bulk single crystals of pre-Cso organic superconductors, has received little ... (1) See 'Bucky news service" available on Internet by sending mail to. Buckya sol 1 ...
10392
J. Am. Chem. SOC.1993,115, 10392-10393
Electrocrystallizing Cm: Synthesis, Single Crystal X-ray Structure, and Magnetic (ESR, SQUID) Characterization of [(C&IS)~P]Z[C,][I]~ Alain PCnicaud,'*tJ Aar6n PerCz-Benitez,? R. Gleason V.,J E. Muiloz P..i and R. Escuderos Instituto de Quimica, Instituto de Fisica, and Instituto de Investigaciones en Materiales Universidad Nacional Autonoma de Mgxico Coyoachn, C.P. 04510, M&.xicoD.F., Mgxico Received July 14, I993
Despite the explosion of research' on C602Jmostly due to its novel chemical nature and the discovery of superconductivity4 and ferromagnetism5 in fulleride salts, there still exist only a few families of well-characterized &based materials. We report here on the synthesis by electrocrystallization of high quality single crystals of volume up to 1 mm3 of a salt of formula [(C6H5)4P]2[C6~] [IIx (0 < x
