 Flat Bottom Transparent Polystyrene Cat. No.: 655101/655161/655192 [GRE96ft.pdfx] Plate-ID (Stacker) Label: Label1 Mode Absorbance Wavelength 590 nm Bandwidth 9 nm Number of Flashes 25 Settle Time 0 ms Start Time:2016/4/4 12:25:07

Supplementary Table S6. The optical density OD at 590nm change with incubation time (Day 6) A B C D E F G H

1 0.0547 1.6527 1.2863 1.1142 0.0886 0.5713 0.2262 0.837

2 0.0626 0.1042 0.0705 1.5074 1.0734 1.3899 0.1285 0.3195

3 0.1068 1.8825 0.0493 0.8603 0.0627 0.0501 0.316 0.0576

4 1.252 0.9703 1.4558 0.5197 0.2601 0.8354 1.0031 0.4495

5 0.0494 0.1184 1.0031 0.2192 0.9752 0.4141 1.3099 0.0859

6 0.3262 0.1074 0.0467 1.5034 0.5789 1.1701 0.0633 0.1917

7 0.5492 1.7623 1.0664 0.0638 0.7435 0.0842 0.05 1.8246

8 1.3413 1.3116 0.8946 0.0491 0.0646 0.1445 0.0472 0.0502

9 0.0498 1.5576 1.4701 0.4985 0.7773 0.094 0.0914 0.088

10 0.0519 0.0925 0.0518 1.2065 1.277 1.5959 0.1108 0.0698

11 0.1353 1.922 0.0484 0.8335 0.1161 0.6155 0.1669 0.9189

12 0.3673 2.0557 0.8031 0.3414 1.5575 0.1825 0.7445 0.7599

The optical density OD at 590nm change with incubation time (Day 7) Application: Tecan i-control Tecan i-control , 1.11.1.0 Device: infinite 200Pro Serial number: 1412005097 Serial number of connected stacker: Firmware: V_3.37_07/12_Infinite (Jul 20 2012/13.56.47) MAI, V_3.37_07/12_Infinite (Jul 20 2012/13.56.47) System NLDX-PC User nldx-PC\nldx Plate Greiner 96 Flat Bottom Transparent Polystyrene Cat. No.: 655101/655161/655192 Plate-ID (Stacker) Label: Label1 Mode Absorbance Wavelength 590 nm Bandwidth 9 nm Number of Flashes 25 Settle Time 0 ms Start Time:2016/4/5 12:26:52

Supplementary Table S7. The optical density OD at 590nm change with incubation time (Day 7) A B C D E F G H

1 0.0522 1.3142 1.3458 1.1163 0.0734 0.5985 0.2309 0.828

2 0.064 0.0987 0.0658 1.4427 1.0983 1.343 0.1192 0.2375

3 0.1273 1.4732 0.0506 0.5278 0.0643 0.0514 0.389 0.058

4 0.618 1.1072 1.0836 0.417 0.2114 0.7634 0.9433 0.4169

5 0.0485 0.1359 1.0068 0.2369 1.0202 0.4257 1.1454 0.0992

6 0.3357 0.0944 0.0475 1.3831 0.5115 1.5413 0.0638 0.2426

7 0.5625 1.3602 1.2612 0.0598 0.7447 0.0699 0.05 1.819

8 0.8066 0.8561 0.8328 0.0482 0.0524 0.1407 0.0475 0.0496

9 0.0489 1.531 1.6411 0.8065 0.7008 0.0837 0.0954 0.098

10 0.0593 0.0867 0.0552 1.0876 1.3708 1.5996 0.115 0.0874

11 0.2206 1.5464 0.0483 0.6636 0.1185 0.6374 0.1552 0.8745

12 0.3769 2.1579 0.8567 0.3717 1.335 0.1904 0.842 0.8023

Sample Report Sample ID: Operator: Instrument ID: Acquisition Date: Method: Inj. Sample Notes:

1 zxy Varian GC/MS #1 4/7/2016 15:33 PM D:\2015data\lina20151029\20140712.mth None Supplementary Table S8. PLFA determination of microbial community composition （FCP）

Peaks: 294("Peak Number" 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20

RT (min)

Area

CAS Number

Name

5.259 5.365 5.431 5.514 5.58 5.701 5.772 5.814 5.894 5.951 5.976 6.05 6.093 6.166 6.361 6.504 6.583 6.629 6.685 6.747

2.87E+06 25416 2.13E+06 162884 67083 60052 41337 103406 88141 69287 105947 131283 46326 1.46E+06 609297 377474 113108 64935 108691 231652

151-10-0 17721-95-8 None 13131-19-6 72439-85-1 1746-13-0 877-44-1 37385-06-1 None 56298-75-0 None 540-97-6 None None 90-12-0 90-12-0 29812-79-1 56599-40-7 None 74630-39-0

Benzene, 1,3-dimethoxyPiperidine, 2,6-dimethyl-1-nitrosoOxalic acid, isobutyl nonyl ester N-Methyl-9-aza-tricyclo[6.2.2.0(2,7)]dod 3,5-Dibutoxy-1,1,1,7,7,7-hexamethyl-3,5Benzene, (2-propenyloxy)Benzene, 1,2,4-triethylPentanamide, N-1H-purin-6-ylOxalic acid, isobutyl nonyl ester 1H-Indene, 1-ethyl-2,3-dihydro-1-methylOxalic acid, allyl nonyl ester Cyclohexasiloxane, dodecamethyl1-(4-Isopropylphenyl)-3-(tetrahydrofuryl N-HEXACOSANE Naphthalene, 1-methylNaphthalene, 1-methylHydroxylamine, O-decyl1,3-Dioxane, 4-(hexadecyloxy)-2-pentadec Limonen-6-ol, pivalate 1-Undecene, 4-methyl-

21 22 23 24 25 26 27 28 29 30 31 32 33 34 35 36 37 38 39 40 41 42 43 44 45 46 47 48 49 50 51

6.924 7.013 7.068 7.147 7.233 7.362 7.438 7.505 7.555 7.694 7.744 7.829 7.925 8.015 8.106 8.154 8.223 8.268 8.355 8.406 8.503 8.526 8.704 8.761 8.854 8.934 9.046 9.131 9.276 9.358 9.463

757678 1.33E+06 185712 199790 222883 627578 282992 659624 445700 251921 269219 498240 360546 87585 179602 52957 205860 1.24E+06 131219 235312 137170 183163 388906 256212 162917 197012 216612 142600 165672 184641 1.16E+06

5345-42-6 None 131147-55-2 30889-32-8 1127-76-0 581-40-8 4630/7/3 575-41-7 575-41-7 98419-10-4 575-41-7 719-22-2 None 55320-02-0 None 540-97-6 644-08-6 138345-00-3 644-08-6 111-82-0 None 192823-15-7 620-47-3 2245-38-7 829-26-5 13151-91-2 None 2131-42-2 2500-59-6 53800-02-5 None

Benzene, 1-methoxy-3-methyl-2-nitroN-HEXACOSANE 5-Ethenyl-5-(1-methyl-3-butenyl)-hexahyd 1,3-Dioxolane-4-methanol, 2-pentadecyl-, Naphthalene, 1-ethylNaphthalene, 2,3-dimethylNaphthalene, 1,2,3,5,6,7,8,8a-octahydroNaphthalene, 1,3-dimethylNaphthalene, 1,3-dimethyl4,4-Dimethyl-3-(3-methylbut-2-enylidene) Naphthalene, 1,3-dimethyl2,5-Cyclohexadiene-1,4-dione, 2,6-bis(1, 1-ETHYLNAPHTHALENE 9,12,15-Octadecatrienoic acid, 2,3-bis(a N-HEXACOSANE Cyclohexasiloxane, dodecamethyl1,1'-Biphenyl, 4-methyl7,9-Di-tertbutyl-1-oxaspiro[4,5]deca-6,9 1,1'-Biphenyl, 4-methylDodecanoic acid, methyl ester 3-(2-Methyl-propenyl)-1H-indene Decane, 2,3,5,8-tetramethylBenzene, 1-methyl-3-(phenylmethyl)Naphthalene, 1,6,7-trimethylNaphthalene, 2,3,6-trimethylTridecane, 6-cyclohexyl3-(2-Methyl-propenyl)-1H-indene Naphthalene, 1,4,6-trimethylOxiraneoctanoic acid, 3-octyl-, methyl e Trifluoroacetic acid,n-tridecyl ester N-HEXACOSANE

52 53 54 55 56 57 58 59 60 61 62 63 64 65 66 67 68 69 70 71 72 73 74 75 76 77 78 79 80 81 82

9.606 9.669 9.712 9.825 10.053 10.15 10.418 10.544 10.596 10.687 10.778 10.82 10.917 11.023 11.331 11.36 11.429 11.723 11.857 11.967 12.084 12.212 12.321 12.514 12.656 12.724 12.824 13.071 13.163 13.232 13.283

167041 98974 124959 76654 89256 300148 117456 200723 60712 79063 145240 232565 71500 1.24E+06 82632 43251 765384 214786 87849 134028 250754 469589 83768 2.16E+06 887559 1.34E+06 744196 163704 453606 54365 64191

13151-91-2 556-68-3 1724-39-6 5129-65-7 None 112-95-8 None 10544-96-4 None 36653-82-4 732-26-3 5129-58-8 None None 1724-39-6 None 5129-58-8 630-06-8 54105-67-8 2490-48-4 930-02-9 None 2825-81-2 7132-64-1 5129-66-8 None None 1724-39-6 7132-64-1 112-39-0 55682-91-2

Tridecane, 6-cyclohexylCyclooctasiloxane, hexadecamethylCyclododecanol Dodecanoic acid, 10-methyl-, methyl este Epicedrol Eicosane Oxalic acid, allyl octadecyl ester Octadecane, 6-methylPhthalic acid, methyl octyl ester 1-Hexadecanol Phenol, 2,4,6-tris(1,1-dimethylethyl)Tridecanoic acid, 12-methyl-, methyl est Methoxyacetic acid, 3-tridecyl ester N-HEXACOSANE Cyclododecanol 2-Amino-6,7-dimethyl-5,6,7,8-tetrahydroTridecanoic acid, 12-methyl-, methyl est Hexatriacontane Heptadecane, 2,6-dimethyl1-Hexadecanol, 2-methylOctadecane, 1-(ethenyloxy)Methoxyacetic acid, 3-tridecyl ester 2-Hexadecenoic acid, methyl ester, (E)Pentadecanoic acid, methyl ester Tetradecanoic acid, 12-methyl-, methyl e N-HEXACOSANE N-HEXACOSANE Cyclododecanol Pentadecanoic acid, methyl ester Hexadecanoic acid, methyl ester Heptacosanoic acid, methyl ester

83 84 85 86 87 88 89 90 91 92 93 94 95 96 97 98 99 100 101 102 103 104 105 106 107 108 109 110 111 112 113

13.379 13.459 13.52 13.721 13.865 13.918 13.98 14.186 14.291 14.372 14.497 14.586 14.637 14.758 14.854 14.969 15.102 15.192 15.26 15.291 15.398 15.497 15.578 15.654 15.721 15.787 15.85 15.916 16.09 16.176 16.243

90238 245048 106562 65315 440229 194193 242757 259809 2.06E+06 25168 1.21E+06 991542 276679 1.47E+06 33008 6.34E+06 32160 98274 93550 62120 255762 132634 337103 674823 1.67E+06 357794 780363 279134 1.43E+06 151670 808861

54153-31-0 502-69-2 14852-31-4 None 84-69-5 2416-20-8 15965-99-8 36653-82-4 5129-60-2 None 29812-79-1 1120-25-8 29812-79-1 1120-25-8 949-41-7 5129-60-2 6386-38-5 54410-98-9 949-41-7 None None None 117-84-0 56875-67-3 2490-49-5 10152-61-1 2490-49-5 2825-81-2 2490-49-5 112-86-7 2490-49-5

2-(2-Diethylamino-ethoxy)-fluoren-9-one 2-Pentadecanone, 6,10,14-trimethyl2-Hexadecanol Oxalic acid, dodecyl neopentyl ester 1,2-Benzenedicarboxylic acid, bis(2-meth Hexadecenoic acid, Z-11Oxirane, [(hexadecyloxy)methyl]1-Hexadecanol Pentadecanoic acid, 14-methyl-, methyl e Limonen-6-ol, pivalate Hydroxylamine, O-decyl9-Hexadecenoic acid, methyl ester, (Z)Hydroxylamine, O-decyl9-Hexadecenoic acid, methyl ester, (Z)1H-Cyclopropa[l]phenanthrene,1a,9b-dihyd Pentadecanoic acid, 14-methyl-, methyl e Benzenepropanoic acid, 3,5-bis(1,1-dimet 1-Nonene, 4,6,8-trimethyl1H-Cyclopropa[l]phenanthrene,1a,9b-dihyd Oxalic acid, decyl propyl ester N-HEXACOSANE Oxalic acid, allyl dodecyl ester Di-n-octylphthalate 7-Hexadecenoic acid, methyl ester, (Z)Hexadecanoic acid, 14-methyl-, methyl es Cyclopropaneoctanoic acid, 2-hexyl-, met Hexadecanoic acid, 14-methyl-, methyl es 2-Hexadecenoic acid, methyl ester, (E)Hexadecanoic acid, 14-methyl-, methyl es Erucic acid Hexadecanoic acid, 14-methyl-, methyl es

114 115 116 117 118 119 120 121 122 123 124 125 126 127 128 129 130 131 132 133 134 135 136 137 138 139 140 141 142 143 144

16.284 16.487 16.586 16.69 16.796 16.905 17.036 17.148 17.251 17.4 17.464 17.559 17.668 17.761 17.821 17.877 17.963 18.092 18.18 18.26 18.354 18.536 18.604 18.706 18.781 18.916 19.02 19.084 19.204 19.246 19.384

1.32E+06 583916 278582 234638 2.03E+06 155944 528256 125568 443911 233348 619757 423380 265664 350500 673758 246490 3.97E+06 9.53E+06 2.23E+06 718806 1.02E+06 3.90E+06 562871 406607 390518 463511 289868 361254 1.85E+06 823650 433417

None 10152-61-1 128-37-0 2529-64-8 2490-25-7 56051-53-7 55520-89-3 18835-33-1 18772-36-6 14852-31-4 2490-25-7 112-80-1 2566-89-4 None 629-96-9 5129-61-3 2462-85-3 1937-62-8 112-62-9 112-62-9 20290-84-0 112-61-8 22393-97-1 None 28813-61-8 55162-61-3 18835-33-1 19780-79-1 55124-97-5 55124-97-5 55124-97-5

N-HEXACOSANE Cyclopropaneoctanoic acid, 2-hexyl-, met Butylated Hydroxytoluene Estra-1,3,5(10)-trien-17.beta.-ol Heptadecanoic acid, 10-methyl-, methyl e Cyclopropanebutanoic acid, 2-[[2-[[2-[(2 Hexadecanoic acid, trimethylsilyl ester 1-Hexacosene Cyclodecasiloxane, eicosamethyl2-Hexadecanol Heptadecanoic acid, 10-methyl-, methyl e Oleic Acid 5,8,11,14-Eicosatetraenoic acid, methyl Oleanitrile 1-Eicosanol Heptadecanoic acid, 16-methyl-, methyl e 9,12-Octadecadienoic acid, methyl ester 9-Octadecenoic acid, methyl ester, (E)9-Octadecenoic acid (Z)-, methyl ester 9-Octadecenoic acid (Z)-, methyl ester 9-Octadecenoic acid (Z)-, hexyl ester Octadecanoic acid, methyl ester 9-Hexadecenoic acid, 9-hexadecenyl ester 2-Methyl-Z,Z-3,13-octadecadienol 2-Nonadecanone 2,4-dinitrophenylhydrazin Tetracontane, 3,5,24-trimethyl1-Hexacosene 2-Hexyl-1-octanol Octadecanoic acid, 17-methyl-, methyl es Octadecanoic acid, 17-methyl-, methyl es Octadecanoic acid, 17-methyl-, methyl es

145 146 147 148 149 150 151 152 153 154 155 156 157 158 159 160 161 162 163 164 165 166 167 168 169 170 171 172 173 174 175

19.486 19.622 19.691 19.786 19.87 20.032 20.141 20.273 20.383 20.461 20.542 20.704 20.76 20.88 21.004 21.089 21.172 21.227 21.31 21.375 21.465 21.603 21.681 21.761 21.864 21.937 22.031 22.086 22.111 22.187 22.25

895916 655207 280929 1.40E+06 260577 4.77E+06 366924 1.13E+06 555458 387349 219845 2.25E+06 618476 617341 368398 424587 257364 348186 1.02E+06 76471 1.67E+06 514551 501600 161687 526390 2.24E+06 382790 81795 139441 365344 394860

301-02-0 18919-94-3 22393-97-1 None 56700-76-6 10152-62-2 None 1120-28-1 641-85-0 18748-91-9 None 505-54-4 2566-89-4 2566-89-4 None None 17673-25-5 56554-77-9 6971-40-0 14852-31-4 None 14852-31-4 55334-01-5 2490-48-4 18919-94-3 1120-28-1 None 29812-79-1 74630-39-0 56847-05-3 1235-74-1

9-Octadecenamide, (Z)Tetracosamethyl-cyclododecasiloxane 9-Hexadecenoic acid, 9-hexadecenyl ester N-HEXACOSANE 9,12,15-Octadecatrienoic acid, 2-phenylCyclopropaneoctanoic acid, 2-octyl-, met .alpha.-d-Xylopyranoside, methyl-2,3,4-t Eicosanoic acid, methyl ester Allopregnane Octadecanoic acid, trimethylsilyl ester Cholestane, 2-formyl-3-(2-methylbenzylid Hexadecanedioic acid 5,8,11,14-Eicosatetraenoic acid, methyl 5,8,11,14-Eicosatetraenoic acid, methyl Tricyclo[20.8.0.0(7,16)]triacontane, 1(2 Tricyclo[20.8.0.0(7,16)]triacontane, 1(2 Phorbol 13-Heptadecyn-1-ol 17-Pentatriacontene 2-Hexadecanol N-HEXACOSANE 2-Hexadecanol Phenanthrene, 9-dodecyltetradecahydro1-Hexadecanol, 2-methylTetracosamethyl-cyclododecasiloxane Eicosanoic acid, methyl ester N-HEXACOSANE Hydroxylamine, O-decyl1-Undecene, 4-methyl9-Octadecen-12-ynoic acid, methyl ester 1-Phenanthrenecarboxylic acid, 1,2,3,4,4

176 177 178 179 180 181 182 183 184 185 186 187 188 189 190 191 192 193 194 195 196 197 198 199 200 201 202 203 204 205 206

22.327 22.405 22.425 22.531 22.67 22.69 22.763 22.935 23.182 23.202 23.3 23.407 23.522 23.607 23.686 23.769 23.787 23.865 23.993 24.073 24.154 24.238 24.332 24.363 24.432 24.452 24.583 24.66 24.736 24.831 24.896

96573 369273 158109 3.20E+06 195657 511630 779279 1.31E+06 109315 98628 823179 541093 2.03E+06 537905 176130 218762 195553 318051 1.18E+06 318293 93542 427887 294351 60561 299065 103580 1.69E+06 1.11E+06 561906 233406 152530

17453-58-6 14852-31-4 18835-33-1 301-02-0 301-02-0 301-02-0 301-02-0 None None 55521-22-7 119-47-1 None None None 14852-31-4 None 83040-97-5 61834-65-9 1472-93-1 1472-93-1 2629-11-0 None None 11094-59-0 None 117-81-7 629-96-9 19780-79-1 56630-69-4 18835-33-1 18835-33-1

3-Phorbinepropanoic acid, 9-acetyl-14-et 2-Hexadecanol 1-Hexacosene 9-Octadecenamide, (Z)9-Octadecenamide, (Z)9-Octadecenamide, (Z)9-Octadecenamide, (Z)2-Methyl-Z,Z-3,13-octadecadienol Tricyclo[20.8.0.0(7,16)]triacontane, 1(2 9,12,15-Octadecatrienoic acid, 2,3-bis[( Phenol, 2,2'-methylenebis[6-(1,1-dimethy Tricyclo[20.8.0.0(7,16)]triacontane, 1(2 Tricyclo[20.8.0.0(7,16)]triacontane, 1(2 2-Methyl-Z,Z-3,13-octadecadienol 2-Hexadecanol 12-Methyl-E,E-2,13-octadecadien-1-ol 3-(6,6-Dimethyl-5-oxohept-2-enyl)-cycloh Allopregnane-3,7,11,20-tetra-one Octadecanedioic acid, dimethyl ester Octadecanedioic acid, dimethyl ester d-Homo-24-nor-17-oxachola-20,22-diene-3, 7,8-Epoxylanostan-11-ol, 3-acetoxyTricyclo[20.8.0.0(7,16)]triacontane, 1(2 Docosahexaenoic acid, 1,2,3-propanetriyl Phthalic acid, cyclohexyl 2-pentyl ester BIS(2-Ethylhexyl)phthalate 1-Eicosanol 2-Hexyl-1-octanol 13-Docosenoic acid, methyl ester 1-Hexacosene 1-Hexacosene

207 208 209 210 211 212 213 214 215 216 217 218 219 220 221 222 223 224 225 226 227 228 229 230 231 232 233 234 235 236 237

24.942 25 25.016 25.036 25.056 25.204 25.233 25.262 25.467 25.497 25.518 25.61 25.705 25.804 25.978 26.074 26.172 26.273 26.383 26.55 26.641 26.707 26.803 26.826 26.901 26.932 26.963 27.069 27.234 27.262 27.296

157854 118577 81183 64080 56976 9.31E+06 3.58E+06 5.28E+06 203957 91481 227560 379503 373667 425226 643602 389892 1.15E+06 242364 159533 448344 507650 426961 108429 58425 403717 140598 145366 1.47E+06 1.31E+06 602676 1.42E+06

None 14852-31-4 None 25328-53-4 None 117-81-7 117-81-7 117-81-7 None 119-07-3 127611-84-1 None None 7098-21-7 18919-94-3 17453-58-6 19780-79-1 30656-76-9 77646-82-3 None 2433-97-8 5353-25-3 1602-42-2 17453-58-6 56797-40-1 None None None None None None

Pregnan-3,11-diol-20-one 2-Hexadecanol 3-Methyl-4-(phenylthio)-2-prop-2-enyl-2, Cholestan-3-one, cyclic 1,2-ethanediyl a 3,19;14,15-Diepoxypregnan-20-one, 3,11,1 BIS(2-Ethylhexyl)phthalate Di-2-ethylhexyl phthalate Di-2-ethylhexyl phthalate Phthalic acid, butyl undecyl ester 1,2-Benzenedicarboxylic acid, decyl octy 3',8,8'-Trimethoxy-3-piperidyl-2,2'-bina Serverogenin acetate Tricyclo[20.8.0.0(7,16)]triacontane, 1(2 Tritetracontane Tetracosamethyl-cyclododecasiloxane 3-Phorbinepropanoic acid, 9-acetyl-14-et 2-Hexyl-1-octanol Cholesterol 3-O-[[2-acetoxy]ethyl]5H-Cyclopropa[3,4]benz[1,2-e]azulen-5-on 9-Methyl-Z-10-tetradecen-1-ol acetate Tricosanoic acid, methyl ester Ethanol, 2-(9-octadecenyloxy)-, (Z)N-2,4-Dnp-L-arginine 3-Phorbinepropanoic acid, 9-acetyl-14-et 7-Hexadecenal, (Z)Serverogenin acetate 9,19-Cyclolanostan-3-ol, 24,24-epoxymeth 9,19-Cyclolanostan-3-ol, 24,24-epoxymeth 4,4,6a,6b,8a,11,11,14b-Octamethyl-1,4,4a 4,4,6a,6b,8a,11,11,14b-Octamethyl-1,4,4a 4,4,6a,6b,8a,11,11,14b-Octamethyl-1,4,4a

238 239 240 241 242 243 244 245 246 247 248 249 250 251 252 253 254 255 256 257 258 259 260 261 262 263 264 265 266 267 268

27.463 27.533 27.638 27.739 27.946 28.096 28.281 28.333 28.411 28.441 28.496 28.526 28.679 28.722 28.812 28.903 28.926 29.039 29.234 29.489 29.571 29.591 29.631 29.651 29.711 29.741 29.824 29.847 29.93 30.001 30.075

338780 59094 1.38E+06 3.03E+06 104101 2.75E+06 94448 269560 105764 51783 161688 95760 397442 131566 249729 131230 57828 1.08E+06 1.03E+06 769624 68309 143079 48114 89877 102445 177642 63816 53446 687860 285264 182297

None None None 545-47-1 None 2442-49-1 30365-65-2 14852-31-4 18641-57-1 None 14852-31-4 18835-33-1 17453-58-6 18835-33-1 14852-31-4 25328-53-4 25328-53-4 122-62-3 111-02-4 55373-89-2 25328-53-4 25328-53-4 55521-22-7 None None None 105-92-0 537-40-6 22399-98-0 22399-98-0 22399-98-0

4,4,6a,6b,8a,11,11,14b-Octamethyl-1,4,4a 4,4,6a,6b,8a,11,11,14b-Octamethyl-1,4,4a Serverogenin acetate Lupeol 3,9.beta.;14,15-Diepoxypregn-16-en-20-on Tetracosanoic acid, methyl ester Ergost-8(14)-en-3-ol, (3.beta.)2-Hexadecanol Docosanoic acid, 1,2,3-propanetriyl este Ethyl iso-allocholate 2-Hexadecanol 1-Hexacosene 3-Phorbinepropanoic acid, 9-acetyl-14-et 1-Hexacosene 2-Hexadecanol Cholestan-3-one, cyclic 1,2-ethanediyl a Cholestan-3-one, cyclic 1,2-ethanediyl a Decanedioic acid, bis(2-ethylhexyl) este 2,6,10,14,18,22-Tetracosahexaene, 2,6,10 Pentacosanoic acid, methyl ester Cholestan-3-one, cyclic 1,2-ethanediyl a Cholestan-3-one, cyclic 1,2-ethanediyl a 9,12,15-Octadecatrienoic acid, 2,3-bis[( 3,9.beta.;14,15-Diepoxypregn-16-en-20-on 3,9.beta.;14,15-Diepoxypregn-16-en-20-on 3,9.beta.;14,15-Diepoxypregn-16-en-20-on Rhodopin Trilinolein Docosanedioic acid, dimethyl ester Docosanedioic acid, dimethyl ester Docosanedioic acid, dimethyl ester

269 270 271 272 273 274 275 276 277 278 279 280 281 282 283 284 285 286 287 288 289 290 291 292 293 294 Area Total:

30.131 30.201 30.427 30.55 30.634 30.698 30.725 30.933 30.987 31.007 31.073 31.108 31.138 31.179 31.436 32.005 33.249 33.268 33.883 34.62 34.935 34.954 36.115 36.14 36.509 36.564 1.78E+08

140624 191243 486931 185729 39228 64118 20893 516465 54395 133869 87542 49965 31000 99247 125597 145481 420097 561915 83023 44366 27736 21404 14936 35030 77040 26290

None 77573-09-2 None 14852-31-4 17453-58-6 17453-58-6 17453-58-6 5802-82-4 5802-82-4 5802-82-4 5802-82-4 5802-82-4 4657-58-3 17453-58-6 6059-43-4 42217-02-7 559-74-0 559-74-0 630-06-8 55682-92-3 None None None 30365-65-2 83-48-7 83-48-7

3,9.beta.;14,15-Diepoxypregn-16-en-20-on 2-Butenoic acid, 2-methyl-, 1,1a,1b,4,4a Oxalic acid, allyl pentadecyl ester 2-Hexadecanol 3-Phorbinepropanoic acid, 9-acetyl-14-et 3-Phorbinepropanoic acid, 9-acetyl-14-et 3-Phorbinepropanoic acid, 9-acetyl-14-et Hexacosanoic acid, methyl ester Hexacosanoic acid, methyl ester Hexacosanoic acid, methyl ester Hexacosanoic acid, methyl ester Hexacosanoic acid, methyl ester Cycloartanol 3-Phorbinepropanoic acid, 9-acetyl-14-et Dehydroergosterol 3,5-dinitrobenzoate 1-Chloroeicosane Friedelan-3-one Friedelan-3-one Hexatriacontane Octacosanoic acid, methyl ester 1-Cyclohexene, 1,3,3-trimethyl-2-(1-meth (7a-Isopropenyl-4,5-dimethyloctahydroind 5-Cholestene-3-ol, 24-methylErgost-8(14)-en-3-ol, (3.beta.)Stigmasterol Stigmasterol

PLFA determination of microbial community composition （SCP） Sample Report Sample ID: 2 Operator: zxy Instrument ID: Varian GC/MS #1 Acquisition Date: 4/7/2016 18:38 PM Method: D:\2015data\lina20151029\20140712.mth Inj. Sample Notes: None Supplementary Table S9. PLFA determination of microbial community composition （SCP） Peaks: 227("Peak Number" 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18

RT (min)

Area

CAS Number

Name

5.26 5.365 5.434 5.516 5.58 5.701 5.773 5.812 5.951 5.978 6.051 6.168 6.361 6.505 6.585 6.629 6.687 6.75

2.39E+06 27808 2.10E+06 190366 76001 56212 33895 66560 41475 50965 25932 1.35E+06 586897 305630 73285 36523 71469 130697

151-10-0 2432-99-7 None 13131-19-6 72439-85-1 1470-94-6 877-44-1 None 56298-75-0 29812-79-1 540-97-6 None 90-12-0 91-57-6 17071-54-4 56599-40-7 544-76-3 195194-80-0

Benzene, 1,3-dimethoxyUndecanoic acid, 11-aminoOxalic acid, isobutyl nonyl ester N-Methyl-9-aza-tricyclo[6.2.2.0(2,7)]dod 3,5-Dibutoxy-1,1,1,7,7,7-hexamethyl-3,51H-Inden-5-ol, 2,3-dihydroBenzene, 1,2,4-triethylMethoxyacetic acid, dodecyl ester 1H-Indene, 1-ethyl-2,3-dihydro-1-methylHydroxylamine, O-decylCyclohexasiloxane, dodecamethylN-HEXACOSANE Naphthalene, 1-methyl2-Methylnaphthalene Hexyl octyl ether 1,3-Dioxane, 4-(hexadecyloxy)-2-pentadec Hexadecane 2-Piperidinone, N-[4-bromo-n-butyl]-

19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 35 36 37 38 39 40 41 42 43 44 45 46 47 48

6.926 7.015 7.071 7.149 7.235 7.361 7.505 7.558 7.695 7.746 7.831 7.927 7.954 8.019 8.106 8.271 8.359 8.409 8.507 8.709 8.764 8.856 8.932 9.047 9.13 9.279 9.359 9.464 9.608 9.714

601856 1.29E+06 146022 166505 165181 548818 679898 375802 211756 246417 452741 210608 91766 55782 124801 1.96E+06 107359 477270 226324 174497 159453 118152 149718 181565 163874 207915 170475 947282 153980 127215

5345-42-6 None 13151-80-9 2765/11/9 None 581-40-8 575-41-7 575-41-7 22198-47-6 None 719-22-2 939-27-5 74630-39-0 55401-63-3 630-06-8 138345-00-3 644-08-6 111-82-0 2027-17-0 620-47-3 829-26-5 829-26-5 13151-90-1 14905-56-7 829-26-5 1115-01-1 53800-02-5 None 13151-91-2 1724-39-6

Benzene, 1-methoxy-3-methyl-2-nitroOxalic acid, isobutyl nonyl ester Undecane, 5-cyclohexylPentadecanal1-ETHYLNAPHTHALENE Naphthalene, 2,3-dimethylNaphthalene, 1,3-dimethylNaphthalene, 1,3-dimethyl4'-Ethoxy-2'-hydroxyoctanophenone 1-ETHYLNAPHTHALENE 2,5-Cyclohexadiene-1,4-dione, 2,6-bis(1, Naphthalene, 2-ethyl1-Undecene, 4-methyl9-Octadecenoic acid (Z)-, 2-(acetyloxy)Hexatriacontane 7,9-Di-tertbutyl-1-oxaspiro[4,5]deca-6,9 1,1'-Biphenyl, 4-methylDodecanoic acid, methyl ester Naphthalene, 2-(1-methylethyl)Benzene, 1-methyl-3-(phenylmethyl)Naphthalene, 2,3,6-trimethylNaphthalene, 2,3,6-trimethylTridecane, 5-cyclohexylTetradecane, 2,6,10-trimethylNaphthalene, 2,3,6-trimethylOctadecanoic acid, 9,10-dihydroxy-, meth Trifluoroacetic acid,n-tridecyl ester N-HEXACOSANE Tridecane, 6-cyclohexylCyclododecanol

49 50 51 52 53 54 55 56 57 58 59 60 61 62 63 64 65 66 67 68 69 70 71 72 73 74 75 76 77 78

10.055 10.418 10.779 10.821 11.019 11.062 11.238 11.434 11.729 11.86 12.099 12.217 12.327 12.519 12.659 12.724 12.823 12.891 13.076 13.166 13.235 13.362 13.471 13.871 13.936 14.124 14.193 14.295 14.377 14.501

87717 33334 119720 200878 275105 118757 46472 1.01E+06 109262 66218 149459 351719 98413 2.55E+06 1.06E+06 668149 155782 199376 100278 473932 124205 333551 277362 180220 391110 89573 64837 2.15E+06 119116 635684

None None 732-26-3 5129-58-8 29812-79-1 29812-79-1 None 5129-58-8 29812-79-1 2490-48-4 14852-31-4 14852-31-4 None 7132-64-1 5129-66-8 None 19780-79-1 56875-67-3 2765/11/9 7132-64-1 112-39-0 102608-53-7 502-69-2 84-78-6 1120-25-8 102608-53-7 None 5129-60-2 10152-71-3 56875-67-3

Epicedrol Oxalic acid, allyl octadecyl ester Phenol, 2,4,6-tris(1,1-dimethylethyl)Tridecanoic acid, 12-methyl-, methyl est Hydroxylamine, O-decylHydroxylamine, O-decylMethyl Z-11-tetradecenoate Tridecanoic acid, 12-methyl-, methyl est Hydroxylamine, O-decyl1-Hexadecanol, 2-methyl2-Hexadecanol 2-Hexadecanol Methyl Z-11-tetradecenoate Pentadecanoic acid, methyl ester Tetradecanoic acid, 12-methyl-, methyl e N-HEXACOSANE 2-Hexyl-1-octanol 7-Hexadecenoic acid, methyl ester, (Z)PentadecanalPentadecanoic acid, methyl ester Hexadecanoic acid, methyl ester 3,7,11,15-Tetramethyl-2-hexadecen-1-ol 2-Pentadecanone, 6,10,14-trimethyl1,2-Benzenedicarboxylic acid, butyl octy 9-Hexadecenoic acid, methyl ester, (Z)3,7,11,15-Tetramethyl-2-hexadecen-1-ol 3-Trifluoroacetoxypentadecane Pentadecanoic acid, 14-methyl-, methyl e Cyclopropaneoctanoic acid, 2-[[2-[(2-eth 7-Hexadecenoic acid, methyl ester, (Z)-

79 80 81 82 83 84 85 86 87 88 89 90 91 92 93 94 95 96 97 98 99 100 101 102 103 104 105 106 107 108

14.591 14.763 14.867 14.989 15.113 15.195 15.262 15.393 15.507 15.583 15.657 15.724 15.79 15.853 15.923 16.093 16.175 16.249 16.341 16.49 16.589 16.622 16.798 16.894 17.04 17.25 17.47 17.564 17.674 17.769

1.88E+06 2.14E+06 133069 8.47E+06 114858 76019 67353 188462 47640 167417 811869 1.71E+06 181495 518396 220930 1.46E+06 88080 1.43E+06 278432 616245 93049 54904 1.90E+06 75470 308080 176707 571016 247104 157569 314867

1120-25-8 1120-25-8 2416-20-8 5129-60-2 6386-38-5 14852-31-4 112-80-1 29812-79-1 29812-79-1 84-64-0 55044-54-7 2490-49-5 42199-20-2 5129-66-8 2825-81-2 1731-92-6 2490-49-5 2490-49-5 56875-67-3 10152-61-1 128-37-0 112-80-1 2490-25-7 54934-57-5 55520-89-3 18772-36-6 2490-25-7 112-80-1 59149-01-8 None

9-Hexadecenoic acid, methyl ester, (Z)9-Hexadecenoic acid, methyl ester, (Z)Hexadecenoic acid, Z-11Pentadecanoic acid, 14-methyl-, methyl e Benzenepropanoic acid, 3,5-bis(1,1-dimet 2-Hexadecanol Oleic Acid Hydroxylamine, O-decylHydroxylamine, O-decyl1,2-Benzenedicarboxylic acid, butyl cycl 11-Hexadecenoic acid, 15-methyl-, methyl Hexadecanoic acid, 14-methyl-, methyl es Cyclopropanepentanoic acid, 2-undecyl-, Tetradecanoic acid, 12-methyl-, methyl e 2-Hexadecenoic acid, methyl ester, (E)Heptadecanoic acid, methyl ester Hexadecanoic acid, 14-methyl-, methyl es Hexadecanoic acid, 14-methyl-, methyl es 7-Hexadecenoic acid, methyl ester, (Z)Cyclopropaneoctanoic acid, 2-hexyl-, met Butylated Hydroxytoluene Oleic Acid Heptadecanoic acid, 10-methyl-, methyl e Heptadecanoic acid, 9-methyl-, methyl es Hexadecanoic acid, trimethylsilyl ester Cyclodecasiloxane, eicosamethylHeptadecanoic acid, 10-methyl-, methyl e Oleic Acid Methyl (Z)-5,11,14,17-eicosatetraenoate Oleanitrile

109 110 111 112 113 114 115 116 117 118 119 120 121 122 123 124 125 126 127 128 129 130 131 132 133 134 135 136 137 138

17.83 17.889 17.972 18.1 18.189 18.25 18.36 18.541 18.604 18.703 18.794 18.911 19.015 19.091 19.2 19.486 19.626 19.688 19.788 20.033 20.143 20.277 20.467 20.633 20.712 20.772 20.881 20.993 21.089 21.229

793538 197585 6.04E+06 1.06E+07 3.50E+06 1.92E+06 997358 4.21E+06 583741 180798 307489 250822 166469 160326 1.97E+06 387613 332213 71943 723505 3.73E+06 81505 493813 216305 37422 1.21E+06 1.60E+06 568401 105349 342492 229346

629-96-9 5129-61-3 2462-85-3 2716-53-2 112-62-9 150-86-7 112-62-9 112-61-8 10152-62-2 None 20576-58-3 930-02-9 17367-08-7 None 2490-19-9 14435-34-8 18919-94-3 25328-53-4 630-06-8 10152-62-2 2091-29-4 1120-28-1 18748-91-9 19780-79-1 505-54-4 2566-89-4 2734-47-6 14852-31-4 1783-84-2 7459-33-8

1-Eicosanol Heptadecanoic acid, 16-methyl-, methyl e 9,12-Octadecadienoic acid, methyl ester 2,3-Dihydroxypropyl elaidate 9-Octadecenoic acid (Z)-, methyl ester Phytol 9-Octadecenoic acid (Z)-, methyl ester Octadecanoic acid, methyl ester Cyclopropaneoctanoic acid, 2-octyl-, met Z,E-2,13-Octadecadien-1-ol 2,6-Dodecadien-1-ol, 3,7,11-trimethyl-, Octadecane, 1-(ethenyloxy)Ethanol, 2-(9,12-octadecadienyloxy)-, (Z N-HEXACOSANE Octadecanoic acid, 10-methyl-, methyl es 2-Octadecenoic acid, methyl ester Tetracosamethyl-cyclododecasiloxane Cholestan-3-one, cyclic 1,2-ethanediyl a Hexatriacontane Cyclopropaneoctanoic acid, 2-octyl-, met 9-Hexadecenoic acid Eicosanoic acid, methyl ester Octadecanoic acid, trimethylsilyl ester 2-Hexyl-1-octanol Hexadecanedioic acid 5,8,11,14-Eicosatetraenoic acid, methyl 5,8,11,14,17-Eicosapentaenoic acid, meth 2-Hexadecanol 8,11,14-Eicosatrienoic acid, (Z,Z,Z)9,12-Octadecadienoyl chloride, (Z,Z)-

139 140 141 142 143 144 145 146 147 148 149 150 151 152 153 154 155 156 157 158 159 160 161 162 163 164 165 166 167 168

21.309 21.469 21.614 21.676 21.94 22.12 22.187 22.269 22.411 22.524 22.551 22.62 22.7 22.774 22.929 23.015 23.177 23.294 23.397 23.528 23.782 23.867 24.006 24.409 24.506 24.574 24.662 24.741 25.005 25.023

490008 1.12E+06 244282 160683 2.35E+06 35613 88263 81686 130601 443975 335277 209570 66754 220715 352599 57252 64269 219744 102776 2.70E+06 122206 49476 777812 34297 87793 356226 574683 108079 20957 35488

629-96-9 19780-79-1 130385-26-1 55401-75-7 1120-28-1 765-14-0 14852-31-4 37577-58-5 14852-31-4 301-02-0 14852-31-4 301-02-0 301-02-0 14852-31-4 None None 3322-62-1 119-47-1 None None 56847-05-3 None 1472-93-1 127611-84-1 20548-62-3 661-19-8 None 56630-69-4 14852-31-4 130385-26-1

1-Eicosanol 2-Hexyl-1-octanol Z-28-Heptatriaconten-2-one Anthracene, 9-dodecyltetradecahydroEicosanoic acid, methyl ester Vinyl lauryl ether 2-Hexadecanol Heneicosanoic acid, 2,3-dimethyl-, methy 2-Hexadecanol 9-Octadecenamide, (Z)2-Hexadecanol 9-Octadecenamide, (Z)9-Octadecenamide, (Z)2-Hexadecanol 2-Methyl-Z,Z-3,13-octadecadienol 2-Methyl-Z,Z-3,13-octadecadienol 9-Octadecenamide Phenol, 2,2'-methylenebis[6-(1,1-dimethy Tricyclo[20.8.0.0(7,16)]triacontane, 1(2 Tricyclo[20.8.0.0(7,16)]triacontane, 1(2 9-Octadecen-12-ynoic acid, methyl ester Oxalic acid, cyclohexylmethyl tridecyl e Octadecanedioic acid, dimethyl ester 3',8,8'-Trimethoxy-3-piperidyl-2,2'-bina Phthalic acid, bis(7-methyloctyl) ester 1-Docosanol Oxalic acid, allyl octadecyl ester 13-Docosenoic acid, methyl ester 2-Hexadecanol Z-28-Heptatriaconten-2-one

169 170 171 172 173 174 175 176 177 178 179 180 181 182 183 184 185 186 187 188 189 190 191 192 193 194 195 196 197 198

25.221 25.251 25.688 25.805 26.171 26.359 26.644 26.692 26.802 26.903 27.065 27.244 27.285 27.464 27.503 27.537 27.637 27.718 27.743 27.856 27.939 28.102 28.285 28.325 28.443 28.475 28.503 28.526 28.581 28.624

3.44E+06 6.34E+06 30231 29931 361660 12229 175727 125711 14197 153738 123790 25598 18060 9556 15645 11737 618696 27924 76217 151280 48150 2.67E+06 84730 277150 34265 37225 45709 62689 75510 36375

117-81-7 117-81-7 127611-84-1 73105-67-6 None 55521-22-7 2433-97-8 2433-97-8 None 54410-98-9 42235-38-1 55162-61-3 17453-58-6 None 56701-08-7 5767-82-8 2425-77-6 None 2425-77-6 None None 2442-49-1 2442-49-1 2442-49-1 2442-49-1 2442-49-1 2442-49-1 2442-49-1 17453-58-6 17453-58-6

Di-2-ethylhexyl phthalate Di-2-ethylhexyl phthalate 3',8,8'-Trimethoxy-3-piperidyl-2,2'-bina 1-Iodo-2-methylundecane Oxalic acid, allyl octadecyl ester 9,12,15-Octadecatrienoic acid, 2,3-bis[( Tricosanoic acid, methyl ester Tricosanoic acid, methyl ester Ethyl iso-allocholate 1-Nonene, 4,6,8-trimethylEicosanebioic acid, dimethyl ester Tetracontane, 3,5,24-trimethyl3-Phorbinepropanoic acid, 9-acetyl-14-et .alpha.-d-Xylopyranoside, methyl-2,3,4-t Carda-4,20(22)-dienolide, 3-[(6-deoxy-35.alpha.-Pregn-16-en-20-one, 3.beta.,12. 1-Decanol, 2-hexylOxalic acid, allyl octadecyl ester 1-Decanol, 2-hexyl3,9.beta.;14,15-Diepoxypregn-16-en-20-on 3,9.beta.;14,15-Diepoxypregn-16-en-20-on Tetracosanoic acid, methyl ester Tetracosanoic acid, methyl ester Tetracosanoic acid, methyl ester Tetracosanoic acid, methyl ester Tetracosanoic acid, methyl ester Tetracosanoic acid, methyl ester Tetracosanoic acid, methyl ester 3-Phorbinepropanoic acid, 9-acetyl-14-et 3-Phorbinepropanoic acid, 9-acetyl-14-et

199 200 201 202 203 204 205 206 207 208 209 210 211 212 213 214 215 216 217 218 219 220 221 222 223 224 225 226 227 Area Total:

28.669 28.696 28.757 28.784 28.817 28.857 29.045 29.239 29.367 29.493 29.556 29.627 29.647 29.672 29.712 29.744 29.783 29.811 29.921 29.988 30.009 30.069 30.089 30.124 30.301 30.427 30.523 30.573 30.754 1.28E+08

82163 79656 24399 44460 49848 71777 713925 940738 56463 389348 166141 51538 28594 34385 35872 37627 19814 19162 298966 54134 113060 40185 32149 80507 10298 345932 50641 42745 1586

2490-48-4 17453-58-6 55521-22-7 16695-32-2 150-86-7 17453-58-6 2425-77-6 111-02-4 None 55373-89-2 55373-89-2 7199-92-0 25328-53-4 17453-58-6 105-92-0 105-92-0 80097-22-9 7199-92-0 None 56599-45-2 30365-65-2 17453-58-6 17453-58-6 17453-58-6 None 195194-80-0 55282-12-7 18835-33-1 75857-77-1

1-Hexadecanol, 2-methyl3-Phorbinepropanoic acid, 9-acetyl-14-et 9,12,15-Octadecatrienoic acid, 2,3-bis[( 2H-Pyran, 2-(7-dodecynyloxy)tetrahydroPhytol 3-Phorbinepropanoic acid, 9-acetyl-14-et 1-Decanol, 2-hexyl2,6,10,14,18,22-Tetracosahexaene, 2,6,10 Tricyclo[20.8.0.0(7,16)]triacontane, 1(2 Pentacosanoic acid, methyl ester Pentacosanoic acid, methyl ester Cholesta-8,24-dien-3-ol, 4-methyl-, (3.b Cholestan-3-one, cyclic 1,2-ethanediyl a 3-Phorbinepropanoic acid, 9-acetyl-14-et Rhodopin Rhodopin 17.beta.-Acetoxy-1',1'-dicarboethoxy-1.b Cholesta-8,24-dien-3-ol, 4-methyl-, (3.b Ethyl iso-allocholate 9-Octadecenoic acid, (2-phenyl-1,3-dioxo Ergost-8(14)-en-3-ol, (3.beta.)3-Phorbinepropanoic acid, 9-acetyl-14-et 3-Phorbinepropanoic acid, 9-acetyl-14-et 3-Phorbinepropanoic acid, 9-acetyl-14-et .pi.-Pentamethylcyclopentadienyl-trichlo 2-Piperidinone, N-[4-bromo-n-butyl]Octadecane, 3-ethyl-5-(2-ethylbutyl)1-Hexacosene 1'-Carboethoxy-1'-cyano-1.beta.,2.beta.-

PLFA determination of microbial community composition （TCP） Sample Report Sample ID: 3 Operator: zxy Instrument ID: Varian GC/MS #1 Acquisition Date: 4/7/2016 20:21 PM Method: D:\2015data\lina20151029\20140712.mth Supplementary Table S10. PLFA determination of microbial community composition （TCP） Peaks: 265("Peak Number" RT (min) Area CAS Number Name 1 5.258 2.85E+06 151-10-0 Benzene, 1,3-dimethoxy2 5.364 18580 17721-95-8 Piperidine, 2,6-dimethyl-1-nitroso3 5.43 1.40E+06 None Oxalic acid, isobutyl nonyl ester 4 5.512 67964 55299-24-6 2H-1,4-Benzodiazepin-2-one, 7-chloro-1,3 5 5.578 41661 72439-85-1 3,5-Dibutoxy-1,1,1,7,7,7-hexamethyl-3,56 5.699 4.30E+04 622-86-6 Benzene, (2-chloroethoxy)7 5.768 16101 877-44-1 Benzene, 1,2,4-triethyl8 5.812 52894 3913/2/8 1-Octanol, 2-butyl9 5.888 34349 13641-74-2 Dimethoxyamphetamine, 2,510 5.951 28515 None Oxalic acid, isobutyl nonyl ester 11 5.973 39172 29812-79-1 Hydroxylamine, O-decyl12 6.049 11920 540-97-6 Cyclohexasiloxane, dodecamethyl13 6.165 1.06E+06 None Oxalic acid, isobutyl nonyl ester 14 6.358 282420 90-12-0 Naphthalene, 1-methyl15 6.503 191360 91-57-6 2-Methylnaphthalene 16 6.581 50506 None Oxalic acid, dodecyl hexyl ester 17 6.626 21092 72439-85-1 3,5-Dibutoxy-1,1,1,7,7,7-hexamethyl-3,518 6.683 49664 55134-08-2 Benzene, (2,3-dimethyldecyl)19 6.745 108237 29812-79-1 Hydroxylamine, O-decyl20 6.922 6.85E+05 5345-42-6 Benzene, 1-methoxy-3-methyl-2-nitro-

21 22 23 24 25 26 27 28 29 30 31 32 33 34 35 36 37 38 39 40 41 42 43 44 45 46 47 48 49 50

7.011 7.065 7.144 7.23 7.357 7.434 7.5 7.553 7.691 7.743 7.826 7.922 8.014 8.102 8.222 8.265 8.352 8.403 8.5 8.523 8.703 8.757 8.85 8.926 9.042 9.127 9.274 9.355 9.459 9.602

1.25E+06 132221 103005 138149 476176 44980 550282 342176 201657 229090 431406 270168 45773 116453 199040 1.47E+06 98934 156931 94606 105544 214880 1.97E+05 132621 152901 174159 68943 157850 1.82E+05 1.02E+06 148710

None 131147-55-2 30889-32-8 1127-76-0 575-41-7 None 575-41-7 581-40-8 22198-47-6 575-41-7 719-22-2 939-27-5 55320-02-0 None 644-08-6 5875-45-6 643-58-3 111-82-0 None None 620-47-3 829-26-5 2245-38-7 561-83-1 14905-56-7 829-26-5 None 31035-07-1 None 13151-91-2

N-HEXACOSANE 5-Ethenyl-5-(1-methyl-3-butenyl)-hexahyd 1,3-Dioxolane-4-methanol, 2-pentadecyl-, Naphthalene, 1-ethylNaphthalene, 1,3-dimethylAlloaromadendrene oxide-(1) Naphthalene, 1,3-dimethylNaphthalene, 2,3-dimethyl4'-Ethoxy-2'-hydroxyoctanophenone Naphthalene, 1,3-dimethyl2,5-Cyclohexadiene-1,4-dione, 2,6-bis(1, Naphthalene, 2-ethyl9,12,15-Octadecatrienoic acid, 2,3-bis(a N-HEXACOSANE 1,1'-Biphenyl, 4-methylPhenol, 2,5-bis(1,1-dimethylethyl)1,1'-Biphenyl, 2-methylDodecanoic acid, methyl ester 3-(2-Methyl-propenyl)-1H-indene 3-(2-Methyl-propenyl)-1H-indene Benzene, 1-methyl-3-(phenylmethyl)Naphthalene, 2,3,6-trimethylNaphthalene, 1,6,7-trimethylBarbituric acid, 5-allyl-5-neopentylTetradecane, 2,6,10-trimethylNaphthalene, 2,3,6-trimethyl3-(2-Methyl-propenyl)-1H-indene 9-Nonadecene N-HEXACOSANE Tridecane, 6-cyclohexyl-

51 52 53 54 55 56 57 58 59 60 61 62 63 64 65 66 67 68 69 70 71 72 73 74 75 76 77 78 79 80

9.669 9.708 9.784 10.048 10.148 10.231 10.413 10.546 10.591 10.773 10.814 10.882 11.014 11.227 11.325 11.353 11.426 11.479 11.559 11.719 11.854 11.959 12.049 12.093 12.21 12.318 12.51 12.652 12.718 12.816

49111 68452 9888 93417 86175 30240 42597 35781 58832 153901 162352 4.52E+04 407307 94406 5.91E+04 3.66E+04 527055 2.74E+04 18746 127360 57314 50021 71448 84677 288898 5.69E+04 2.22E+06 955536 741276 1.46E+05

556-68-3 143-28-2 7383-90-6 None 629-62-9 21895-14-7 1454-84-8 55282-12-7 None 732-26-3 5129-58-8 61141-66-0 None None None None 5129-58-8 27458-92-0 25117-30-0 29812-79-1 29812-79-1 14852-31-4 14852-31-4 14852-31-4 14852-31-4 2825-81-2 7132-64-1 5129-66-8 None None

Cyclooctasiloxane, hexadecamethylOleyl Alcohol 1,1'-Biphenyl, 3,4'-dimethylEpicedrol Pentadecane Benzene, 1,1'-methylenebis[3-methyl1-Nonadecanol Octadecane, 3-ethyl-5-(2-ethylbutyl)Phthalic acid, methyl nonyl ester Phenol, 2,4,6-tris(1,1-dimethylethyl)Tridecanoic acid, 12-methyl-, methyl est 1,1'-Biphenyl, 3,4-diethylN-HEXACOSANE Methyl Z-11-tetradecenoate E-10-Pentadecenol 2-Amino-6,7-dimethyl-5,6,7,8-tetrahydroTridecanoic acid, 12-methyl-, methyl est Isotridecanol4-Methyldocosane Hydroxylamine, O-decylHydroxylamine, O-decyl2-Hexadecanol 2-Hexadecanol 2-Hexadecanol 2-Hexadecanol 2-Hexadecenoic acid, methyl ester, (E)Pentadecanoic acid, methyl ester Tetradecanoic acid, 12-methyl-, methyl e N-HEXACOSANE Oxalic acid, allyl tridecyl ester

81 82 83 84 85 86 87 88 89 90 91 92 93 94 95 96 97 98 99 100 101 102 103 104 105 106 107 108 109 110

12.874 12.94 13.065 13.159 13.23 13.268 13.356 13.454 13.863 13.918 13.98 14.182 14.286 14.492 14.581 14.752 14.967 15.096 15.184 15.248 15.39 15.492 15.593 15.647 15.716 15.786 15.847 15.911 16.087 16.172

68093 7.05E+04 67135 486604 55587 81628 1.69E+05 130253 253320 204179 87766 87761 2.17E+06 579018 1.24E+06 1.36E+06 6.39E+06 8.21E+04 4.17E+04 8.64E+04 133332 4.02E+04 363306 627140 1.99E+06 337776 741109 154040 1.55E+06 87952

2777-58-4 36653-82-4 2765/11/9 7132-64-1 629-83-4 55682-91-2 102608-53-7 502-69-2 84-78-6 1120-25-8 5129-66-8 36653-82-4 5129-60-2 22393-83-5 1120-25-8 1120-25-8 5129-60-2 6386-38-5 None 2490-48-4 74630-39-0 None 10152-69-9 56875-67-3 2490-49-5 55044-54-7 2490-49-5 2825-81-2 2490-49-5 112-80-1

6-Octadecenoic acid, methyl ester, (Z)1-Hexadecanol PentadecanalPentadecanoic acid, methyl ester Triacontanoic acid, methyl ester Heptacosanoic acid, methyl ester 3,7,11,15-Tetramethyl-2-hexadecen-1-ol 2-Pentadecanone, 6,10,14-trimethyl1,2-Benzenedicarboxylic acid, butyl octy 9-Hexadecenoic acid, methyl ester, (Z)Tetradecanoic acid, 12-methyl-, methyl e 1-Hexadecanol Pentadecanoic acid, 14-methyl-, methyl e 9-Hexadecenoic acid, hexadecyl ester, (Z 9-Hexadecenoic acid, methyl ester, (Z)9-Hexadecenoic acid, methyl ester, (Z)Pentadecanoic acid, 14-methyl-, methyl e Benzenepropanoic acid, 3,5-bis(1,1-dimet Oxalic acid, allyl undecyl ester 1-Hexadecanol, 2-methyl1-Undecene, 4-methylOxalic acid, allyl dodecyl ester Cyclopropanenonanoic acid, 2-[(2-butylcy 7-Hexadecenoic acid, methyl ester, (Z)Hexadecanoic acid, 14-methyl-, methyl es 11-Hexadecenoic acid, 15-methyl-, methyl Hexadecanoic acid, 14-methyl-, methyl es 2-Hexadecenoic acid, methyl ester, (E)Hexadecanoic acid, 14-methyl-, methyl es Oleic Acid

111 112 113 114 115 116 117 118 119 120 121 122 123 124 125 126 127 128 129 130 131 132 133 134 135 136 137 138 139 140

16.24 16.274 16.33 16.48 16.606 16.693 16.792 16.892 17.036 17.25 17.461 17.555 17.664 17.757 17.82 17.874 17.961 18.095 18.178 18.26 18.351 18.531 18.606 18.705 18.781 18.898 19.015 19.081 19.201 19.244

986819 549128 345494 5.08E+05 121724 48577 2.11E+06 89006 2.25E+05 1.87E+05 808355 236028 101762 304339 230412 1.84E+05 4.05E+06 1.14E+07 2.13E+06 505298 537881 3.15E+06 351187 75913 69933 128386 57217 106523 1.21E+06 955814

2490-49-5 None 56875-67-3 10152-61-1 112-80-1 5353-25-3 2490-25-7 54934-57-5 55520-89-3 18772-36-6 2490-25-7 42199-20-2 59149-01-8 None 1454-85-9 112-61-8 112-63-0 2716-53-2 112-62-9 112-62-9 112-62-9 112-61-8 10152-62-2 None 18835-33-1 40710-43-8 871-70-5 None 55124-97-5 55124-97-5

Hexadecanoic acid, 14-methyl-, methyl es N-HEXACOSANE 7-Hexadecenoic acid, methyl ester, (Z)Cyclopropaneoctanoic acid, 2-hexyl-, met Oleic Acid Ethanol, 2-(9-octadecenyloxy)-, (Z)Heptadecanoic acid, 10-methyl-, methyl e Heptadecanoic acid, 9-methyl-, methyl es Hexadecanoic acid, trimethylsilyl ester Cyclodecasiloxane, eicosamethylHeptadecanoic acid, 10-methyl-, methyl e Cyclopropanepentanoic acid, 2-undecyl-, Methyl (Z)-5,11,14,17-eicosatetraenoate Oleanitrile 1-Heptadecanol Octadecanoic acid, methyl ester 9,12-Octadecadienoic acid (Z,Z)-, methyl 2,3-Dihydroxypropyl elaidate 9-Octadecenoic acid (Z)-, methyl ester 9-Octadecenoic acid (Z)-, methyl ester 9-Octadecenoic acid (Z)-, methyl ester Octadecanoic acid, methyl ester Cyclopropaneoctanoic acid, 2-octyl-, met Z,E-3,13-Octadecadien-1-ol 1-Hexacosene 1-Pentacontanol Octadecanedioic acid Oxalic acid, allyl nonyl ester Octadecanoic acid, 17-methyl-, methyl es Octadecanoic acid, 17-methyl-, methyl es

141 142 143 144 145 146 147 148 149 150 151 152 153 154 155 156 157 158 159 160 161 162 163 164 165 166 167 168 169 170

19.38 19.475 19.619 19.685 19.781 19.855 20.027 20.147 20.271 20.376 20.458 20.701 20.759 20.874 20.989 21.083 21.177 21.227 21.306 21.461 21.599 21.677 21.746 21.932 22.013 22.078 22.176 22.262 22.419 22.538

96196 531116 467057 8.79E+04 635791 59477 3.74E+06 122179 649487 64108 68529 1.08E+06 475774 184442 3.55E+04 1.07E+05 53273 95148 200056 734291 195909 81944 73111 1.69E+06 124354 53423 70151 95757 196531 4.93E+06

55124-97-5 629-54-9 556-71-8 593-03-3 630-06-8 14852-31-4 10152-62-2 629-96-9 1120-28-1 None 18748-91-9 505-54-4 2566-89-4 2566-89-4 150-86-7 None 56630-73-0 None 629-96-9 40710-43-8 72845-33-1 55334-01-5 14852-31-4 1120-28-1 4130-54-5 14852-31-4 18835-33-1 37577-58-5 14852-31-4 301-02-0

Octadecanoic acid, 17-methyl-, methyl es Hexadecanamide Cyclononasiloxane, octadecamethyl3-Hexadecanol Hexatriacontane 2-Hexadecanol Cyclopropaneoctanoic acid, 2-octyl-, met 1-Eicosanol Eicosanoic acid, methyl ester Serverogenin acetate Octadecanoic acid, trimethylsilyl ester Hexadecanedioic acid 5,8,11,14-Eicosatetraenoic acid, methyl 5,8,11,14-Eicosatetraenoic acid, methyl Phytol Z,E-2,13-Octadecadien-1-ol 9,15-Octadecadienoic acid, methyl ester 3-(1,5-Dimethyl-hex-4-enyl)-2,2-dimethyl 1-Eicosanol 1-Pentacontanol 1,6-Octadiene, 3-ethoxy-3,7-dimethylPhenanthrene, 9-dodecyltetradecahydro2-Hexadecanol Eicosanoic acid, methyl ester Stearic acid hydrazide 2-Hexadecanol 1-Hexacosene Heneicosanoic acid, 2,3-dimethyl-, methy 2-Hexadecanol 9-Octadecenamide, (Z)-

171 172 173 174 175 176 177 178 179 180 181 182 183 184 185 186 187 188 189 190 191 192 193 194 195 196 197 199 200 Area Total:

22.754 22.848 22.93 23.166 23.29 23.39 23.406 23.522 23.585 23.604 23.778 23.848 23.866 24.206 24.227 24.247 24.309 24.328 24.45 24.578 24.654 24.745 24.819 24.896 24.935 25.007 25.213 25.272 25.439

616073 172929 772930 126947 554800 1.05E+05 130847 921487 118764 461159 150511 42841 64390 123305 33804 42239 68039 63862 177464 1.02E+06 676015 263298 81754 58979 57177 123569 7.27E+06 3.95E+06 161055 1.10E+08

301-02-0 301-02-0 301-02-0 301-02-0 119-47-1 None None None None None None None 18835-33-1 30889-32-8 30889-32-8 55320-07-5 18835-33-1 17453-58-6 None 629-96-9 2425-77-6 18835-33-1 18835-33-1 18835-33-1 74630-16-3 14852-31-4 117-81-7 117-81-7 4376-20-9

9-Octadecenamide, (Z)9-Octadecenamide, (Z)9-Octadecenamide, (Z)9-Octadecenamide, (Z)Phenol, 2,2'-methylenebis[6-(1,1-dimethy Tricyclo[20.8.0.0(7,16)]triacontane, 1(2 Tricyclo[20.8.0.0(7,16)]triacontane, 1(2 Tricyclo[20.8.0.0(7,16)]triacontane, 1(2 2-Methyl-Z,Z-3,13-octadecadienol 2-Methyl-Z,Z-3,13-octadecadienol 2-Myristynoyl pantetheine Oxalic acid, butyl cyclohexylmethyl este 1-Hexacosene 1,3-Dioxolane-4-methanol, 2-pentadecyl-, 1,3-Dioxolane-4-methanol, 2-pentadecyl-, Heptanoic acid, docosyl ester 1-Hexacosene 3-Phorbinepropanoic acid, 9-acetyl-14-et Phthalic acid, 2-ethylhexyl isohexyl est 1-Eicosanol 1-Decanol, 2-hexyl1-Hexacosene 1-Hexacosene 1-Hexacosene Phosphonous dichloride, (1,7,7-trimethyl 2-Hexadecanol Di-2-ethylhexyl phthalate Di-2-ethylhexyl phthalate 1,2-Benzenedicarboxylic acid, mono(2-eth